CN107417019A - A kind for the treatment of Technology for Petroleum Water Flooding - Google Patents

A kind for the treatment of Technology for Petroleum Water Flooding Download PDF

Info

Publication number
CN107417019A
CN107417019A CN201710821802.2A CN201710821802A CN107417019A CN 107417019 A CN107417019 A CN 107417019A CN 201710821802 A CN201710821802 A CN 201710821802A CN 107417019 A CN107417019 A CN 107417019A
Authority
CN
China
Prior art keywords
water
oil
tank
petroleum
oil field
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710821802.2A
Other languages
Chinese (zh)
Inventor
刘训东
程寒飞
刘昀
冯植飞
白扬
李启超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huatian Engineering and Technology Corp MCC
Original Assignee
Huatian Engineering and Technology Corp MCC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huatian Engineering and Technology Corp MCC filed Critical Huatian Engineering and Technology Corp MCC
Priority to CN201710821802.2A priority Critical patent/CN107417019A/en
Publication of CN107417019A publication Critical patent/CN107417019A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/048Breaking emulsions by changing the state of aggregation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/001Processes for the treatment of water whereby the filtration technique is of importance
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/30Treatment of water, waste water, or sewage by irradiation
    • C02F1/32Treatment of water, waste water, or sewage by irradiation with ultraviolet light
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/40Devices for separating or removing fatty or oily substances or similar floating material
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/54Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
    • C02F1/56Macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/10Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/04Disinfection

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)
  • Physical Water Treatments (AREA)

Abstract

The present invention discloses a kind for the treatment of Technology for Petroleum Water Flooding, oil field extracted water passes sequentially through regulation tank, aeration precipitation tank, oil water separator, tiny flocculation tank, high efficiency particulate air filter and ultraviolet sterilizer, and demulsifier and coagulant are added by pipe-line mixer before aeration precipitation tank, by pipe-line mixer dosing coagulant before tiny flocculation tank, the water outlet after processing reaches the requirement of oil field reinjection water water quality index.A kind for the treatment of Technology for Petroleum Water Flooding of the present invention solves the problems, such as that existing treatment Technology for Petroleum Water Flooding is difficult to oil field produced water process reaching oil field reinjection water standard, has the characteristics of dosing is few, sludge yield is small, energy consumption is low, treatment effect stability and high efficiency.

