CN107436273A - A kind of Chinese medicine extract dynamic boiling point saturated vapor pressure analyzer - Google Patents
A kind of Chinese medicine extract dynamic boiling point saturated vapor pressure analyzer Download PDFInfo
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- CN107436273A CN107436273A CN201710741862.3A CN201710741862A CN107436273A CN 107436273 A CN107436273 A CN 107436273A CN 201710741862 A CN201710741862 A CN 201710741862A CN 107436273 A CN107436273 A CN 107436273A
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- chinese medicine
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- vapor pressure
- vacuum
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- 239000003814 drug Substances 0.000 title claims abstract description 32
- 238000009835 boiling Methods 0.000 title claims abstract description 30
- 229920006395 saturated elastomer Polymers 0.000 title claims abstract description 27
- 238000001035 drying Methods 0.000 claims abstract description 8
- 238000010079 rubber tapping Methods 0.000 claims description 10
- 230000001105 regulatory effect Effects 0.000 claims description 9
- 238000000034 method Methods 0.000 description 9
- 238000001514 detection method Methods 0.000 description 8
- 239000003390 Chinese drug Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 2
- 206010067484 Adverse reaction Diseases 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000935 solvent evaporation Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N7/00—Analysing materials by measuring the pressure or volume of a gas or vapour
- G01N7/14—Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference
- G01N7/16—Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference by heating the material
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/02—Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering
- G01N25/08—Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering of boiling point
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Drying Of Solid Materials (AREA)
Abstract
The invention discloses a kind of Chinese medicine extract dynamic boiling point saturated vapor pressure analyzer, including vavuum pump, the vavuum pump is connected with No.1 vacuum buffer tank and No. two vacuum buffer tanks respectively by pipeline, it is connected between the No.1 vacuum buffer tank and No. two vacuum buffer tanks by pipeline, No. two vacuum buffer tanks are connected with drying tower, condenser and ebuillition of heated device in turn by pipeline.The present invention is based on dynamic boiling point saturated vapor pressure correlation theory, it is possible to achieve is detected for the Chinese medicine extract under the conditions of various concentrations in different boiling saturated vapor pressure corresponding with its.
Description
Technical field
The present invention relates to Chinese medicine extract concentration process technical field, more particularly to a kind of Chinese medicine extract dynamic to boil
Point-saturated vapor pressure analyzer.
Background technology
Herbal pharmaceutical is the important component of China's medicinal industry, has been written into the strategical planning of made in China 2025,
Lift the horizontal target of its processing and manufacturing to have gone up as national strategy highly, modernization of Chinese medicine technology is in the complete of socio-economic development
Had great significance in office.But at present, tcm product quality is irregular not between the herbal pharmaceutical industry generally existing batch in China
Together, adverse reaction of tcm accident is reported in media often, and is Chinese medicine the main reason for cause herbal medicine efficacy and quality fluctuation phenomenon
The unstability of extraction process product quality.
Traditional Chinese drug inspissation process is the key link of traditional Chinese medicine quality control, and traditional Chinese drug inspissation is that Chinese medicine extract heats in the external world
Under effect, make the process of its solvent evaporation, obtain the process of high concentration Chinese medical concrete.In the process, the boiling of Chinese medicine extract
Point-saturated vapor pressure can be changed with the raising of Solid content concentration in its solution, and both critical physical parameter is drilled
Change trend then directly affects the regulation of the process control procedure of traditional Chinese drug inspissation.
At present, more fall behind for traditional Chinese drug inspissation process mid-boiling point-research of the saturated vapor pressure in this production process, no
Research and development and the actual requirement of engineering of traditional Chinese drug inspissation production technology can sufficiently be instructed.
Therefore, designing and providing one kind can realize that Chinese medicine extract boiling point-saturated vapor pressure detection device is Chinese medicine life
A production field technical problem urgently to be resolved hurrily.
The content of the invention
The invention aims to overcome deficiency of the prior art, there is provided and a kind of Chinese medicine extract dynamic boiling point-
Saturated vapor pressure analyzer, based on dynamic boiling point-saturated vapor pressure correlation theory, it is possible to achieve under the conditions of various concentrations
Chinese medicine extract is in different boiling saturated vapor pressure detection corresponding with its.
The purpose of the present invention is achieved through the following technical solutions.
