CN107417074A - A kind of preparation method of quartzy ingot, apparatus and system - Google Patents

A kind of preparation method of quartzy ingot, apparatus and system Download PDF

Info

Publication number
CN107417074A
CN107417074A CN201710747278.9A CN201710747278A CN107417074A CN 107417074 A CN107417074 A CN 107417074A CN 201710747278 A CN201710747278 A CN 201710747278A CN 107417074 A CN107417074 A CN 107417074A
Authority
CN
China
Prior art keywords
ingot
quartzy
quartzy ingot
correction factor
sectional dimension
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201710747278.9A
Other languages
Chinese (zh)
Other versions
CN107417074B (en
Inventor
郭飞
张金银
谭路
熊良明
罗杰
杭常东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yangtze Optical Fibre and Cable Co Ltd
Original Assignee
Yangtze Optical Fibre and Cable Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yangtze Optical Fibre and Cable Co Ltd filed Critical Yangtze Optical Fibre and Cable Co Ltd
Priority to CN201710747278.9A priority Critical patent/CN107417074B/en
Publication of CN107417074A publication Critical patent/CN107417074A/en
Application granted granted Critical
Publication of CN107417074B publication Critical patent/CN107417074B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B20/00Processes specially adapted for the production of quartz or fused silica articles, not otherwise provided for
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

The invention discloses a kind of quartzy ingot preparation method, apparatus and system.Methods described controls blanking speed using quartz particles fusion sediment quartz ingot and according to following steps:When in the quartzy ingot of deposition highly less than sectional dimension change critical altitude, deformation caused by quartzy ingot sectional dimension deviation caused by deadweight is compensated according to its highly smaller blanking velocity smaller principle, controls blanking speed;When in the quartzy ingot of deposition highly higher than sectional dimension change critical altitude, the compensation rate for changing critical altitude according to sectional dimension controls blanking speed.Described device includes rotation platform lifting motor, quartz raw material and fed intake amount controller and host computer.The system includes correction factor acquisition module, blanking velocity control module, quartzy ingot height assay module and quartzy ingot hypomere sectional dimension assay module.The present invention obtains the quartzy ingot of size uniform on the premise of precipitation equipment is not increased, do not improve significant loss, reduction manufacturing procedure.