Description

A kind for the treatment of Technology for Petroleum Water Flooding
Technical field
The present invention relates to field of waste water treatment, more particularly to a kind for the treatment of Technology for Petroleum Water Flooding.
Background technology
With the continuous exploitation in oil field, the continuous development of oil recovery technique, oil field successively experienced once, is secondary, adopting three times Oil.Primary oil recovery is power by natural energy;Secondary oil recovery keeps strata pressure in a manner of artificial recharge;Tertiary oil recovery is logical Cross and change the characteristic for injecting water to improve tar productivity, oil field is substantially carried out secondary, tertiary oil recovery at present.From the aqueous of underground extraction Crude oil claims " Produced Liquid ", and the water separated by dehydration is referred to as " oil field extracted water ", also referred to as " oilfield sewage ".China is most of Oil field comes into the middle and later periods of exploitation, and moisture content is generally 90% or so even up to 95%, therefore, at recovered water After reason recharge to underground be oil field production indispensable program.
The leading indicator handled oil field extracted water is oil content and suspension.It is thousands of that reinjected water will inject underground Rice, if water quality unclean (suspension is not up to standard or particle diameter of particle is exceeded) can cause to block the tiny gap in rock stratum quickly, Make it difficult to the depth for reaching setting, it has been found that a part of oil field region reinjected water is difficult to recharge, even if using higher than general pressure Power is also difficult to re-injection, causes rock stratum to block here it is reinjected water water quality before this is unqualified, for this by abandoned well.Cause This, oil field wishes to improve re-injection water quality, generally improves a standard class, to meet that oil field extends wanting for well recovery cycle Ask.
The content of the invention
The problem of not reaching the requirement of oil field reinjection water water quality index for existing treatment Technology for Petroleum Water Flooding, the present invention carries For a kind for the treatment of Technology for Petroleum Water Flooding that can effectively improve oil field reinjection water water quality.
The concrete technical scheme of the present invention is as follows:
A kind for the treatment of Technology for Petroleum Water Flooding, oil field extracted water pass sequentially through regulation tank, aeration precipitation tank, water-oil separating Device, tiny flocculation tank, high efficiency particulate air filter and ultraviolet sterilizer, the water outlet after processing reach the requirement of oil field reinjection water water quality index, The technique comprises the following steps that:
1) oil field extracted water initially enters regulation tank, and the water quality, water to raw water are adjusted;
2) regulation tank water outlet adds demulsifier, coagulant by pipe-line mixer, is demulsified, tiny flocculation reaction;
3) sewage after pipe-line mixer enters aeration precipitation tank, the pollutant such as oily substance and surfactant with Bubble floating band water-outlet body, suspended solid are then deposited on aeration precipitation tank bottom under the effect of catching etc. of gravity, Electrostatic Absorption and net, Realize oily sludge thing and suspended solid while separate and remove;
4) sewage after aeration precipitation tank is handled enters oil water separator, further removal step 3) in do not remove Oil emulsion;
5) sewage after oil water separator is handled is by pipe-line mixer dosing coagulant, subsequently into tiny flocculation tank;
6) sewage after the processing of tiny flocculation tank enters high efficiency particulate air filter, oil emulsion, the SS further efficiently gone in water removal Deng pollutant;
7) sewage after high efficiency particulate air filter is handled flows through ultraviolet sterilizer, kills sulfate reducing bacteria in sewage, corruption Raw bacterium and iron bacteria etc..
Further, described coagulant is using aluminum sulfate, aluminium polychloride, ferric trichloride, bodied ferric sulfate, polypropylene One or more in acid amides etc.;Demulsifier is using in cationic, anionic, nonionic, amphitypy ionic demulsifying agent One or more.
Further, in described aeration precipitation tank, aeration precipitation tank bottom even is provided with aeration head, is set at middle part There is dissolved air water release head.
Further, the filter medium made of high polymer material is used in described oil water separator.
Further, the filtrate in described high efficiency particulate air filter include micropore ceramics filtrate, quartz sand, gravel, anthracite, Manganese sand, magnetic iron ore filtrate, shell filtrate, porcelain sand filter material, haydite, garnet filtrate, medical stone filtrate, active oxidation aluminium ball and boiling One or more in stone filtrate.
