CN107362089A - 一种发质调理免洗喷雾 - Google Patents
一种发质调理免洗喷雾 Download PDFInfo
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Abstract
本发明公开了一种发质调理免洗喷雾，包括落地生根黄酮、凌霄花挥发油、老鹳草鞣质、库拉索芦荟汁、甘油、玉米淀粉、苯甲酸钠等成分。喷雾中含有的落地生根黄酮能有效调节头皮血管微循环，凌霄花挥发油进一步舒缓头皮，促进营养成分的吸收，结合老鹳草鞣质抑制细胞脂质过氧化并抑制头部微生物繁殖，几种成分协同作用，能起到清洁头皮，舒缓头皮，促进发根吸收营养的作用；且本发明的喷雾能促进虫、菌刺激消退，使相关物质刺激导致的瘙痒肿痛得到缓解，从而减少了头皮损伤，维持头部肌肤的健康；有很好的补水作用，可有效防止由于头发水分和蛋白流失造成的发梢受损，减少头发分叉、枯黄、脆弱、打结等问题，有效调理发质。
Description
技术领域
本发明涉及日用化学品领域，具体涉及一种发质调理免洗喷雾。
背景技术
一般人的头发，其发质由发根向发尾递减，这是因为受到了氧化伤害，导致结构松弛，毛躁、分叉和变黄随之而来。日常的过度烫染发不当，头发的蛋白质纤维会受到碱的伤害而流失，液会呈现无弹性的症状。头发是否有光泽是头发质量的直观体现，因此，很多人都希望把头发护理得更加光亮，通过油脂、保湿物质，利用洗发、润丝、护发、日常护理等途径，补充头发保湿物质，进而增进头发内水分含量，使头发更柔亮。
市面上的洗发护发产品林林总总，但很多选用的原料含杂质成分可能对人体健康存在安全隐患，长期使用安全风险大，如甲醛释放体类、尼泊金酯类防腐剂对人体有致癌风险；合成色素对人体易导致皮肤过敏；含环氧乙烷结构的原料会带人微量的易使人致癌的二噁烷等。因此，护发产品的安全和有效，是消费者所期待的。
发明内容
基于此，本发明的目的在于提供一种发质护理免洗喷雾，能有效调节头皮血流微循环，缓解头皮瘙痒，减少头屑，改善发质。
为了达到上述目的，本发明提供如下的技术方案：
一种发质调理免洗喷雾包括以下质量份的组分：落地生根黄酮0.5-2.0％、凌霄花挥发油2.0-5.0％、老鹳草鞣质0.5-3.0％。
优选地，落地生根黄酮0.8-1.5％、凌霄花挥发油2.5-4.0％％、老鹳草鞣质0.8-2.5％。
最优选的，落地生根黄酮1.2％、凌霄花挥发油3.5％、老鹳草鞣质1.8％。
所述的落地生根黄酮的制备方法包括：采集新鲜落地生根，洗净，烘干，切碎片用粉碎机粉碎得落地生根粉；按照1：(12-15)的比例将落地生根粉加入30-60℃石油醚中，采用超声处理25-35min，取出放冷，过滤，弃去石油醚；待药渣挥干石油醚后，加入70-70％乙醇溶液中75-85W，48-53kHz下超声辅助下浸提，过滤，合并滤液；药渣用70-70％乙醇洗涤2-3次，滤液合并；用70-70％乙醇定容滤液，得落地生根黄酮。
所述的凌霄花挥发油的制备方法包括：将新鲜凌霄花洗净，烘干，切碎片用粉碎机成凌霄花粉；将上述所得花粉用1-5倍重量份的60～80％乙醇浸泡10～30分钟，萃取采用36～43℃恒温萃取的方式，萃取压力27～30MPa，CO2流速3.5～4kg/h，分离压力4～6MPa，萃取时间1.5～2h；分离提纯，得凌霄花挥发油。
所述的老鹳草鞣质的制备方法包括：将新鲜老鹳草洗净，烘干，切碎片用粉碎机成老鹳草粉末；按照重量比1:4的比例将老鹳草粉末加入溶剂水浴浸提，过滤；滤液进行活性炭脱色，过滤，得粗提液；将上述所得粗提液，按照2:1比例加入乙酸乙酯，40-45℃摇床水浴保温28-35min，静置分层，得老鹳草鞣质。且所述的老鹳草鞣质制备方法中，水浴浸提使用的溶剂为水、丙酮、乙酸乙酯复配溶剂。
所述喷雾还包括以下质量份的组分：库拉索芦荟汁0.1-0.5％、甘油3.0-5.0％、玉米淀粉0.1-0.5％、苯甲酸钠0.01-0.1％、山梨酸钾0.01-0.1、聚乙二醇-400.2-0.8％、聚季铵盐-110.2-0.6％、变性乙醇5.0-10％、去离子水余量。
本发明还提供一种发质调理免洗喷雾的制备方法，包括以下步骤：
(1)将甘油、玉米淀粉、苯甲酸钠、山梨酸钾、聚乙二醇-40、聚季铵盐-11、去离子水搅拌微加热至55-60℃，溶解均匀，制得A相；
(2)将落地生根黄酮、凌霄花挥发油、老鹳草鞣质、变性乙醇混合溶解完全，制得B相；
(3)将B相加入A相，800-1300r/min速度下搅拌3-5min，搅拌均匀，出料。
对本发明的植物成分作如下介绍：
