CN107386004A - A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper - Google Patents
A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper Download PDFInfo
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- CN107386004A CN107386004A CN201710859811.0A CN201710859811A CN107386004A CN 107386004 A CN107386004 A CN 107386004A CN 201710859811 A CN201710859811 A CN 201710859811A CN 107386004 A CN107386004 A CN 107386004A
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-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
- D21H11/02—Chemical or chemomechanical or chemothermomechanical pulp
- D21H11/04—Kraft or sulfate pulp
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/06—Paper forming aids
- D21H21/10—Retention agents or drainage improvers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
- D21H21/20—Wet strength agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/28—Colorants ; Pigments or opacifying agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/34—Ignifugeants
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Paper (AREA)
Abstract
It is packed for being sustained the preparation technology of odor type flame-retardant decorative paper the invention discloses a kind of gift box, it is characterized in that, crosslinking agent sodium tripolyphosphate, capsule heart lemon extract, emulsifier tween 20 are well mixed, are added drop-wise in chitosan-acetic acid solution, cross-linking reaction obtains being sustained essence microcapsule；By APP, diatomite mixing and ball milling, addition is silane coupler modified, obtains the composite flame-proof filler of coupling modifier；Distilled water, sodium hexametaphosphate dispersant are added into titanium dioxide, is sanded and disperses to obtain pigment solution；Wood pulp is soaked, is beaten, dry after refrigerate equilibrium water conten, discongest, then be well mixed with above resulting material and retention agent, wet strength agent, pH adjusting agent, obtain slurry；Whitewashing forms l Water Paper, then through squeezing, drying, maturation process obtains sustained release odor type flame-retardant decorative paper.
Description
Technical field
The present invention relates to packing box field, and in particular to a kind of gift box is packed for being sustained the preparation work of odor type flame-retardant decorative paper
Skill.
Background technology
Facing paper is a kind of new industry, paper for daily use, and the production of facing paper will mainly fill out during manufacturing paper with pulp
Material is all added to slurry pool and mixed with paper pulp, and then being manufactured paper with pulp through paper machine forms.Essence microcapsule is using natural or synthetic
High polymer material essence is wrapped up, can both avoid the direct light of essence, heat influence and cause oxidation deterioration, again may be used
To avoid the volatilization of active ingredient in essence, the release of fragrance matter is effectively controlled, improves the stability of fragrance.With string
Construction material, house decorative material, packaging material for primary raw material etc. are a kind of combustible materials for causing fire.String
Flame Retardant Mechanism and the flame-retarded technology exploitation of paper are to reduce disaster hidden-trouble, reduce the need of casualties and property loss in fire
Will.Addition inorganic combustion inhibitor is the effective ways for preparing fire retardant papers in slurry.
The content of the invention
The present invention solves the technical problem of the preparation that a kind of gift box of offer is packed for being sustained odor type flame-retardant decorative paper
Technique, the facing paper fire resistance according to this method preparation is good and has slow-release fragrance.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper, it is characterised in that according to the following steps
Carry out：
A. it is sustained the ionic cross-linking preparation technology of essence microcapsule：
Into 1-2 parts by weight wall material chitosans 1:5-10 adds spirit of vinegar, and stirring and dissolving, it is 2-2.5g/L's to be made into mass concentration
Chitosan-acetic acid solution；
Into 1-2 parts by weight of crosslinking agent sodium tripolyphosphates 1:5-10 adds distilled water, stirring and dissolving, adds the 3-4 parts by weight capsule hearts
Lemon extract, 1-2 parts by weight Emulsifier polysorbas20s, after high-speed stirred is uniform, are added drop-wise in chitosan-acetic acid solution, molten with NaOH
It is 5-6 that liquid, which adjusts pH, continues stirring crosslinking reaction 30-40min, filters, washs, vacuum freeze drying obtains being sustained the micro- glue of essence
Capsule；
B. the coupling modifier of composite flame-proof filler：
Into 0.1-0.2 parts by weight Silane coupling agent KH550s 1:1-2 adds absolute ethyl alcohol dilution, and it is 3- to adjust pH with glacial acetic acid
5, obtain coupling modifier；
By 4-7 parts by weight APP, 6-9 parts by weight diatomite mixing and ball millings, 100-200 mesh sieves are crossed, obtain composite flame-proof filler,
1:5-10 adds ethanol, in 65-75 DEG C of stirring of water-bath high speed, ultrasonic disperse 20-30min, is slowly added to coupling modifier, after
Continuous stirring in water bath 1-2h, filters, is dried to constant weight at 100-105 DEG C, obtain the composite flame-proof filler of coupling modifier；
C. the mashing of facing paper, manufacture paper with pulp, squeeze, dry curing process：
Into 15-20 parts by weight pigment titanium whites 1:40-50 adds distilled water, pours into frosting dispersion machine, adds 1-2 parts by weight
Sodium hexametaphosphate dispersant, scattered 1-2h obtain pigment solution；
20-30 parts by weight bleached sulphate softwood pulps and 70-80 parts by weight BRATSK pulpboards are torn into small
Piece is put into soaked overnight in distilled water, pours into beater and is beaten, until beating degree is 40-45oSR, is then got rid of with drier
Dry, sealing is put into refrigerated overnight in refrigerator, after equilibrium water conten, is added in paper pulp standard fluffer and carries out discongesting 5-10min, machine
Under tool stirring, pigment solution, 5-10 parts by weight retention agent, 1-2 parts by weight wet strength agent, 1-3 parts by weight pH adjusting agent and a, b are added
Middle resulting material, continue to stir 10-20min, obtain slurry；
Slurry is poured into sheet forming apparatus, opens agitator and mashing pump, whitewashing forms l Water Paper, by l Water Paper in page squeezer
Upper squeezing, then it is placed on sheet dryer in 100-105 DEG C of heat drying 15-20min, places into 100-105 DEG C of baking oven
Maturation process 30-40min is carried out, obtains the sustained release odor type flame-retardant decorative paper.