Compared with prior art, the advantage of the invention is that:Present invention process solves existing oil field produced water process The problem of technique is difficult to oil field produced water process reaching oil field reinjection water standard, with dosing is few, sludge yield is small, energy The characteristics of consuming low, treatment effect stability and high efficiency.
Brief description of the drawings
Fig. 1 is a kind of schematic flow sheet for the treatment of Technology for Petroleum Water Flooding of the present invention.
Embodiment
With reference to Figure of description, present invention process is further described through.
A kind for the treatment of Technology for Petroleum Water Flooding include regulation tank, aeration precipitation tank, oil water separator, tiny flocculation tank, efficiently Filter and ultraviolet sterilizer etc.;Demulsifier and coagulant are added by pipe-line mixer before aeration precipitation tank;Before tiny flocculation tank Pass through pipe-line mixer dosing coagulant.
Coagulant is using one kind in aluminum sulfate, aluminium polychloride, ferric trichloride, bodied ferric sulfate, polyacrylamide etc. It is or several;Demulsifier is using the one or more in cationic, anionic, nonionic, amphitypy ionic demulsifying agent.
Filtrate in high efficiency particulate air filter includes micropore ceramics filtrate, quartz sand, gravel, anthracite, manganese sand, magnetic iron ore filter One in material, shell filtrate, porcelain sand filter material, haydite, garnet filtrate, medical stone filtrate, active oxidation aluminium ball and zeolite filler Kind is several.
Embodiment 1
With reference to accompanying drawing 1, take oil content less than 3000mg/L, polymer content less than 1000mg/L, surface-active contents Handled less than the ternary compound oil drive oil field extracted water of 500mg/L, alkali content less than 1500mg/L.
Oil field extracted water initially enters regulation tank, and the water quality, water to raw water are adjusted, and reduce because of raw water quality, water Influence of the change of amount to subsequent technique, ensures the stable operation of subsequent technique;
Regulation tank water outlet adds demulsifier (acrylic compounds reverse-phase emulsifier BH-10) 10~30mg/ by pipe-line mixer L, coagulant (aluminium polychloride) 30~60mg/L, it is demulsified, tiny flocculation reaction;
Sewage after pipe-line mixer enters aeration precipitation tank, and aeration precipitation tank bottom even is provided with aeration head, Dissolved air water release head is provided with middle part.A large amount of bubbles and the release of middle part dissolved air water release head using the release of bottom aeration head Microbubble, will be by pollutants such as demulsification, the oily substance in the reacted oil field extracted water of tiny flocculation and surfactants Removed with bubble floating band water-outlet body, suspended solid is then deposited on exposure under the effect of catching etc. of gravity, Electrostatic Absorption and net Gas settles pot bottom, realizes to oil-containing and suspended solid while separates the effect removed;Aeration time is 6-10h, and gas-water ratio is 10:1~20:1 (aeration head and dissolved air water release head allocation proportion are 1:1~2:1).
Sewage after aeration precipitation tank is handled enters oil water separator, is used in oil water separator by high polymer material Manufactured filter medium realizes water-oil separating, further removes the oil emulsion not removed in aeration precipitation tank technique;
Sewage after oil water separator is handled, subsequently into tiny flocculation tank, is mixed by pipe-line mixer dosing coagulant Solidifying agent uses aluminium polychloride, 30~60mg/L of dosage;
Sewage after the processing of tiny flocculation tank enters high efficiency particulate air filter, and the filtrate in high efficiency particulate air filter is using micropore ceramics filter The pollutant such as material, the oil emulsion further efficiently gone in water removal, SS;
Sewage after high efficiency particulate air filter is handled flows through ultraviolet sterilizer, kill sulfate reducing bacteria (SRB) in sewage, Saprophytic bacteria (TGB) and iron bacteria (FB) etc..20~40s of ultraviolet irradiation time, effective 15~30mj/cm of uv dosage2
After ultraviolet sterilizer is handled, water outlet reaches《Clastic rock reservoir water water quality fertilizer index and analysis method》 Oil content≤15.0mg/L, suspended solids content≤5.0mg/L, suspended particle median diameter in (SY/T 5329-2012)≤ 3.0um Con trolling index.
More than, only presently preferred embodiments of the present invention, but protection scope of the present invention is not limited thereto is any to be familiar with sheet Those skilled in the art the invention discloses technical scope in, the change or replacement that can readily occur in should all be covered Within protection scope of the present invention.Therefore, protection scope of the present invention should be defined by the protection domain that claim is defined.