Description

A kind of preparation method of quartzy ingot, apparatus and system
Technical field
The invention belongs to quartz material preparation field, more particularly, to a kind of preparation method of quartzy ingot, device and is System.
Background technology
The quartz material that preform uses have to its appearance uniformity, air bubble content and impurity content etc. compared with For the requirement of harshness, the quartz material prepared at present using glass sand as raw material, its appearance uniformity needs to pass through Follow-up multiple working procedure processing could meet to require.
Gas smelting is the Main Means for preparing quartzy idiosome material using natural siliceous sand as raw material at present, and this method is Quartz sand is melted to the quartzy ingot for being formed and being relatively large in diameter, cross section chi of the obtained quartzy ingot on different height under oxyhydrogen flame Very little deviation is larger, can not meet the requirement of uniaxial direct tensile.To solve the above problems, need manufactured quartzy ingot being put into graphite earthenware Melting traction stretching forms the thinner quartz pushrod of diameter in crucible, but in drawing process is drawn, quartz material is in relatively molten Melt flow regime, quartz pushrod apparent size uniformity is still not easily controlled, and in drawing process quartz material surface very Various impurity and bubble are readily incorporated, need to be made a return journey by being machined or corroding except the uneven part of apparent size and table Face impurity and the higher part of defect content, if desired thinner quartz material, then be stretched to required chi by stretching device again Very little quartz material, in whole process, substantial amounts of material can be wasted during melting traction stretching and machining etc. In material, particularly melting traction drawing process, substantial amounts of material can be remained in crucible.
The size of quartzy ingot prepared by gas smelting is increasing at present, and diameter can be prepared by being mentioned in patent CN105314825A More than 700mm quartzy ingot, quartz material can be reduced to a certain extent in melting traction stretching and other process Loss, but must expect rate be no more than 80%.
A kind of cvd furnace of basic rod structure is refer in patent CN105036520A, the temperature ladder of depositional plane can be reduced Degree, is advantageous to the size uniform of product, but still needs to follow-up melting traction stretch process;
Therefore the manufacturing procedure of reduction quartz material is needed, improves the dimensional homogeneity of quartzy ingot, and reduce impurity Introduce, rate must be expected by being lifted, the further cost for reducing whole preparation process.
The content of the invention
For the disadvantages described above or Improvement requirement of prior art, the invention provides a kind of preparation method of quartzy ingot, dress Put and system, its object is to be compensated by Material control to gravity, using existing quartzy ingot preparation facilities, prepare chi Very little uniform quartzy ingot, and rate height must be expected, thus solve quartzy ingot size prepared by quartzy ingot preparation method it is uneven or The low technical problem of material rate.
To achieve the above object, according to one aspect of the present invention, there is provided a kind of preparation method of quartzy ingot, using stone English particle fusion deposits quartzy ingot and controls blanking speed according to following steps:
When in the quartzy ingot of deposition highly less than sectional dimension change critical altitude, according to its highly smaller blanking velocity Smaller principle compensates to deformation caused by quartzy ingot sectional dimension deviation caused by deadweight, controls blanking speed;
When in the quartzy ingot of deposition highly higher than sectional dimension change critical altitude, change critical height according to sectional dimension The compensation rate control blanking speed of degree.
Preferably, the preparation method of the quartzy ingot, it highly faces when the quartzy ingot in deposition less than sectional dimension change During boundary's height, the blanking speed meets following relation:
V1=[1+k (r, h)] V2r2ρ
Wherein:V1For blanking speed, i.e., raw material injected volume in the unit interval;V2For using the rotation of quartz particles fusion sediment Turn platform fall off rate;R is target quartz ingot radius;ρ is quartz material density;K (r, h) is correction factor, and it is with depositing Quartzy ingot height h dullness positive correlations, itself and the quartzy ingot radius dullness positive correlation in deposition.
Preferably, the preparation method of the quartzy ingot, its correction factor k (r, h) span is 0.02~0.15.
Preferably, the preparation method of the quartzy ingot, its described correction factor determine as follows:
Determine radius r for given target quartz, the correction factor and the quartzy ingot in deposition highly meet with Lower relation:
K (r, h)=α h+ η
Wherein, α and η is constant, and η is burn tinctuer.
Preferably, the preparation method of the quartzy ingot, its described constant α calculate as follows:
α=a/ (1- η);
Wherein, a is negative value or uniform blanking of the gravity pressure that is subject to of quartzy ingot with the slope of highly linear change curve Shi Suoshu quartz ingot cross sectional radius with the slope of highly linear change curve negative value;η is burn tinctuer.
Preferably, the preparation method of the quartzy ingot, it measures the size below fusion sediment position in real time, calculates in real time Quartzy ingot cross sectional radius is with the slope of highly linear change curve, the tune using the negative value of the slope as the correction factor Whole amount, Real-time Feedback adjust the correction factor.