Wherein, spirit of vinegar concentration described in step a is 8-10%, and high-speed stirred speed is 800-1000rpm, NaOH solution
Concentration is 2-4%.
Fluffer rotating speed described in step c is 15000-16000rpm, and mechanical agitation speed is 900-1000rpm, retention
Agent is the polyacrylamide solution that concentration is 4-6%, and wet strength agent is the polyamideepichlorohydrin solution that concentration is 8-9%, and pH is adjusted
Section agent is the aluminum sulfate solution that concentration is 1-2%.
The present invention reaction mechanism and have the beneficial effect that：
Using lemon extract be the capsule heart, chitosan as wall material, sodium tripolyphosphate be crosslinking agent, polysorbas20 for emulsifying agent, pass through ion
Sustained release essence microcapsule is made in cross-linking method, and chitosan, there occurs crosslinked action, occurs with sodium tripolyphosphate between chitosan and essence
Intermolecular force, essence embedding is in microcapsules, had good sustained release effect.
APP, diatomite mixing and ball milling are obtained into compound flame retardant filler, use Silane coupling agent KH550
Surface modification is carried out to compounded mix, modification can improve the hydrophobicity of compounded mix, improve its stability in water, gather
Ammonium phosphate can increase the cigarette rate of release and CO generating rates of combustion process, and diatomite can effectively suppress smog and CO release,
The collaboration that both produce condensed phase acts on into charcoal, improves the flame retardant effect of pattern.
Paper pulp, pigment titanium white, modifying agent, retention agent, wet strength agent, pH adjusting agent are mixed to get slurry, whitewashing is formed
L Water Paper, then through squeezing, drying, maturation process, obtain being sustained odor type flame-retardant decorative paper.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment
A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper, it is characterised in that according to the following steps
Carry out：
A. it is sustained the ionic cross-linking preparation technology of essence microcapsule：
Into 2kg wall material chitosans 1:10 add spirit of vinegar, stirring and dissolving, are made into the chitosan acetic acid that mass concentration is 2.5g/L
Solution；
Into 1kg crosslinking agent sodium tripolyphosphates 1:10 add distilled water, stirring and dissolving, add 4kg capsule hearts lemon extract, 1kg breasts
Agent polysorbas20, after high-speed stirred is uniform, it is added drop-wise in chitosan-acetic acid solution, it is 5-6 to adjust pH with NaOH solution, continues to stir
Cross-linking reaction 35min, filter, wash, vacuum freeze drying obtains being sustained essence microcapsule；
B. the coupling modifier of composite flame-proof filler：
Into 0.1kg Silane coupling agent KH550s 1:1 adds absolute ethyl alcohol dilution, and it is 4-5 to adjust pH with glacial acetic acid, obtains coupling and changes
Property agent；
By 4kg APPs, 6kg diatomite mixing and ball millings, 200 mesh sieves are crossed, obtain composite flame-proof filler, 1:10 add ethanol,
The stirring of 65-75 DEG C of water-bath high speed, ultrasonic disperse 30min, are slowly added to coupling modifier, continue stirring in water bath 1h, filter,
Constant weight is dried at 100-105 DEG C, obtains the composite flame-proof filler of coupling modifier；
C. the mashing of facing paper, manufacture paper with pulp, squeeze, dry curing process：
Into 15kg pigment titanium whites 1:40 add distilled water, pour into frosting dispersion machine, add 2kg dispersant hexa metaphosphoric acids
Sodium, scattered 2h obtain pigment solution；
25kg bleached sulphates softwood pulp and 75kg BRATSK pulpboards are torn into small pieces and be put into distilled water
Soaked overnight, pour into beater and be beaten, until beating degree is 40-45oSR, then dried with drier, sealing is put into refrigerator
After interior refrigerated overnight, equilibrium water conten, it is added in paper pulp standard fluffer and discongest 10min, under mechanical agitation, adds pigment
Resulting material in solution, 5kg retention agents, 2kg wet strength agents, 1kg pH adjusting agents and a, b, continue to stir 20min, obtain slurry；
Slurry is poured into sheet forming apparatus, opens agitator and mashing pump, whitewashing forms l Water Paper, by l Water Paper in page squeezer
Upper squeezing, then it is placed on sheet dryer in 100-105 DEG C of heat drying 20min, places into 100-105 DEG C of baking oven and carry out
Maturation process 40min, obtain the sustained release odor type flame-retardant decorative paper.