Claims (5)

1. a kind for the treatment of Technology for Petroleum Water Flooding, oil field extracted water pass sequentially through regulation tank, aeration precipitation tank, oil water separator, Tiny flocculation tank, high efficiency particulate air filter and ultraviolet sterilizer, the water outlet after processing reach the requirement of oil field reinjection water water quality index, and it is special Sign is that the technique comprises the following steps that:
1) oil field extracted water initially enters regulation tank, and the water quality, water to raw water are adjusted;
2) regulation tank water outlet adds demulsifier, coagulant by pipe-line mixer, is demulsified, tiny flocculation reaction;
3) sewage after pipe-line mixer enters aeration precipitation tank, and the pollutant such as oily substance and surfactant is with bubble Float band water-outlet body, and suspended solid is then deposited on aeration precipitation tank bottom under the effect of catching etc. of gravity, Electrostatic Absorption and net, realizes Oily sludge thing and suspended solid separate simultaneously to be removed;
4) sewage after aeration precipitation tank is handled enters oil water separator, further removal step 3) in the emulsification that does not remove Oil;
5) sewage after oil water separator is handled is by pipe-line mixer dosing coagulant, subsequently into tiny flocculation tank;
6) sewage after the processing of tiny flocculation tank enters high efficiency particulate air filter, the oil emulsion that further efficiently goes in removing water, the dirt such as SS Contaminate thing;
7) sewage after high efficiency particulate air filter is handled flows through ultraviolet sterilizer, kills sulfate reducing bacteria in sewage, saprophytic bacteria With iron bacteria etc..
A kind of 2. treatment Technology for Petroleum Water Flooding according to claim 1, it is characterised in that:Described coagulant uses sulphur One or more in sour aluminium, aluminium polychloride, ferric trichloride, bodied ferric sulfate, polyacrylamide etc.;Demulsifier using sun from One or more in subtype, anionic, nonionic, amphitypy ionic demulsifying agent.
A kind of 3. treatment Technology for Petroleum Water Flooding according to claim 1, it is characterised in that:Described aeration precipitation tank In, aeration precipitation tank bottom even is provided with aeration head, and dissolved air water release head is provided with middle part.
A kind of 4. treatment Technology for Petroleum Water Flooding according to claim 1, it is characterised in that:In described oil water separator Using the filter medium made of high polymer material.
A kind of 5. treatment Technology for Petroleum Water Flooding according to claim 1, it is characterised in that:In described high efficiency particulate air filter Filtrate include micropore ceramics filtrate, quartz sand, gravel, anthracite, manganese sand, magnetic iron ore filtrate, shell filtrate, porcelain sand filter material, One or more in haydite, garnet filtrate, medical stone filtrate, active oxidation aluminium ball and zeolite filler.
CN201710821802.2A 2017-09-13 2017-09-13 A kind for the treatment of Technology for Petroleum Water Flooding Pending CN107417019A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710821802.2A CN107417019A (en) 2017-09-13 2017-09-13 A kind for the treatment of Technology for Petroleum Water Flooding

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710821802.2A CN107417019A (en) 2017-09-13 2017-09-13 A kind for the treatment of Technology for Petroleum Water Flooding

Publications (1)

Publication Number Publication Date
CN107417019A true CN107417019A (en) 2017-12-01

Family

ID=60433469

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710821802.2A Pending CN107417019A (en) 2017-09-13 2017-09-13 A kind for the treatment of Technology for Petroleum Water Flooding

Country Status (1)

Country Link
CN (1) CN107417019A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108314231A (en) * 2018-01-29 2018-07-24 北京桑德环境工程有限公司 A kind of industrial park advanced treatment of wastewater and the system and method for reuse
CN112811667A (en) * 2021-01-21 2021-05-18 上海蓝科石化环保科技股份有限公司 Sequence type oil removing system and method
EP3753907A4 (en) * 2018-02-13 2021-10-20 Graduate School at Shenzhen, Tsinghua University Injected water treatment method, injected water treatment device and application thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5330650A (en) * 1992-10-30 1994-07-19 Nalco Chemical Company Dispersion polymers for oil field water clarification
CN101066818A (en) * 2007-06-04 2007-11-07 万奥普(北京)石油工程技术开发研究院有限公司 Process of treating oil-bearing sewage for ternary combination flooding in oil field
CN101172726A (en) * 2007-11-08 2008-05-07 长庆石油勘探局 Method and technological process for treating sewage of oil recovery
CN201288079Y (en) * 2008-11-12 2009-08-12 大庆油田有限责任公司 Aeration precipitation tank
CN106542677A (en) * 2017-02-14 2017-03-29 中冶华天南京工程技术有限公司 A kind of ternary composite driving oil field produced water treatment technique
CN106977027A (en) * 2017-03-16 2017-07-25 中国石油天然气股份有限公司 Deep treatment system and method for oilfield produced sewage