According to another aspect of the present invention, there is provided a kind of preparation facilities of quartzy ingot, including rotation platform lifting electricity Machine, quartz raw material feed intake amount controller and host computer;The rotation platform lifting motor is connected with the host computer signal; The host computer is connected with the quartz raw material injected volume controller signals;
The host computer obtains the rotation platform lifting fall off rate that the rotation platform lifting motor provides, according to this hair The preparation method of bright offer, the quartz raw material is controlled to feed intake the blanking speed of amount controller.
Preferably, the preparation facilities, it also includes dimension measuring device, is arranged near the outer furnace outlet of burner hearth, uses In the quartzy ingot hypomere size of detection.
According to another aspect of the present invention, there is provided a kind of quartzy ingot is prepared with the control system that feeds intake, including amendment system Number acquisition module, blanking velocity control module, quartzy ingot height assay module and quartzy ingot hypomere sectional dimension calibrating mould Block;
The quartzy ingot height assay module, for obtaining the quartzy ingot height in deposition, and submit to the amendment system Number acquisition module;
The quartzy ingot hypomere sectional dimension assay module, for obtaining in its hypomere sectional dimension of the quartzy ingot of deposition, And submit to the correction factor acquisition module;
The correction factor acquisition module, according to the quartzy ingot height and hypomere sectional dimension, determine the amendment Coefficient, and submit to the blanking velocity control module;
It is described descend rate control module, blanking velocity is calculated according to the correction factor and controls blanking.
Preferably, the quartzy ingot is prepared with the control system that feeds intake, its described quartzy height assay module and the blanking Rate control module is connected, and will highly submit to the blanking velocity control module in the quartzy ingot of deposition;
The blanking control module judges whether to recalculate correction factor:
When the quartzy ingot is highly less than or equal to default sectional dimension change critical altitude, amendment system is recalculated Number;Otherwise correction factor is not recalculated.
In general, by the contemplated above technical scheme of the present invention compared with prior art, it can obtain down and show Beneficial effect:
The preparation method of quartzy ingot provided by the invention, according to the target size of quartzy ingot, blanking speed is controlled, compensates stone Deformation caused by the deadweight of English ingot, so that on the premise of precipitation equipment is not increased, do not improve significant loss, reduction manufacturing procedure, Obtain the quartzy ingot of size uniform, diameter fluctuation < 2%.Method provided by the invention, without the melting traction stretching in crucible Process, reduce subsequent processing operations, such as polish, must expect rate so as to improve.
Device provided by the invention, it is simple in construction without accessories such as crucibles.System provided by the invention, can be preferably simultaneous Hold existing fusion sediment device.
Brief description of the drawings
Fig. 1 is quartzy ingot preparation method flow chart provided by the invention;
Fig. 2 is preparation method correction factor provided by the invention with height change curve synoptic diagram;
Fig. 3 is method correction factor provided in an embodiment of the present invention with height change curve synoptic diagram.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, it is right below in conjunction with drawings and Examples The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and It is not used in the restriction present invention.As long as in addition, technical characteristic involved in each embodiment of invention described below Conflict can is not formed each other to be mutually combined.
The preparation method of quartzy ingot provided by the invention, quartzy ingot is deposited using training of qi method and controlled down according to following steps Expect speed:
When in the quartzy ingot of deposition highly less than sectional dimension change critical altitude, according to its highly smaller blanking velocity Smaller principle compensates to deformation caused by quartzy ingot sectional dimension deviation caused by deadweight, controls blanking speed;
When in the quartzy ingot of deposition highly higher than sectional dimension change critical altitude, change critical height according to sectional dimension The compensation rate control blanking speed of degree.
V1=[1+k (r, h)] V2r2ρ
Wherein:V1For blanking speed, i.e., raw material injected volume in the unit interval;V2For using the rotation of quartz particles fusion sediment Turn platform fall off rate;R is target quartz ingot radius;ρ is quartz material density;K (r, h) is correction factor, and it is with depositing Quartzy ingot height h dullness positive correlations, its quartzy ingot radius dullness positive correlation deposited.
Correction factor k (r, h) span is 0.02~0.15.When the quartzy ingot in deposition is highly higher than sectional dimension It is that sectional dimension no longer changes because of epimere pressure to change critical altitude, and now correction factor is by no longer because of the increase of height And change.
The correction factor determines as follows:
Determine radius r for given target quartz, the correction factor and the quartzy ingot in deposition highly meet with Lower relation:
K (r, h)=α h+ η
Wherein, α and η is constant, and η is burn tinctuer.
α can use standardization to carry out linear fit determination, can also calculate as follows:
α=a/ (1- η);
Wherein, a is negative value or uniform blanking of the gravity pressure that is subject to of quartzy ingot with the slope of highly linear change curve Shi Suoshu quartz ingot cross sectional radius with the slope of highly linear change curve negative value;η is burn tinctuer.
Preparation method of the present invention it is critical that determine the value of the correction factor, the correction factor with it is described The quartzy ingot height of deposition is linear related, can be confirmed from following two direction:
On the one hand, theoretically quartzy ingot is regarded as vertical using Differential Principle for the radius r of target quartz ingot It is divided into the geometry of minute cells on direction, the weight dm's of each minute cells, i.e. now minute cells is high apart from sample bottom Dh and the radius r of this minute cells function are spent, is expressed as:
Dm (h, r)=ρ π r2dh;
Then the superposition of each minute cells can be drawn under height h using integral principle, quartzy ingot be subject to from Weight power P (h, r).
The change curve of gravity pressure that quartzy ingot is subject to pressure P (h, r) suffered by height can be drawn, this curve is in Linear relationship, carried out obtaining the linear relation of curve after data fitting, with the increase of height, pressure can reduce. The gravity pressure that quartzy ingot is subject to the slope of highly linear change curve negative value, you can as the correction factor with it is described In the slope of the quartzy ingot highly linear change curve of deposition, i.e. constant a, as shown in Figure 2.
On the other hand, from actual measured results:Within the unit interval, blanking quality and theoretical deposition quartz ingot quality In the case of identical, blanking speed V is set1With the turntable fall off rate V deposited using particle fusion is adapted to2Relation meet:
V1=V2r2ρ;
Quartzy ingot sample is prepared from lower from cylinder upper, that section radius are gradually reduced, the quartzy ingot cross-sectional area with Highly linear changes, and by its linear fit, can obtain the quartzy ingot cross-sectional area with highly linear change curve.The stone English ingot cross-sectional area with the slope of highly linear change curve negative value, you can deposited as the correction factor with described Quartzy ingot highly linear change curve slope, i.e. constant a.
Preferred scheme, the size below fusion sediment position is measured in real time, calculates quartzy ingot cross sectional radius in real time with height Spend linear change slope of a curve, the adjustment amount using the negative value of the slope as the correction factor, Real-time Feedback adjustment institute State correction factor.
The preparation facilities of quartzy ingot provided by the invention, including the control of rotation platform lifting motor, quartz raw material inventory Device, host computer and dimension measuring device;The rotation platform lifting motor is connected with the host computer signal;It is described upper Machine is connected with the quartz raw material injected volume controller signals;
The host computer obtains the rotation platform lifting fall off rate that the rotation platform lifting motor provides, according to this hair The preparation method of the quartzy ingot of bright offer, the quartz raw material is controlled to feed intake the blanking speed of amount controller.
When in the quartzy ingot of deposition highly higher than sectional dimension change critical altitude, under being controlled according to material balance principle Expect speed.
The dimension measuring device, it is arranged near the outer furnace outlet of burner hearth, for detecting quartzy ingot hypomere size.
Dimension measuring device, such as infrared distance sensor are installed below fusion sediment position, for detecting quartz The size of post hypomere, the measurement position are remained in burner hearth, by quartzy cylinder depositional plane hypomere close to stockhole The monitoring of cross-sectional dimension, Real-time Feedback adjust the value of correction factor, last trickle adjustment sedimentation rate, keep deposition flat Weighing apparatus, reduces the floating of the cross-sectional dimension of quartzy cylinder, improves the dimensional homogeneity of quartzy ingot.
, can be according to raw material blanking speed V by above-mentioned control1To adjust fall off rate V2, so that sedimentary is not only Balance can be reached with blanking material in quality, good uniformity can be also kept in product size.
Quartzy ingot preparation feeding system provided by the invention, including correction factor acquisition module, blanking velocity control mould Block, quartzy ingot height assay module and quartzy ingot hypomere sectional dimension assay module;
The quartzy ingot height assay module, for obtaining the quartzy ingot height in deposition, and submit to the amendment system Number acquisition module;
The quartzy ingot hypomere sectional dimension assay module, for obtaining in its hypomere sectional dimension of the quartzy ingot of deposition, And submit to the correction factor acquisition module;
The correction factor acquisition module, according to the quartzy ingot height and hypomere sectional dimension, determine the amendment Coefficient, and submit to the blanking velocity control module;
It is described descend rate control module, blanking velocity is calculated according to the correction factor and controls blanking.