Wherein, spirit of vinegar concentration described in step a is 10%, and high-speed stirred speed is 1000rpm, and NaOH solution concentration is
4%。
Fluffer rotating speed described in step c is 16000rpm, and mechanical agitation speed is 1000rpm, and retention agent is that concentration is
6% polyacrylamide solution, wet strength agent are the polyamideepichlorohydrin solution that concentration is 8%, and pH adjusting agent is that concentration is 2%
Aluminum sulfate solution.
Claims (4)
1. a kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper, it is characterised in that by crosslinking agent tripolyphosphate
Sodium, capsule heart lemon extract, emulsifier tween 20 are well mixed, are added drop-wise in chitosan-acetic acid solution, cross-linking reaction is sustained
Essence microcapsule；By APP, diatomite mixing and ball milling, addition is silane coupler modified, obtains the compound resistance of coupling modifier
Fire filler；Distilled water, sodium hexametaphosphate dispersant are added into titanium dioxide, is sanded and disperses to obtain pigment solution；Wood pulp is soaked,
Mashing, equilibrium water conten is refrigerated after drying, discongested, then mixed with above resulting material and retention agent, wet strength agent, pH adjusting agent
It is even, obtain slurry；Whitewashing forms l Water Paper, then through squeezing, drying, maturation process obtains sustained release odor type flame-retardant decorative paper.
2. a kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper, it is characterised in that：
A. it is sustained the ionic cross-linking preparation technology of essence microcapsule：
Into 1-2 parts by weight wall material chitosans 1:5-10 adds spirit of vinegar, and stirring and dissolving, it is 2-2.5g/L's to be made into mass concentration
Chitosan-acetic acid solution；
Into 1-2 parts by weight of crosslinking agent sodium tripolyphosphates 1:5-10 adds distilled water, stirring and dissolving, adds the 3-4 parts by weight capsule hearts
Lemon extract, 1-2 parts by weight Emulsifier polysorbas20s, after high-speed stirred is uniform, are added drop-wise in chitosan-acetic acid solution, molten with NaOH
It is 5-6 that liquid, which adjusts pH, continues stirring crosslinking reaction 30-40min, filters, washs, vacuum freeze drying obtains being sustained the micro- glue of essence
Capsule；
B. the coupling modifier of composite flame-proof filler：
Into 0.1-0.2 parts by weight Silane coupling agent KH550s 1:1-2 adds absolute ethyl alcohol dilution, and it is 3- to adjust pH with glacial acetic acid
5, obtain coupling modifier；
By 4-7 parts by weight APP, 6-9 parts by weight diatomite mixing and ball millings, 100-200 mesh sieves are crossed, obtain composite flame-proof filler,
1:5-10 adds ethanol, in 65-75 DEG C of stirring of water-bath high speed, ultrasonic disperse 20-30min, is slowly added to coupling modifier, after
Continuous stirring in water bath 1-2h, filters, is dried to constant weight at 100-105 DEG C, obtain the composite flame-proof filler of coupling modifier；
C. the mashing of facing paper, manufacture paper with pulp, squeeze, dry curing process：
Into 15-20 parts by weight pigment titanium whites 1:40-50 adds distilled water, pours into frosting dispersion machine, adds 1-2 parts by weight
Sodium hexametaphosphate dispersant, scattered 1-2h obtain pigment solution；
20-30 parts by weight bleached sulphate softwood pulps and 70-80 parts by weight BRATSK pulpboards are torn into small
Piece is put into soaked overnight in distilled water, pours into beater and is beaten, until beating degree is 40-45oSR, is then got rid of with drier
Dry, sealing is put into refrigerated overnight in refrigerator, after equilibrium water conten, is added in paper pulp standard fluffer and carries out discongesting 5-10min, machine
Under tool stirring, pigment solution, 5-10 parts by weight retention agent, 1-2 parts by weight wet strength agent, 1-3 parts by weight pH adjusting agent and a, b are added
Middle resulting material, continue to stir 10-20min, obtain slurry；
Slurry is poured into sheet forming apparatus, opens agitator and mashing pump, whitewashing forms l Water Paper, by l Water Paper in page squeezer
Upper squeezing, then it is placed on sheet dryer in 100-105 DEG C of heat drying 15-20min, places into 100-105 DEG C of baking oven
Maturation process 30-40min is carried out, obtains the sustained release odor type flame-retardant decorative paper.