A kind of Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer, including vavuum pump, the vavuum pump pass through pipeline
It is connected respectively with No.1 vacuum buffer tank and No. two vacuum buffer tanks, the No.1 vacuum buffer tank and No. two vacuum buffer tanks
Between be connected by pipeline, No. two vacuum buffer tanks by pipeline be connected with turn drying tower, condenser and heating boil
Rise device.
Vacuum valve is provided with the pipeline that the vavuum pump is connected with No.1 vacuum buffer tank, No. two vacuum buffer tanks.
The No.1 vacuum buffer tank top is connected with No.1 vacuum regulating valve and No.1 pressure gauge, and bottom is connected by pipeline
It is connected to No.1 tapping valve.
No. two vacuum buffer tank top is provided with No. two pressure gauges, and bottom is connected with No. two tapping valves by pipeline.
No. two vacuum pressure regulation are provided with the pipeline connected between the No.1 vacuum buffer tank and No. two vacuum buffer tanks
Valve.
No. three pressure gauges are provided with the pipeline connected between the drying tower and condenser.
The ebuillition of heated device is provided with thermometer.
Compared with prior art, beneficial effect caused by technical scheme is:
(1) present invention in, ebuillition of heated device can load relatively large number of Chinese medicine extract, with static method measure boiling point-
Saturated vapor pressure is compared, and this equipment causes it to sample the overall representative of concentration shortage it is possible to prevente effectively from measurement solution detection limit is very few
Detection error caused by property;
(2) in the present invention, using double vacuum buffer tanks-vacuum dual-stage buffer regulation system, it can effectively realize and set
Standby vacustat, avoid the fluctuation of the vacuum in detection process, it is difficult to the phenomenon effectively adjusted;
(3) in the present invention, by the way of same vavuum pump provides double vacuum buffer tanks vacuum source simultaneously, it is possible to protect
Vacuum in card system will not produce larger fluctuation because of the working characteristics of pump in itself, can also reduce equipment cost, keep away
Exempt from equipment waste.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention.
Reference:1 vavuum pump;2 vacuum valves;3 No. two vacuum regulating valves;4 No.1 pressure gauges;5 No. two pressure gauges;6 one
Number vacuum buffer tank;7 No.1 tapping valves;8 No. two vacuum buffer tanks;9 No. two tapping valves;10 drying towers;11 thermometers;12 No. three
Pressure gauge;13 condensers;14 ebuillition of heated devices;15 No.1 vacuum breakers.
Embodiment
The invention will be further described below in conjunction with the accompanying drawings.
To become apparent the purpose of patent of the present invention, feature, below in conjunction with the accompanying drawings to the specific reality of patent of the present invention
The mode of applying is further described.It should be noted that accompanying drawing uses using very simplified form and non-accurately ratio,
Only to purpose that is convenient, lucidly aiding in illustrating patent Example of the present invention.
Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer of the present invention, it is used as detection Chinese medicine extract boiling point-full
With vapour pressure equipment, based on dynamic boiling point-saturated vapor pressure correlation theory, it is possible to achieve for the Chinese medicine under the conditions of various concentrations
Extract solution is in different boiling saturated vapor pressure detection corresponding with its.
As shown in figure 1, Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer of the present invention, including it is vavuum pump 1, dry
Dry tower 10, condenser 13 and ebuillition of heated device 14.The vavuum pump 1 passes through pipeline and No.1 vacuum buffer tank 6 and No. two vacuum
Surge tank 8 is connected, and vacuum valve 2 is housed on the pipeline.The top of No.1 vacuum buffer tank 6 is connected with No.1 vacuum pressure regulation
Valve 15 and No.1 pressure gauge 4, bottom are connected with No.1 tapping valve 7 by pipeline.The No.1 vacuum buffer tank 6 and No. two vacuum
It is connected between surge tank 8 by pipeline, No. two vacuum regulating valves 3 is housed on the pipeline.No. two vacuum buffer tanks 8 top
No. two pressure gauges 5 are installed, bottom is connected with No. two tapping valves 9 by pipeline.No. two vacuum buffer tanks 8 by pipeline with
Drying tower 10 is connected, and the drying tower 10 is connected by pipeline with condenser 13, and No. three pressure gauges 12 are housed on the pipeline.Institute
The condenser 13 stated is connected by pipeline with ebuillition of heated device 14, and the ebuillition of heated device 14 is provided with thermometer 11.