Preferred scheme, the quartzy height assay module is connected with the blanking velocity control module, by the stone of deposition English ingot highly submits to the blanking velocity control module;The blanking control module judges whether to recalculate correction factor: When the quartzy ingot is highly less than or equal to default sectional dimension change critical altitude, correction factor is recalculated;Otherwise Do not recalculate correction factor.
Prior art controls blanking speed simply by raw material blanking quality and the mass balance relation of decline product V1With rotation platform fall off rate V2Relation, not consider answer product should conduct oneself with dignity caused by extruding of the upper strata to lower floor, so as to lead Cause product size that uneven phenomenon is presented.The introducing of correction factor, it can offset in product preparation process because of self extrusion institute Caused dimensional discrepancy, so as to be modified to the sectional dimension of product so that the size fluctuation of quartz material within 2%, According to the radius of product and deposition height, correction factor needs constantly adjustment.When the quartzy ingot in deposition reach a certain height, under After section puddle departs from flame certain distance, temperature declines, and viscosity increase, sectional dimension is no longer because epimere pressure becomes Change, i.e., after the quartzy ingot of deposition highly reaches sectional dimension change critical altitude, correction factor change can be ignored, and be applicable thing Expect balance principle.
It is embodiment below:
A kind of preparation method of quartzy ingot, quartzy ingot is deposited using training of qi method:
Average grain diameter 140um quartz sand is fitted into feeding device, prepares follow-up blanking.First backward blowtorch is passed through hydrogen Lighted with oxygen, form stable oxyhydrogen flame, hydrogen total flow is 158slm, and oxygen total flow is 91slm, and rotation platform is from stove Thorax mouth rises the position of 474mm arrival observation panels with 5.3mm/min speed, and fire box temperature stability contorting is at 1570 DEG C ± 20 DEG C, feeding device is opened, carries out quartz sand feed.
And control blanking speed according to following steps:
When the quartzy ingot in deposition is highly direct less than the distance of flame focus to stockhole+100mm, i.e. fire box temperature energy The height of influence, various sizes of burner hearth, this is highly different, and burner hearth is bigger, and the size is bigger, and the present embodiment burner hearth is applicable Sectional dimension change critical altitude when being 545mm, according to the smaller principle of its highly smaller blanking velocity to caused by deadweight Deformation caused by quartzy ingot sectional dimension deviation compensates, and controls blanking speed;
The blanking speed meets following relation:
V1=[1+k (r, h)] V2r2ρ
Wherein:V1For blanking speed, i.e., raw material injected volume in the unit interval;V2For using the rotation of quartz particles fusion sediment Turn platform fall off rate;R is target quartz ingot radius;ρ is quartz material density;K (r, h) is correction factor, and it is with depositing Quartzy ingot height h dullness positive correlations, itself and the quartzy ingot radius dullness positive correlation in deposition.
Blanking speed is 26.27g/min, and rotation platform rotating speed is 14rpm, and fall off rate is initially set 1.10mm/ min.Fall off rate with deposition can change, and fall off rate can be gradually reduced, and meet V1=k (r, h) V2r2ρ's Relation, after 571min, fall off rate is reduced to 0.87mm/min, stops blanking afterwards.
Correction factor k (r, h) initial value is 0.04, rate of change 0.068, is determined as follows:
Target prepares diameter 140mm quartzy ingot, pre-set radius r=70mm, quartzy ingot is divided into vertical direction micro- Junior unit, the weight m of each minute cells is calculated successively, now the weight m of each minute cells is exactly now minute cells Apart from sample bottom height hnAnd the radius r of this minute cells function, and m (hn, r=68) and=4624 ρ π hn, then basis The superposition of each minute cells is it can be calculated that in different height hnUnder, pressure P that quartzy ingot is subject to, then pass through and be superimposed meter Calculate, it can be deduced that pressure P (h, r) change curve suffered by whole quartzy ingot different height, after being carried out data fitting The linear relation for obtaining curve is P=-0.065h+1.15.This slope of curve is -0.065, takes the negative value 0.065 of the slope, And correction factor k (r, h) rate of change α=0.065/ (1- η), it is 0.068, raw material burn tinctuer is 4%, therefore correction factor k The initial value of (r, h) is 0.04.
The correction factor is according to the size measured in real time below fusion sediment position, according to the size measured in real time The bigger principle of the more big correction factor, Real-time Feedback adjust the correction factor.As shown in Figure 3.
When being highly higher than 545mm in the quartzy ingot of deposition, no longer change correction factor.
Stop blanking, be prepared into size φ 139.4mm ± 2.3mm, height 502mm apparent size is uniform, and quartzy ingot is straight The fluctuation in footpath is less than 2%, and bright quartzy cylindrical material.Directly the stretched device stretching of quartzy cylindrical material is prepared into 42 × 1000mm of diameter quartz column, material rate is obtained as 92.4%.
As it will be easily appreciated by one skilled in the art that the foregoing is merely illustrative of the preferred embodiments of the present invention, not to The limitation present invention, all any modification, equivalent and improvement made within the spirit and principles of the invention etc., all should be included Within protection scope of the present invention.

