CN107413292A - A kind of double-layer glass reaction kettle - Google Patents
A kind of double-layer glass reaction kettle Download PDFInfo
- Publication number
- CN107413292A CN107413292A CN201710832621.XA CN201710832621A CN107413292A CN 107413292 A CN107413292 A CN 107413292A CN 201710832621 A CN201710832621 A CN 201710832621A CN 107413292 A CN107413292 A CN 107413292A
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- China
- Prior art keywords
- reactor
- layer glass
- double
- reaction kettle
- glass
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00085—Plates; Jackets; Cylinders
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00162—Controlling or regulating processes controlling the pressure
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00189—Controlling or regulating processes controlling the stirring velocity
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0254—Glass
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention relates to reactor R ＆ D design technical field, more particularly to a kind of double-layer glass reaction kettle, the present invention to adopt the following technical scheme that：A kind of double-layer glass reaction kettle, including inner layer glass reactor, glass outer reactor, motor, agitator, kettle cover, constant pressure funnel, condenser and Backflow bottle, a liftable support is provided with above base, it is glass outer reactor above liftable support, inner layer glass reactor jacket is in glass outer reactor, 4 holes are provided with kettle cover, respectively constant pressure funnel interface, agitator pass through hole, condenser interface and charging aperture, a controller is provided with behind liftable support, the advantage of the invention is that：By adding circulation fluid in interlayer, temperature adjustment is carried out to reaction, and realizes distillation, the function of backflow, inner layer glass reactor bottom is funnel-shaped design, is sufficiently mixed medicine in kettle, and kettle can realize hand-operated lifting by adjusting base lifting support.
Description
Technical field：
The present invention relates to reactor R ＆ D design technical field, more particularly to a kind of double-layer glass reaction kettle.
Background technology：
Traditional single-glass reactor in the lower section of reactor, it is necessary to set a heater, kettle is irremovable knot
Structure, all cause certain puzzlement with cleaning for feeding intake, it is therefore desirable to further to improve research and development.
The content of the invention：
It is an object of the invention to provide a kind of glass reaction kettle, in particular, in that providing a kind of double-layer glass reaction kettle.
To reach above-mentioned purpose, the present invention adopts the following technical scheme that：A kind of double-layer glass reaction kettle, including inner layer glass
Reactor, glass outer reactor, motor, agitator, kettle cover, constant pressure funnel, condenser, one is provided with above base can
Lifting support, liftable support top are glass outer reactors, and inner layer glass reactor jacket is mounted in glass outer reactor,
4 holes are provided with kettle cover, respectively constant pressure funnel interface, agitator passes through hole, condenser interface and charging aperture, liftable branch
A controller is provided with behind frame.
Further, described inner layer glass reactor bottom is in funnel-form, and outside drain hole is fixed with flange plate structure
Outside outer layer glass reactor.
Further, described motor is connected with agitator, through the flange hole among kettle cover, extends to internal layer container
It is interior.
Further, described agitator is made up of agitating shaft and double-deck paddle.
Further, described agitating shaft internal layer is stainless steel, and outer layer has one layer of teflon-coated.
Further, circulation fluid entrance is provided with below described glass outer reactor, glass outer reactor
Top goes out to be provided with circulation fluid refluxing opening close to opening.
The advantage of the invention is that：Double-layer glass reaction kettle, by adding circulation fluid in interlayer, reaction can be added
Temperature or cooling processing, and realize distillation, backflow while carry out, it is ensured that experiment high efficiency progress, kettle can hand-operated lifting, just
Taken out in feeding intake with bulk crystals, be easy to clean, inner layer glass reactor bottom is funnel-shaped design, makes medicine in kettle abundant
Hybrid reaction, discharge is convenient, is easy to clean, prevents cross pollution between medicine.
Brief description of the drawings：
Accompanying drawing 1 is a kind of double-layer glass reaction kettle main structure diagram of embodiment 1.
Embodiment：
Embodiment 1：Reference picture 1, a kind of double-layer glass reaction kettle, including inner layer glass reactor 1, glass outer reactor 2, electricity
Machine 3, agitator 4, kettle cover 5, constant pressure funnel 6, condenser 7, a liftable support 9, liftable branch are provided with above base
The top of frame 9 is glass outer reactor 2, and inner layer glass reactor 1 is sleeved in glass outer reactor 2, and 5 are provided with kettle cover
4 holes, respectively constant pressure funnel interface, agitator are set by hole, condenser interface and charging aperture, the rear of liftable support
There is a controller.
In the present embodiment, all parts are installed on request, material is added to internal layer from the charging aperture 10 on kettle cover 5
Glass reactor 1, the mixing speed of the pressure and agitator 4 in kettle is adjusted as desired, the interlayer 8 of double-layer glass reaction kettle can
Freezing liquid or deep fat are added, material is cooled or heating treatment, is reacted at normal temperatures, leading to upper running water can be by reaction heat
Amount is taken away, and coordinates the condenser 7 on kettle cover 5 and Backflow bottle 11 to realize distillation or backflow, and constant pressure funnel 6 can be on kettle cover 5
Continue to add materials toward internal layer glass reactor 1 under vacuum environment, after reaction terminates, material can be put from the discharging opening 12 of bottom
Go out, the circulation fluid in interlayer 8 is discharged from the circulation fluid porch 14 of the lower section of glass outer reactor 2.
Further, the described bottom of inner layer glass reactor 1 is in funnel-form, the outside flange plate structure 15 of drain hole 12
Fixed, quick dismounting is convenient to discharge solid material, it is ensured that the clean hygiene in kettle, prevents that next time, cross pollution occurred for experiment.
Further, described motor 3 is connected with agitator 4, the flange hole through among kettle cover 5, extends to internal layer
Glass reactor 1, extends torque, increases the stirring dynamics of agitator 4, and is avoided that motor 3 touches reactant
Material, causes to damage, also improves safety coefficient to motor 3.
Further, described agitator 4 is made up of agitating shaft 16 and double-deck paddle 17, and the internal layer of agitating shaft 16 is not
Rust steel material, outer layer have one layer of teflon-coated, and the axis body of stainless steel ensure that the hardness of agitating shaft 16, polytetrafluoroethylene (PTFE)
Parcel can protect the axis body of agitating shaft 16 not corroded by reaction mass, extend its service life, double-deck structure of paddle 17 can make
Reaction mass mixes evenly.
Further, the lower section of described glass outer reactor 2 is provided with circulation fluid entrance 13, glass outer reactor
Top go out to be provided with circulation fluid refluxing opening 14 close to opening, after reaction terminates, circulation fluid can flow back from circulation fluid in interlayer 8
Mouth 14 is discharged, and is prevented circulation fluid from being deposited in interlayer 8, is avoided that reactor is caused to damage.
Certainly, better embodiment of the present invention is these are only, the use range of the present invention is not limited with this, therefore, it is every
Equivalent change is made in the principle of the invention to should be included within the scope of the present invention.
Claims (6)
1. a kind of double-layer glass reaction kettle, including inner layer glass reactor, glass outer reactor, motor, agitator, kettle cover,
Constant pressure funnel, condenser and Backflow bottle, it is characterised in that：A liftable support, liftable support are provided with above base
Top is glass outer reactor, and inner layer glass reactor jacket is provided with 4 holes in glass outer reactor on kettle cover,
Respectively constant pressure funnel interface, agitator are provided with one by hole, condenser interface and charging aperture, the rear of liftable support
Controller.
A kind of 2. double-layer glass reaction kettle according to claim 1, it is characterised in that：Described inner layer glass reactor bottom
Portion is in funnel-form, and drain hole is fixed on the bottom of glass outer reactor with flange plate structure.
A kind of 3. double-layer glass reaction kettle according to claim 1, it is characterised in that：Described motor is connected with agitator
Connect, through the flange hole among kettle cover, extend in internal layer container.
A kind of 4. double-layer glass reaction kettle according to claim 1, it is characterised in that：Described agitator by agitating shaft and
Double-deck paddle composition.
A kind of 5. double-layer glass reaction kettle according to claim 4, it is characterised in that：Described agitating shaft internal layer is stainless
Steel material, outer layer have one layer of teflon-coated.
A kind of 6. double-layer glass reaction kettle according to claim 1, it is characterised in that：Described glass outer reactor
Lower section is provided with circulation fluid entrance, and the top of glass outer reactor goes out to be provided with circulation fluid refluxing opening close to opening.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710832621.XA CN107413292A (en) | 2017-09-15 | 2017-09-15 | A kind of double-layer glass reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710832621.XA CN107413292A (en) | 2017-09-15 | 2017-09-15 | A kind of double-layer glass reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107413292A true CN107413292A (en) | 2017-12-01 |
Family
ID=60432933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710832621.XA Withdrawn CN107413292A (en) | 2017-09-15 | 2017-09-15 | A kind of double-layer glass reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107413292A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111589392A (en) * | 2020-06-28 | 2020-08-28 | 苏州北开生化设备有限公司 | High-strength corrosion-resistant glass reaction kettle and preparation method thereof |
-
2017
- 2017-09-15 CN CN201710832621.XA patent/CN107413292A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111589392A (en) * | 2020-06-28 | 2020-08-28 | 苏州北开生化设备有限公司 | High-strength corrosion-resistant glass reaction kettle and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20171201 |