CN107414090A - A kind of non-crystaline amorphous metal powder preparation facilities - Google Patents

A kind of non-crystaline amorphous metal powder preparation facilities Download PDF

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Publication number
CN107414090A
CN107414090A CN201710558368.3A CN201710558368A CN107414090A CN 107414090 A CN107414090 A CN 107414090A CN 201710558368 A CN201710558368 A CN 201710558368A CN 107414090 A CN107414090 A CN 107414090A
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CN
China
Prior art keywords
storehouse
separation bin
neck
amorphous metal
atomized
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Withdrawn
Application number
CN201710558368.3A
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Chinese (zh)
Inventor
张真真
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Individual
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Individual
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Priority to CN201710558368.3A priority Critical patent/CN107414090A/en
Publication of CN107414090A publication Critical patent/CN107414090A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/002Making metallic powder or suspensions thereof amorphous or microcrystalline
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/086Cooling after atomisation
    • B22F2009/0864Cooling after atomisation by oil, other non-aqueous fluid or fluid-bed cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0896Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid particle transport, separation: process and apparatus

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  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention discloses a kind of non-crystaline amorphous metal powder preparation facilities,Including being atomized storehouse,The top in the atomization storehouse is provided with feed pipe,The side in atomization storehouse connects with the right side of feed tube,The liquid feeding end of feed tube is provided with liquid pump,The inside top in atomization storehouse is provided with high pressure nozzle,The top of high pressure nozzle and the bottom of feed pipe connect,The side wall of high pressure nozzle is provided with spray orifice,The inner side for being atomized storehouse is provided with cooling bucket,The side wall of cooling bucket is provided with through hole,The bottom in atomization storehouse is provided with separation bin,The bottom in storehouse and the top of separation bin is atomized to penetrate,The side of separation bin and the inlet end of escape pipe connect,The outlet side of escape pipe is provided with air pump,The inside of separation bin is provided with filter screen flexible pipe,The bottom of filter screen flexible pipe is connected with fixing groove,The present invention,The amorphous powdered alloy impurity of preparation is few,The powder sphericity of preparation is high,Carry screening function,Reject the powder particle for not meeting size,The material produced can be used directly in next process.

Description

A kind of non-crystaline amorphous metal powder preparation facilities
Technical field
The present invention relates to non-crystaline amorphous metal preparing technical field, specially a kind of non-crystaline amorphous metal powder preparation facilities.
Background technology
With the development of science and technology, increasing production material occurs, the thing followed also have various processings these The machinery of material, current manufacturing industry have a kind of material more popular, are exactly amorphous powder, and amorphous powder uses gas in the prior art Prepared by atomization method, bulk amorphous alloy manufacturing process mainly has the non-crystaline amorphous metals such as water quenching, copper mold casting method, casting die Prepared by material influenceed by cooling medium heat conduction velocity and itself glassy state Forming ability, and aqueous vapor is used in aerosolization preparation Be cooled to it is common, but aqueous vapor atomization cooling treatment be only suitable for respective material use, make the non-crystaline amorphous metal powder oxygen made Too high levels, impurity increase etc., result in the unavailable of material, it is impossible to comprehensive cooling, make the sphericity of powder poor, cause Production and application is influenceed, manufactured material can not separate with cooling article, cause manufactured material not use directly, finished-product material It can not screen, it is impossible to ensure the unified specification of product.
The content of the invention
The technical problem to be solved in the present invention is to overcome the defects of existing, there is provided a kind of non-crystaline amorphous metal powder preparation facilities, The amorphous powdered alloy impurity of preparation is few, and the powder sphericity of preparation is high, carries screening function, rejects the powder for not meeting size Particle, the material produced can be used directly in next process.
To achieve the above object, the present invention provides following technical scheme:A kind of non-crystaline amorphous metal powder preparation facilities, including mist Change storehouse, the top in the atomization storehouse is provided with feed pipe, is atomized the side in storehouse and is connected with the right side of feed tube, the liquid feeding end of feed tube Provided with liquid pump, the inside top for being atomized storehouse is provided with high pressure nozzle, and the top of high pressure nozzle and the bottom of feed pipe connect, high pressure spray The side wall of mouth is provided with spray orifice, and the inner side for being atomized storehouse is provided with cooling bucket, and the side wall for cooling down bucket is provided with through hole, and the bottom for being atomized storehouse is provided with Separation bin, it is atomized the bottom in storehouse and the top of separation bin and penetrates, the side of separation bin and the inlet end of escape pipe connect, escape pipe Outlet side be provided with air pump, the inside of separation bin is provided with filter screen flexible pipe, and the bottom of separation bin is provided with fixing groove, the top of filter screen flexible pipe Portion is connected with cooling bucket, and the bottom of filter screen flexible pipe is connected with fixing groove, and the bottom of separation bin is provided with screening storehouse, screens the side in storehouse Provided with neck one, the opposite side for screening storehouse is provided with neck two, sieve plate is connected between neck one and neck two, sieve plate is close to neck Two one end is provided with groove, and the side of sieve plate and the telescopic end of electric expansion bar connect, and the fixing end of electric expansion bar is through sieve Select the front portion in storehouse and extend to outside and be connected with screening the fixed plate that the outside in storehouse is provided with, the bottom of sieve plate is close to the side of groove Provided with riser, riser is provided with swash plate one close to the side of groove, and the bottom of swash plate one is connected with through screening storehouse side and extended To the reject chute of outside, the one end of riser away from groove is provided with swash plate two, and the bottom of swash plate two is connected with through screening storehouse and prolonged The blow tank of outside is extended, the output end of air pump is connected with extraneous air purifying processor, and input and the liquid nitrogen bottle of liquid pump connect Connect, the input of liquid pump, air pump and electric expansion bar electrically connects with the output end of external power switch.
As a preferred technical solution of the present invention, the spray orifice is no less than four, and the spray orifice no less than four is with ring The mode of shape array is evenly distributed in the side of high pressure nozzle, and through hole is three groups every group six, three groups of through holes no less than six It is evenly distributed with array way.
As a preferred technical solution of the present invention, the neck one is higher than neck two, and sieve plate is to be obliquely installed.
As a preferred technical solution of the present invention, the aperture of filter screen flexible pipe side is less than the diameter of making material.
As a preferred technical solution of the present invention, it is atomized between storehouse and cooling bucket and is full of liquid nitrogen.
Compared with prior art, the beneficial effects of the invention are as follows:This non-crystaline amorphous metal powder preparation facilities, the amorphous of preparation close Bronze end impurity is few, and the powder sphericity of preparation is high, carries screening function, rejects the powder particle for not meeting size, produces Material can directly next process use.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention;
Fig. 2 cross-sectional views of the present invention.
In figure:1 atomization storehouse, 2 feed pipes, 3 feed tubes, 4 liquid pumps, 5 high pressure nozzles, 6 spray orifices, 7 cooling buckets, 8 through holes, 9 points From storehouse, 10 escape pipes, 11 air pumps, 12 filter screen flexible pipes, 13 fixing grooves, 14 screening storehouses, 15 necks one, 16 necks two, 17 sieve plates, 18 Groove, 19 electric expansion bars, 20 fixed plates, 21 risers, 22 swash plates one, 23 reject chutes, 24 swash plates two, 25 blow tanks.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made Embodiment, belong to the scope of protection of the invention.
Fig. 1-2 is referred to, the present invention provides a kind of technical scheme:A kind of non-crystaline amorphous metal powder preparation facilities, including atomization Storehouse 1, the top in atomization storehouse 1 are provided with feed pipe 2, and the side in atomization storehouse 1 connects with the right side of feed tube 3, the liquid feeding end of feed tube 3 Provided with liquid pump 4, the inside top in atomization storehouse 1 is provided with high pressure nozzle 5, and the top of high pressure nozzle 5 is connected with the bottom of feed pipe 2, The side wall of high pressure nozzle 5 is provided with spray orifice 6, and spray orifice 6 is no less than four, and the spray orifice 6 no less than four is put down in a manner of annular array The side of high pressure nozzle 5 is distributed in, the inner side in atomization storehouse 1 is provided with cooling bucket 7, is atomized between storehouse 1 and cooling bucket 7 and is full of liquid Nitrogen, the side wall of cooling bucket 7 are provided with through hole 8, and through hole 8 is three groups every group six, and three groups of through holes 8 no less than six are with array way It is evenly distributed, the bottom in atomization storehouse 1 is provided with separation bin 9, is atomized the bottom in storehouse 1 and is penetrated with the top of separation bin 9, separation bin 9 Side is connected with the inlet end of escape pipe 10, and the outlet side of escape pipe 10 is provided with air pump 11, and the inside of separation bin 9 is soft provided with filter screen Pipe 12, the aperture of the side of filter screen flexible pipe 12 are less than the diameter of making material, and the bottom of separation bin 9 is provided with fixing groove 13, and filter screen is soft The top of pipe 12 is connected with cooling bucket 7, and the bottom of filter screen flexible pipe 12 is connected with fixing groove 13, and the bottom of separation bin 9 is provided with screening Storehouse 14, the side in screening storehouse 14 are provided with neck 1, and the opposite side in screening storehouse 14 is provided with neck 2 16, neck 1 and neck two Sieve plate 17 is connected between 16, neck 1 is higher than neck 2 16, and sieve plate 17 is is obliquely installed, and sieve plate 17 is close to neck 2 16 One end is provided with groove 18, and the side of sieve plate 17 is connected with the telescopic end of electric expansion bar 19, and the fixing end of electric expansion bar 19 is passed through Wear the front side in screening storehouse 14 and extend to outside and be connected with screening the fixed plate 20 that the front side in storehouse 14 is provided with, the bottom of sieve plate 17 is leaned on The side of nearly groove 18 is provided with riser 21, and riser 21 is provided with swash plate 1 close to the side of groove 18, and the bottom of swash plate 1 connects It is connected to through the screening side of storehouse 14 and extends to the reject chute 23 of outside, the one end of riser 21 away from groove 18 is provided with swash plate two 24, the bottom of swash plate 2 24 is connected with through screening storehouse 14 and extends to the blow tank 25 of outside.The output end of air pump 11 with it is outer The connection of portion purification of air processor, the input of liquid pump 4 are connected with liquid nitrogen bottle, liquid pump 4, air pump 11 and electric expansion bar 19 it is defeated Enter end to electrically connect with the output end of external power switch, external power switch control liquid pump 4, air pump 11 and electric expansion bar 19 are equal Using method commonly used in the prior art.
When in use:External power switch is opened, the material heated enters equipment from feed pipe 2, and material passes through high pressure Nozzle 5 sprays the material of spray pattern from spray orifice 6, and the liquid nitrogen that liquid pump 4 is extracted in liquid nitrogen bottle enters in atomization storehouse 1 by feed tube Cavity at, the material coolant that liquid nitrogen enters cooling bucket 7 and spray pattern by through hole 8 forms non-crystaline amorphous metal powder Dirt, non-crystaline amorphous metal dust together enter in filter screen flexible pipe 12 with nitrogen, and nitrogen retains from filter screen through non-crystaline amorphous metal dust, gas Pump startup, extract the nitrogen filtered out in separation bin 9 out by escape pipe and discharge, non-crystaline amorphous metal dust conveys by filter screen flexible pipe 12 To screening storehouse 14, sieve plate 17 is fallen into, electric expansion bar 19 is rocked before and after starting drive sieve plate, the non-crystaline amorphous metal for the size that meets the requirements Dust falls on the surface of swash plate 2 24 by sieve aperture, is discharged by blow tank 25, and the dust to fall short of specifications rolls to lead to through sieve plate 17 Groove 18, non-crystaline amorphous metal dust falls by groove 18 discharges on the surface of swash plate 1 from reject chute 23.
The present invention, make the amorphous powdered alloy impurity of preparation few using liquid nitrogen cooling technology, the rapid powder for making preparation of refrigeration Last sphericity is high, carries screening function, rejects the powder particle for not meeting size, the material produced can be directly in lower one of work Sequence uses.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (5)

1. a kind of non-crystaline amorphous metal powder preparation facilities, including atomization storehouse(1), it is characterised in that:The atomization storehouse(1)Top set There is feed pipe(2), it is atomized storehouse(1)Side and feed tube(3)Right side connection, feed tube(3)Liquid feeding end be provided with liquid pump (4), it is atomized storehouse(1)Inside top be provided with high pressure nozzle(5), high pressure nozzle(5)Top and feed pipe(2)Bottom connect Connect, high pressure nozzle(5)Side wall be provided with spray orifice(6), it is atomized storehouse(1)Inner side be provided with cooling bucket(7), cool down bucket(7)Side wall Provided with through hole(8), it is atomized storehouse(1)Bottom be provided with separation bin(9), it is atomized storehouse(1)Bottom and separation bin(9)Top pass through It is logical, separation bin(9)Side and escape pipe(10)Inlet end connection, escape pipe(10)Outlet side be provided with air pump(11), point From storehouse(9)Inside be provided with filter screen flexible pipe(12), separation bin(9)Bottom be provided with fixing groove(13), filter screen flexible pipe(12)Top Portion and cooling bucket(7)Connection, filter screen flexible pipe(12)Bottom and fixing groove(13)Connection, separation bin(9)Bottom be provided with screening Storehouse(14), screen storehouse(14)Side be provided with neck one(15), screen storehouse(14)Opposite side be provided with neck two(16), neck one (15)With neck two(16)Between be connected with sieve plate(17), sieve plate(17)Close to neck two(16)One end be provided with groove(18), Sieve plate(17)Side and electric expansion bar(19)Telescopic end connection, electric expansion bar(19)Fixing end through screening storehouse (14)Front portion and extend to outside with screening storehouse(14)The fixed plate that is provided with of outside(20)Connection, sieve plate(17)Bottom lean on Nearly groove(18)Side be provided with riser(21), riser(21)Close to groove(18)Side be provided with swash plate one(22), swash plate one (22)Bottom be connected with through screening storehouse(14)Side and the reject chute for extending to outside(23), riser(21)Away from groove (18)One end be provided with swash plate two(24), swash plate two(24)Bottom be connected with through screening storehouse(14)And extend to going out for outside Hopper(25), liquid pump(4), air pump(11)And electric expansion bar(19)Input and the output end of external power switch be electrically connected Connect, air pump(11)Output end be connected with extraneous air purifying processor, liquid pump(4)Input be connected with liquid nitrogen bottle.
A kind of 2. non-crystaline amorphous metal powder preparation facilities according to claim 1, it is characterised in that:The spray orifice(6)Much In four, the spray orifice no less than four(6)High pressure nozzle is evenly distributed in a manner of annular array(5)Side, through hole(8) For three groups every group six, three groups of through holes no less than six(8)It is evenly distributed with array way.
A kind of 3. non-crystaline amorphous metal powder preparation facilities according to claim 1, it is characterised in that:The neck one(15)It is high In neck two(16), sieve plate(17)To be obliquely installed.
A kind of 4. non-crystaline amorphous metal powder preparation facilities according to claim 1, it is characterised in that:The atomization storehouse(1)With Cool down bucket(7)Between be full of liquid nitrogen.
A kind of 5. non-crystaline amorphous metal powder preparation facilities according to claim 1, it is characterised in that:The filter screen flexible pipe(12) The aperture of side is less than the diameter of making material.
CN201710558368.3A 2017-07-10 2017-07-10 A kind of non-crystaline amorphous metal powder preparation facilities Withdrawn CN107414090A (en)

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CN201710558368.3A CN107414090A (en) 2017-07-10 2017-07-10 A kind of non-crystaline amorphous metal powder preparation facilities

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5488813A (en) * 1977-12-26 1979-07-14 Kobe Steel Ltd Preparation of sinterde body by powder metallurgy
CN102925824A (en) * 2012-11-23 2013-02-13 北京科技大学 Preparation method for zirconium-based amorphous alloy as well as powder and large-sized block of zirconium-based amorphous alloy
CN103962564A (en) * 2014-04-18 2014-08-06 浙江旭德新材料有限公司 Method for preparing spherical bronze alloy powder
CN106191517A (en) * 2016-08-10 2016-12-07 浙江旭德新材料有限公司 A kind of preparation method of the copper and tin Ni-Bi alloy powder for producing bi-metal shaft bushing material
CN206104890U (en) * 2016-09-14 2017-04-19 武汉拓材科技有限公司 Atomizing and pulverizing system of superfine indium powder prepares

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5488813A (en) * 1977-12-26 1979-07-14 Kobe Steel Ltd Preparation of sinterde body by powder metallurgy
CN102925824A (en) * 2012-11-23 2013-02-13 北京科技大学 Preparation method for zirconium-based amorphous alloy as well as powder and large-sized block of zirconium-based amorphous alloy
CN103962564A (en) * 2014-04-18 2014-08-06 浙江旭德新材料有限公司 Method for preparing spherical bronze alloy powder
CN106191517A (en) * 2016-08-10 2016-12-07 浙江旭德新材料有限公司 A kind of preparation method of the copper and tin Ni-Bi alloy powder for producing bi-metal shaft bushing material
CN206104890U (en) * 2016-09-14 2017-04-19 武汉拓材科技有限公司 Atomizing and pulverizing system of superfine indium powder prepares

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Application publication date: 20171201