Claims (10)

1. a kind of preparation method of quartzy ingot, it is characterised in that using quartz particles fusion sediment quartz ingot and according to following step Rapid control blanking speed:
It is smaller according to its highly smaller blanking velocity when in the quartzy ingot of deposition highly less than sectional dimension change critical altitude Principle deformation caused by quartzy ingot sectional dimension deviation caused by deadweight is compensated, control blanking speed;
When in the quartzy ingot of deposition highly higher than sectional dimension change critical altitude, change critical altitude according to sectional dimension Compensation rate controls blanking speed.
2. the preparation method of quartzy ingot as claimed in claim 1, it is characterised in that when deposition quartzy ingot highly less than section During the change in size critical altitude of face, the blanking speed meets following relation:
V1=[1+k (r, h)] V2r2ρ
Wherein:V1For blanking speed, i.e., raw material injected volume in the unit interval;V2For using the rotary flat of quartz particles fusion sediment Platform fall off rate;R is target quartz ingot radius;ρ is quartz material density;K (r, h) is correction factor, itself and the stone in deposition English ingot height h dullness positive correlations, itself and the quartzy ingot radius dullness positive correlation in deposition.
3. the preparation method of quartzy ingot as claimed in claim 2, it is characterised in that correction factor k (r, h) span is 0.02~0.15.
4. the preparation method of quartzy ingot as claimed in claim 2, it is characterised in that the correction factor is true as follows It is fixed:
Determine radius r for given target quartz, the correction factor highly meets with ShiShimonoseki with the quartzy ingot in deposition System:
K (r, h)=α h+ η
Wherein, α and η is constant, and η is burn tinctuer.
5. the preparation method of quartzy ingot as claimed in claim 4, it is characterised in that the constant α calculates as follows:
α=a/ (1- η);
Wherein, a is negative value of the gravity pressure that quartzy ingot is subject to the slope of highly linear change curve or uniform blanking when institute State negative value of the quartzy ingot cross sectional radius with the slope of highly linear change curve;η is burn tinctuer.
6. the preparation method of quartzy ingot as claimed in claim 2, it is characterised in that in real time below measurement fusion sediment position Size, slope of the quartzy ingot cross sectional radius with highly linear change curve is calculated in real time, using the negative value of the slope as institute The adjustment amount of correction factor is stated, Real-time Feedback adjusts the correction factor.
7. a kind of preparation facilities of quartzy ingot, it is characterised in that controlled including rotation platform lifting motor, quartz raw material inventory Device and host computer;The rotation platform lifting motor is connected with the host computer signal;The host computer and the quartz are former Material injected volume controller signals are connected;
The host computer obtains the rotation platform lifting fall off rate that the rotation platform lifting motor provides, according to claim Preparation method described in 1 to 6, the quartz raw material is controlled to feed intake the blanking speed of amount controller.
8. preparation facilities as claimed in claim 7, it is characterised in that also including dimension measuring device, be arranged at the outer stove of burner hearth Thorax near exit, for detecting quartzy ingot hypomere size.
9. a kind of quartzy ingot is prepared with the control system that feeds intake, it is characterised in that including correction factor acquisition module, blanking velocity control Molding block, quartzy ingot height assay module and quartzy ingot hypomere sectional dimension assay module;
The quartzy ingot height assay module, for obtaining the quartzy ingot height in deposition, and submit to the correction factor and obtain Modulus block;
The quartzy ingot hypomere sectional dimension assay module, for obtaining in its hypomere sectional dimension of the quartzy ingot of deposition, and carry Give the correction factor acquisition module;
The correction factor acquisition module, according to the quartzy ingot height and hypomere sectional dimension, the correction factor is determined, And submit to the blanking velocity control module;
It is described descend rate control module, blanking velocity is calculated according to the correction factor and controls blanking.
10. quartzy ingot as claimed in claim 9 is prepared with the control system that feeds intake, it is characterised in that the quartz height is examined and determine Module is connected with the blanking velocity control module, and mould is controlled by the blanking velocity is highly submitted in the quartzy ingot of deposition Block;
The blanking control module judges whether to recalculate correction factor:
When the quartzy ingot is highly less than or equal to default sectional dimension change critical altitude, correction factor is recalculated; Otherwise correction factor is not recalculated.
CN201710747278.9A 2017-08-28 2017-08-28 Preparation method, device and system of quartz ingot Active CN107417074B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710747278.9A CN107417074B (en) 2017-08-28 2017-08-28 Preparation method, device and system of quartz ingot