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5330650A (en) * 1992-10-30 1994-07-19 Nalco Chemical Company Dispersion polymers for oil field water clarification
CN101066818A (en) * 2007-06-04 2007-11-07 万奥普(北京)石油工程技术开发研究院有限公司 Process of treating oil-bearing sewage for ternary combination flooding in oil field
CN101172726A (en) * 2007-11-08 2008-05-07 长庆石油勘探局 Method and technological process for treating sewage of oil recovery
CN201288079Y (en) * 2008-11-12 2009-08-12 大庆油田有限责任公司 Aeration precipitation tank
CN106542677A (en) * 2017-02-14 2017-03-29 中冶华天南京工程技术有限公司 A kind of ternary composite driving oil field produced water treatment technique
CN106977027A (en) * 2017-03-16 2017-07-25 中国石油天然气股份有限公司 Deep treatment system and method for oilfield produced sewage

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
上海建筑设计研究院等: "《给排水设计手册.材料设备(续册3)》", 30 April 1999 *
全国勘察设计注册工程师环保专业管理委员会等: "《注册环保工程师专业考试复习教材》", 31 May 2007 *
陈观文等: "《分离膜应用与工程实例》", 30 November 2007 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108314231A (en) * 2018-01-29 2018-07-24 北京桑德环境工程有限公司 A kind of industrial park advanced treatment of wastewater and the system and method for reuse
EP3753907A4 (en) * 2018-02-13 2021-10-20 Graduate School at Shenzhen, Tsinghua University Injected water treatment method, injected water treatment device and application thereof
CN112811667A (en) * 2021-01-21 2021-05-18 上海蓝科石化环保科技股份有限公司 Sequence type oil removing system and method
CN112811667B (en) * 2021-01-21 2023-07-04 上海蓝科石化环保科技股份有限公司 Sequential oil removing system and method

Similar Documents

Publication Publication Date Title
CN106660836A (en) Electrochemical treatment methods
CN205127549U (en) Industrial wastewater treatment device
CN107417019A (en) A kind for the treatment of Technology for Petroleum Water Flooding
CN105236682B (en) Processing method and processing device containing oil-polluted water
CN110255792A (en) A kind of extra permeability oilfield recovered water stably reaching standard processing system and its treatment process
CN106430737A (en) Low-permeability oilfield reinjection water treatment method
CN104787923B (en) Oilfield sewage movable skid-mounted formula processing method
CN104016520A (en) Device for pre-treating coal chemical industry wastewater by air flotation coupled with coagulation and method for pre-treating coal chemical industry wastewater by device
CN102583816B (en) Method for reusing and treating oily wastewater by adopting nitrogen gas floatation technology
CN103102926B (en) A kind of crude oil electric desalting and Electric Desalting Wastewater treatment process
CN102718285B (en) Oily sewage physical demulsification method for oil field
CN204151169U (en) A kind of fracturing outlet liquid recycling and processing equipment
CN108033601A (en) The method of operation wastewater in oil field processing
CN205275333U (en) Oil field extraction water composite treatment system
CN102040310A (en) Sewage treatment method for reinjection of produced water from oil field to low-permeability oil field
CN107365008A (en) Vehicle-mounted fracturing return-discharge waste liquid treatment system
CN103523982A (en) Electric coagulation oil-water settling separator
CN207581543U (en) A kind of bearing sewage for ternary combination flooding in oil processing unit
CN204022596U (en) A kind of oil-gas field fracturing waste liquor effective, harmless treatment unit
CN104649355A (en) Air flotation-magnetic separation treatment system of oil-containing wastewater
CN105621723A (en) Petroleum sewage treatment method
CN104211231A (en) Method for treating waste liquid of oil field measures
CN209554943U (en) A kind of integrated purifying processing unit for oil extraction waste water
CN104310643A (en) Combined device for oily sewage treatment
CN105254054B (en) A kind of oil field extracted water multiple treating system and method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20171201