3. a kind of gift box according to claim 2 is packed for being sustained the preparation technology of odor type flame-retardant decorative paper, its feature exists
In spirit of vinegar concentration described in step a is 8-10%, and high-speed stirred speed is 800-1000rpm, and NaOH solution concentration is 2-4%.
4. a kind of gift box according to claim 2 is packed for being sustained the preparation technology of odor type flame-retardant decorative paper,
Characterized in that, fluffer rotating speed described in step c is 15000-16000rpm, mechanical agitation speed is 900-
1000rpm, retention agent are the polyacrylamide solutions that concentration is 4-6%, and wet strength agent is the daiamid epoxy chlorine third that concentration is 8-9%
Alkane solution, pH adjusting agent are the aluminum sulfate solutions that concentration is 1-2%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710859811.0A CN107386004A (en) | 2017-09-21 | 2017-09-21 | A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710859811.0A CN107386004A (en) | 2017-09-21 | 2017-09-21 | A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper |
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| Publication Number | Publication Date |
|---|---|
| CN107386004A true CN107386004A (en) | 2017-11-24 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710859811.0A Pending CN107386004A (en) | 2017-09-21 | 2017-09-21 | A kind of gift box is packed for being sustained the preparation technology of odor type flame-retardant decorative paper |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108559133A (en) * | 2018-04-20 | 2018-09-21 | 南京工业大学 | Preparation method of diatomite-based inorganic-organic hybrid flame retardant |
| CN109046192A (en) * | 2018-08-28 | 2018-12-21 | 浙江大学 | A kind of plants essential oil chitosan nano mcirocapsule and its preparation method and application |
| CN110396861A (en) * | 2019-07-08 | 2019-11-01 | 天津科技大学 | A kind of preparation method of microencapsulation fire retardant |
| CN113367537A (en) * | 2020-08-27 | 2021-09-10 | 黄继龙 | Traditional Chinese medicine pillow for mental patients and preparation method thereof |
| CN116289322A (en) * | 2023-03-13 | 2023-06-23 | 浙江理工大学 | Preparation method of cationized hydrophobic microcapsule flame-retardant paper |
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| CN203961185U (en) * | 2014-05-30 | 2014-11-26 | 苏州国昊壁纸有限公司 | A kind of environmental protection wallpaper of aroma type |
| CN106676945A (en) * | 2016-12-30 | 2017-05-17 | 芜湖市哈贝纸业有限公司 | Corrugating base paper |
| CN106702808A (en) * | 2016-12-09 | 2017-05-24 | 张日龙 | Wear-proof plain-color decoration body paper and preparation method thereof |
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2017
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| CN203961185U (en) * | 2014-05-30 | 2014-11-26 | 苏州国昊壁纸有限公司 | A kind of environmental protection wallpaper of aroma type |
| CN106702808A (en) * | 2016-12-09 | 2017-05-24 | 张日龙 | Wear-proof plain-color decoration body paper and preparation method thereof |
| CN106676945A (en) * | 2016-12-30 | 2017-05-17 | 芜湖市哈贝纸业有限公司 | Corrugating base paper |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108559133A (en) * | 2018-04-20 | 2018-09-21 | 南京工业大学 | Preparation method of diatomite-based inorganic-organic hybrid flame retardant |
| CN109046192A (en) * | 2018-08-28 | 2018-12-21 | 浙江大学 | A kind of plants essential oil chitosan nano mcirocapsule and its preparation method and application |
| CN110396861A (en) * | 2019-07-08 | 2019-11-01 | 天津科技大学 | A kind of preparation method of microencapsulation fire retardant |
| CN110396861B (en) * | 2019-07-08 | 2022-02-18 | 天津科技大学 | Preparation method of microencapsulated flame retardant |
| CN113367537A (en) * | 2020-08-27 | 2021-09-10 | 黄继龙 | Traditional Chinese medicine pillow for mental patients and preparation method thereof |
| CN116289322A (en) * | 2023-03-13 | 2023-06-23 | 浙江理工大学 | Preparation method of cationized hydrophobic microcapsule flame-retardant paper |
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Application publication date: 20171124 |