During using this equipment detection Chinese medicine extract boiling point-saturated vapor pressure, a certain amount of Chinese medicine is carried first
Take liquid to add in ebuillition of heated device 14, thermometer 11 is sufficiently submerged in Chinese medicine extract, close No.1 tapping valve 7, two
Number tapping valve 9, No.1 vacuum regulating valve 15 and No. two vacuum regulating valves 3, vacuum valve 2 is opened, give vavuum pump 1 to be powered and start, take out
Air in null device, until pressure that all pressure gauges in equipment are shown reaches minimum, coolant is passed through condenser 13
To the working stability of condenser 13, ebuillition of heated device 14 is opened, when the Chinese medicine extract in ebuillition of heated device 14 comes to life, is adjusted
Small heating power, when making in the enough slow drip back firing equipment of its steam condensing reflux liquid energy, maintain heating power constant, record this
When solution boiling temperature and No. three pressure 12 represent numbers, the pressure registration is the saturated vapor under this solution boiling temperature
Pressure, gradually increasing No.1 vacuum regulating valve 15 and No. two vacuum regulating valves 3 increases equipment pressure, maintenance No.1 pressure during this
The registration of table 4 is higher than No. two registrations of pressure gauge 5, ensures that No. three registrations of pressure gauge 12 are according to 3kpa pressurizations during this regulation
Gradually increase, after being pressurized each time, all maintain a period of time to boil to its thermometer stable reading again to solution, remember respectively
Solution boiling temperature and No. three registrations of pressure gauge 12 under the conditions of the lower different pressures of record, you can obtain under different boiling temperature conditionss
Vapour pressure of the solution saturation corresponding to it.
Although the function and the course of work of the present invention are described above in conjunction with accompanying drawing, the invention is not limited in
Above-mentioned concrete function and the course of work, above-mentioned embodiment is only schematical, rather than restricted, ability
The those of ordinary skill in domain is not departing from present inventive concept and scope of the claimed protection situation under the enlightenment of the present invention
Under, many forms can also be made, these are belonged within the protection of the present invention.
Claims (7)
1. a kind of Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer, including vavuum pump (2), it is characterised in that described true
Empty pump (2) is connected with No.1 vacuum buffer tank (6) and No. two vacuum buffer tanks (8) respectively by pipeline, the No.1 vacuum
It is connected between surge tank (6) and No. two vacuum buffer tanks (8) by pipeline, No. two vacuum buffer tanks (8) pass through pipeline
It is connected with drying tower (10), condenser (13) and ebuillition of heated device (14) in turn.
2. Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer according to claim 1, it is characterised in that described
Vacuum valve (2) is provided with the pipeline that vavuum pump (2) is connected with No.1 vacuum buffer tank (6), No. two vacuum buffer tanks (8).
3. Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer according to claim 1, it is characterised in that described
No.1 vacuum buffer tank (6) top is connected with No.1 vacuum regulating valve (15) and No.1 pressure gauge (4), and bottom is connected by pipeline
There is No.1 tapping valve (7).
4. Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer according to claim 1, it is characterised in that described
No. two vacuum buffer tank (8) tops are provided with No. two pressure gauges (5), and bottom is connected with No. two tapping valves (9) by pipeline.
5. Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer according to claim 1, it is characterised in that described
No. two vacuum regulating valves (3) are provided with the pipeline connected between No.1 vacuum buffer tank (6) and No. two vacuum buffer tanks (8).
6. Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer according to claim 1, it is characterised in that described
No. three pressure gauges (12) are provided with the pipeline connected between drying tower (10) and condenser (13).
7. Chinese medicine extract dynamic boiling point-saturated vapor pressure analyzer according to claim 1, it is characterised in that described
Ebuillition of heated device (14) is provided with thermometer (11).
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111781228A (en) * | 2019-04-04 | 2020-10-16 | 应急管理部化学品登记中心 | Test device for measuring boiling point of viscous substance and application thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111781228A (en) * | 2019-04-04 | 2020-10-16 | 应急管理部化学品登记中心 | Test device for measuring boiling point of viscous substance and application thereof |
CN111781228B (en) * | 2019-04-04 | 2023-07-28 | 中国石油化工股份有限公司 | Test device for measuring boiling point of viscous substance and application thereof |
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