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710747278.9A CN107417074B (en) 2017-08-28 2017-08-28 Preparation method, device and system of quartz ingot

Publications (2)

Publication Number Publication Date
CN107417074A true CN107417074A (en) 2017-12-01
CN107417074B CN107417074B (en) 2020-04-14

Family

ID=60434694

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710747278.9A Active CN107417074B (en) 2017-08-28 2017-08-28 Preparation method, device and system of quartz ingot

Country Status (1)

Country Link
CN (1) CN107417074B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109437551A (en) * 2018-12-12 2019-03-08 长飞光纤光缆股份有限公司 A method of high purity quartz material is prepared using tailing

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6203611B1 (en) * 1999-10-19 2001-03-20 Memc Electronic Materials, Inc. Method of controlling growth of a semiconductor crystal to automatically transition from taper growth to target diameter growth
CN202208676U (en) * 2011-09-13 2012-05-02 湖北菲利华石英玻璃股份有限公司 Feeding device for quartz glass ingot melting
CN103387330A (en) * 2013-07-30 2013-11-13 湖北菲利华石英玻璃股份有限公司 Quantitative starting method for producing quartz glass ingots
CN204874270U (en) * 2015-08-10 2015-12-16 湖北菲利华石英玻璃股份有限公司 A vertical deposition furnace for producing synthetic quartz glass spindle of jumbo size
CN206375814U (en) * 2017-01-18 2017-08-04 锦州新世纪石英玻璃有限公司 The post forming device of the quartzy ingot quality of lifting

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6203611B1 (en) * 1999-10-19 2001-03-20 Memc Electronic Materials, Inc. Method of controlling growth of a semiconductor crystal to automatically transition from taper growth to target diameter growth
CN202208676U (en) * 2011-09-13 2012-05-02 湖北菲利华石英玻璃股份有限公司 Feeding device for quartz glass ingot melting
CN103387330A (en) * 2013-07-30 2013-11-13 湖北菲利华石英玻璃股份有限公司 Quantitative starting method for producing quartz glass ingots
CN204874270U (en) * 2015-08-10 2015-12-16 湖北菲利华石英玻璃股份有限公司 A vertical deposition furnace for producing synthetic quartz glass spindle of jumbo size
CN206375814U (en) * 2017-01-18 2017-08-04 锦州新世纪石英玻璃有限公司 The post forming device of the quartzy ingot quality of lifting

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109437551A (en) * 2018-12-12 2019-03-08 长飞光纤光缆股份有限公司 A method of high purity quartz material is prepared using tailing

Also Published As

Publication number Publication date
CN107417074B (en) 2020-04-14

Similar Documents

Publication Publication Date Title
CN104220386B (en) Texture the accurate roller shaping of sheet material glass
CN100400446C (en) Method and apparatus for producing preformed glass part
CN105936584B (en) A kind of preparation method of quartz glass
CN202576197U (en) Control system for stabilizing quality of molten borosilicate glass
TWI519498B (en) A glass plate manufacturing method and a glass plate manufacturing apparatus
EP4137467A1 (en) System and method for improving uniformity of pcvd raw material vapor deposition, and use thereof
CN101538112B (en) Production method and production line of glass envelope of bathroom heater lamp
CN112624599A (en) Control device and control method for uniform density of multi-deposition blowtorch
CN107417074A (en) A kind of preparation method of quartzy ingot, apparatus and system
JP2007254247A (en) Glass molding production device and method for producing glass molding
CN105948468A (en) Quartz glass manufacturing device
CN102887624B (en) A kind of manufacture method of super large caliber quartz glass tube
TWI432385B (en) Method of manufacturing vitreous silica crucible
KR20040000689A (en) Raw material providing device for chemical vapor deposition process
CN102992582B (en) Sheet-glass tank furnace structure with independent clarifying part and adjusting method thereof
CN108467184A (en) The preparation method and device of a kind of high uniformly quartz glass of large scale
US20230148131A1 (en) Direct loading of glass gobs into traversable blank molds
CN206970461U (en) Multifunction quartz glass continuous induction melting furnace
TWI438158B (en) Method of manufacturing vitreous silica crucible
JP6452091B2 (en) Sintering method of porous glass preform for optical fiber
CN202953921U (en) Plate glass tank furnace structure with independent clarification part
CN111153590B (en) Germanium tetrachloride tympanic bulla device of high accuracy
CN112299702A (en) OVD deposition equipment and method for automatically adjusting deposition speed to match target weight
CN109437551B (en) Method for preparing high-purity quartz material by utilizing tailings
US4615720A (en) Method and apparatus for melting glass

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant