CN107400761A - The heat treatment method of advanced ultra supercritical rotor forging - Google Patents

The heat treatment method of advanced ultra supercritical rotor forging Download PDF

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Publication number
CN107400761A
CN107400761A CN201610341760.8A CN201610341760A CN107400761A CN 107400761 A CN107400761 A CN 107400761A CN 201610341760 A CN201610341760 A CN 201610341760A CN 107400761 A CN107400761 A CN 107400761A
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China
Prior art keywords
forging
heat treatment
furnace
cooled
stove
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CN201610341760.8A
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Chinese (zh)
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CN107400761B (en
Inventor
王晓芳
程莉
赵永锋
凌进
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Shanghai Electric Heavy Forging Co Ltd
Shanghai Heavy Machinery Plant Co Ltd
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Shanghai Electric Heavy Forging Co Ltd
Shanghai Heavy Machinery Plant Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0068Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for particular articles not mentioned below
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00Heat treatment of ferrous alloys
    • C21D6/002Heat treatment of ferrous alloys containing Cr
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/009Pearlite

Abstract

The invention discloses a kind of heat treatment method of the advanced ultra supercritical rotor forging of COST FB2 steels, for carrying out crystal grain refinement heat treatment to the advanced ultra supercritical rotor forging of COST FB2 steels, comprises the following steps:The first step, austenitizing processing;Second step, it is furnace-cooled to balance change temperature and carries out isothermal processes;3rd step, speed limit, which is furnace-cooled to, comes out of the stove.The present invention directly enters stove progress influence of high austenizing temp processing after making forging process for fuel, makes full use of waste heat after forging, the heat time is short, and austenitizing effect is good, can make even tissue inside and outside forging.Invention can obtain pearlite type balance change tissue, crystal grain thinning degree, cut off original thick Structure Inheritance after equilibrium temperature isothermal transformation processing.Subsequent speed limit stove is cold, can avoid the excessive internal stress of rotor forging and produce cracking.

Description

The heat treatment method of advanced ultra supercritical rotor forging
Technical field
The present invention relates to a kind of heat treatment method of forging, and in particular to a kind of advanced ultra supercritical rotor forging of COST-FB2 steels Heat treatment method.
Background technology
Ultra supercritical coal-fired unit is current advanced generation technology ripe in the world, has significant efficient, energy-conservation and environmental protection excellent Gesture, current developed country all competitively use and developed this new technology.Chinese clean coal generation technology is also with Development of Ultra-Supercritical fire Group of motors is Main way, while it is also to solve electricity shortage, improve energy utilization rate and curb environmental pollution to develop the technology The most real and effective approach of problem.The advanced ultra supercritical rotor forging of COST-FB2 steels surpasses for 625 DEG C of double reheats Supercritical thermal power unit.
COST-FB2 steel belongs to 9wt%~10wt%Cr Ascalloys, have alloying element species is more, alloy content height and The good feature of quenching degree.But heavy forging Structure Inheritance is serious made of the steel grade, crystal grain need to be carried out to rotor forging after forging Refinement is heat-treated to meet forging detection and requirement.
Existing crystal grain refinement heat-treatment technology method has:(1) critical zone is quickly heated, and obtains spherical austenite;(2) repeatedly Austenitizing recrystallizes normalized treatment.But by COST-FB2 steel forgings advanced ultra supercritical rotor forging section is big, tonnage Greatly, need to control its heating and cooling velocity in heat treatment process, to avoid internal stress in heat treatment process excessive and cracked, Therefore can not quickly be heated by existing critical zone to control the grain size of forging.
In addition, COST-FB2 steel rotor forging Structure Inheritances are serious, normalized treatment is recrystallized using existing repeatedly austenitizing, The original thick tissue of meeting heredity after one side normalized treatment, can not effective crystal grain thinning;On the other hand, meeting in normalizing cooling procedure Greatly tissue and thermal stress superposition are produced, easily causes forging cracking.Therefore, above two prior heat treatment process method without Method meets COST-FB2 steel forgings crystal grain refinement heat treatment requirements.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of heat treatment of the advanced ultra supercritical rotor forging of COST-FB2 steels Method, it can make rotor forging obtain preferable grain refining effect in the case of not easy to crack.
In order to solve the above technical problems, the technology of the heat treatment method of the advanced ultra supercritical rotor forging of COST-FB2 steels of the present invention Solution is to comprise the following steps:
The first step, austenitizing processing;
It is 850 ± 10 DEG C of stove to be expected that the forging for forging completion is directly inserted into temperature, 1070 are warming up to≤30 DEG C/h speed~ 1100 DEG C of progress soaking isothermal holdings, realize that influence of high austenizing temp is handled;The soaking time of soaking isothermal holding be 1.5~ 2.0h/100mm。
Second step, it is furnace-cooled to balance change temperature and carries out isothermal processes;
Rotor forging is furnace-cooled to 700~780 DEG C of balance change temperature and carries out isothermal structural transformation, and soaking time is at least 300h;
3rd step, speed limit, which is furnace-cooled to, comes out of the stove;
After isothermal structural transformation terminates, it is furnace-cooled to≤200 DEG C with≤8 DEG C/h speed limits and comes out of the stove, completes crystal grain refinement heat treatment.
What the present invention can reach has the technical effect that:
The present invention, which makes directly to enter stove after forging process for fuel, carries out influence of high austenizing temp processing, makes full use of waste heat after forging, during heating Between it is short, austenitizing effect is good, can make even tissue inside and outside forging.Invention, can after equilibrium temperature isothermal transformation processing Pearlite type balance change tissue is obtained, crystal grain thinning degree, cuts off original thick Structure Inheritance.Subsequent speed limit stove is cold, can avoid The excessive internal stress of rotor forging and produce cracking.
The present invention is simple to operate, and cost reduces, and energy resource consumption is few, disclosure satisfy that workpiece requirement.
Brief description of the drawings
The present invention is further detailed explanation with reference to the accompanying drawings and detailed description:
Fig. 1 is the schematic diagram of the heat treatment method of the advanced ultra supercritical rotor forging of COST-FB2 steels of the present invention.
Embodiment
As shown in figure 1, the heat treatment method of the advanced ultra supercritical rotor forging of COST-FB2 steels of the present invention, for COST-FB2 The advanced ultra supercritical rotor forging of steel carries out crystal grain refinement heat treatment, comprises the following steps:
The first step, austenitizing processing;
After forging process for fuel completion, without air cooling;The forging for forging completion is directly inserted into the stove to be expected that temperature is 850 ± 10 DEG C, With≤30 DEG C/h speed be warming up to 1070~1100 DEG C progress soaking isothermal holdings, soaking time be 1.5~2.0h/100mm (i.e. Forging is incubated 1.5~2.0 hours per 100mm net sectional areas, if net sectional area is 1000mm forging, need to be incubated 15~20 Hour), realize that influence of high austenizing temp is handled, to eliminate forging stress, simultaneously uniform formation is good to obtain for adjustment forging grain size Matrix;
Second step, it is furnace-cooled to balance change temperature and carries out isothermal processes;
Rotor forging is furnace-cooled to 700~780 DEG C of balance change temperature and carries out isothermal structural transformation, and soaking time is at least 300h, with Obtain and change complete pearlite type balance change tissue, crystal grain thinning degree, cut off original thick Structure Inheritance;
3rd step, speed limit, which is furnace-cooled to, comes out of the stove;
After isothermal structural transformation terminates, it is furnace-cooled to≤200 DEG C with≤8 DEG C/h speed limits and comes out of the stove, completes crystal grain refinement heat treatment.
The present invention makes COST-FB2 steel grades held for some time at 1070~1100 DEG C, and crystal grain will not drastically grow up;The present invention Consider COST-FB2 Steel material characteristics, the factor such as forging final forging temperature and effective cross-section size, determine COST-FB2 steel forgings Part crystal grain refinement heat treatment process parameter.
The present invention abandons critical zone and quickly heated, and obtains spherical austenite and multiple austenitizing recrystallization two kinds of tradition of normalized treatment Crystal grain refinement heat-treatment technology method, employ austenite Homogenization Treatments add isothermal processes obtain balance change tissue method To refine COST-FB2 steel forgings coarse grains.
The present invention makes full use of waste heat after forging, can not only save the energy, and forging can be made to reach austenitizing guarantor in the short period Temperature, adjustment forging grain size and homogeneous wrought tissue, good basic organization is provided for follow-up isothermal transformation.Isothermal processes After can obtain the complete pearlite type balance change tissue of transformation, crystal grain thinning degree, cut off original thick Structure Inheritance, improve and turn Sub- forging ultrasonic flaw detection detection sensitivity, good basic organization is provided for lower step property heat treatment.It is simultaneously subsequent Speed limit cooling can reduce forging internal stress, avoid forging cracking.

Claims (2)

  1. A kind of 1. heat treatment method of the advanced ultra supercritical rotor forging of COST-FB2 steels, for first to COST-FB2 steels Enter ultra supercritical rotor forging and carry out crystal grain refinement heat treatment, it is characterised in that comprise the following steps:
    The first step, austenitizing processing;
    It is 850 ± 10 DEG C of stove to be expected that the forging for forging completion is directly inserted into temperature, 1070 are warming up to≤30 DEG C/h speed~ 1100 DEG C of progress soaking isothermal holdings, realize that influence of high austenizing temp is handled;
    Second step, it is furnace-cooled to balance change temperature and carries out isothermal processes;
    Rotor forging is furnace-cooled to 700~780 DEG C of balance change temperature and carries out isothermal structural transformation, and soaking time is at least 300h;
    3rd step, speed limit, which is furnace-cooled to, comes out of the stove;
    After isothermal structural transformation terminates, it is furnace-cooled to≤200 DEG C with≤8 DEG C/h speed limits and comes out of the stove, completes crystal grain refinement heat treatment.
  2. 2. the heat treatment method of the advanced ultra supercritical rotor forging of COST-FB2 steels according to claim 1, its feature It is, the soaking time of soaking isothermal holding is 1.5~2.0h/100mm in the first step.
CN201610341760.8A 2016-05-20 2016-05-20 The heat treatment method of advanced ultra supercritical rotor forging Active CN107400761B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109402365A (en) * 2018-12-21 2019-03-01 扬州龙川钢管有限公司 A kind of conditioning treatment process solving T/P91, T/P92 mixed grain structure
CN113667807A (en) * 2020-05-15 2021-11-19 上海电气电站设备有限公司 Heat-resistant steel, heat treatment method and application
CN114875214A (en) * 2022-06-01 2022-08-09 东北大学 Heat treatment method of COST-FB2 steel large forging

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US5716468A (en) * 1994-12-26 1998-02-10 The Japan Steel Works, Ltd. Process for producing high-and low-pressure integral-type turbine rotor
CN101831535A (en) * 2009-03-12 2010-09-15 上海重型机器锻件厂 Heat treatment method after forging of ultra-supercritical high and medium pressure rotor steel
CN102134637A (en) * 2011-01-18 2011-07-27 上海交通大学 Method for refining grains of large medium high alloy steel forgings
CN103305673A (en) * 2013-07-01 2013-09-18 江阴市恒业锻造有限公司 Method for manufacturing fine-grain 35CrNi3MoV steel large forging stock
CN103343200A (en) * 2013-07-01 2013-10-09 江阴市恒业锻造有限公司 Short-process thermal treatment method of large 35CrNi3MoV steel forgings

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Publication number Priority date Publication date Assignee Title
US5716468A (en) * 1994-12-26 1998-02-10 The Japan Steel Works, Ltd. Process for producing high-and low-pressure integral-type turbine rotor
CN101831535A (en) * 2009-03-12 2010-09-15 上海重型机器锻件厂 Heat treatment method after forging of ultra-supercritical high and medium pressure rotor steel
CN102134637A (en) * 2011-01-18 2011-07-27 上海交通大学 Method for refining grains of large medium high alloy steel forgings
CN103305673A (en) * 2013-07-01 2013-09-18 江阴市恒业锻造有限公司 Method for manufacturing fine-grain 35CrNi3MoV steel large forging stock
CN103343200A (en) * 2013-07-01 2013-10-09 江阴市恒业锻造有限公司 Short-process thermal treatment method of large 35CrNi3MoV steel forgings

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Title
刘志祥: "12%Cr超超临界转子钢热处理基础研究与工艺模拟", 《中国优秀硕士学问论文全文数据库 工程科技I辑》 *
王晓芳: "620℃汽轮机转子锻件用钢晶粒细化热处理工艺研究", 《大型铸锻件》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109402365A (en) * 2018-12-21 2019-03-01 扬州龙川钢管有限公司 A kind of conditioning treatment process solving T/P91, T/P92 mixed grain structure
CN113667807A (en) * 2020-05-15 2021-11-19 上海电气电站设备有限公司 Heat-resistant steel, heat treatment method and application
CN114875214A (en) * 2022-06-01 2022-08-09 东北大学 Heat treatment method of COST-FB2 steel large forging

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