落地生根是景天科植物落地生根的全草及根，其提取物包含多种生物活性成分，有生物碱、萜类、甾体类、黄酮类、醌类以及苯丙类等。落地生根黄酮能有效的调节血液的凝血作用，加快损伤处修复，抑制正常处凝固堵塞，进而调节血液微循环。同时也能对外部的微生物进行抑制作用，减少微生物的分泌物对头皮的刺激。
凌霄花为紫葳科植物凌霄或美洲凌霄的干燥花，有调理血液微循环，缓解瘙痒和痤疮的情况。含有三萜类、苯丙醇苷、黄酮类、花色素和挥发油等成分。本产品主要使用凌霄花挥发油。其能显著抑制DNA损伤断裂，能有效防止氧化损伤造成的细胞损伤，同时能调节血管通透性，使局部皮肤由于炎症或蚊虫导致的瘙痒肿胀症状得到缓解与消退。且凌霄花挥发油能很好地改善血流流速，避免不正常的流速造成充血淤血出血等症状。
老鹳草为牻牛儿苗科老鹳草属植物，主要含有鞣质、黄酮类、有机酸和挥发油等化学成分。具有消炎抗菌、抗氧化、抗损伤等功效。其中老鹳草鞣质能有效抑制微生物在皮肤表面吸附和生长，能选择性结合微生物内部的酶，从而抑制酶活性，进而杀死微生物。同时老鹳草鞣质也能抑制人体细胞内细胞器的脂质过氧化，进而防止脂质过氧化的损伤，另外能有效还原有害金属离子，保护维生素C不进行自氧化失活。
与现有技术相比，本发明具有的有益效果如下：(1)本发明的免洗喷雾中含有的落地生根黄酮能有效调节头皮血管微循环，凌霄花挥发油进一步舒缓头皮，促进营养成分的吸收，结合老鹳草鞣质抑制细胞脂质过氧化并抑制头部微生物繁殖，几种成分协同作用，能起到清洁头皮，舒缓头皮，促进发根吸收营养的作用；(2)本发明的喷雾能促进虫、菌刺激消退，使相关物质刺激导致的瘙痒肿痛得到缓解，从而减少了头皮损伤，维持头部肌肤的健康；(3)本发明的喷雾有很好的补水作用，可有效防止由于头发水分和蛋白流失造成的发梢受损，减少头发分叉、枯黄、脆弱、打结等问题；(4)本发明的产品不仅能有效调理发质，其使用也方便，免洗的喷雾剂型可以随时给头发补充营养。
具体实施方式
以下结合具体实施例对本发明作进一步阐述。
本发明实施例1-5本发明发质调理免洗喷雾配方见表1
表1
上述的落地生根黄酮的制备方法如下：
采集新鲜落地生根，洗净，烘干，切碎片用粉碎机粉碎得落地生根粉；按照1：15的比例将落地生根粉加入45℃石油醚中，采用超声处理30min，取出放冷，过滤，弃去石油醚；待药渣挥干石油醚后，加入70％乙醇溶液中80W，50kHz下超声辅助下浸提，过滤，合并滤液；药渣用70％乙醇洗涤3次，滤液合并；用70％乙醇定容滤液，得落地生根黄酮。
上述的凌霄花挥发油的制备方法如下：
将新鲜凌霄花洗净，烘干，切碎片用粉碎机成凌霄花粉；将上述所得花粉用5倍重量份的70％乙醇浸泡30分钟，萃取采用40℃恒温萃取的方式，萃取压力30MPa，CO2流速4kg/h，分离压力5MPa，萃取时间2h；分离提纯，得凌霄花挥发油。
上述的老鹳草鞣质的制备方法如下：
将新鲜老鹳草洗净，烘干，切碎片用粉碎机成老鹳草粉末；按照重量比1:4的比例将老鹳草粉末加入溶剂水浴浸提，过滤；滤液进行活性炭脱色，过滤，得粗提液；将上述所得粗提液，按照2:1比例加入乙酸乙酯，45℃摇床水浴保温30min，静置分层，得老鹳草鞣质。且所述的老鹳草鞣质制备方法中，水浴浸提使用的溶剂为水、丙酮、乙酸乙酯复配溶剂。
实施例1-5一种发质调理免洗喷雾的制备方法如下：
(4)将甘油、玉米淀粉、苯甲酸钠、山梨酸钾、聚乙二醇-40、聚季铵盐-11、去离子水搅拌微加热至60℃，溶解均匀，制得A相；
(5)将落地生根黄酮、凌霄花挥发油、老鹳草鞣质、变性乙醇混合溶解完全，制得B相；
(6)将B相加入A相，1000r/min速度下搅拌5min，搅拌均匀，出料。
对比例1
与实施例1的区别是未加入落地生根黄酮，其他制备条件和方法与实施例1相同。
对比例2
与实施例1的区别是未加入凌霄花挥发油，其他制备条件和方法与实施例1相同。
对比例3
与实施例1的区别是未加入老鹳草鞣质，其他制备条件和方法与实施例1相同。
功效试验
实施例1-5和对比例1-3制备的产品进行试用检测效果，同时以一款市售的宣称具有调理发质功效的化妆品为对照组。
测试对象：各实验组均为30名志愿者(25-50岁)。
所有志愿者使用所在组的产品，试用为期一个月，第30天统计一次试用结果，实验结果见表2
表2
上述数据表明，实施例1-5制得的产品调理发质效果明显高于对比例和对照组，本发明发质调理免洗喷雾中的落地生根黄酮、凌霄花挥发油和老鹳草鞣质三种成分协同增效，不仅能起到清洁头皮，舒缓头皮，促进发根吸收营养的作用，还能减少头发分叉、枯黄、脆弱、打结等问题。
上述实施例仅说明本发明的实施方案，并没有对本发明有任何形式上的限制；任何从事本专业的技术人员，都有能力利用揭示的技术内容作出一些更动或修饰，成为等同变化的等效实施例，根据本发明技术实质，对本发明进行简单修改、等同变化与修饰，均属于本发明技术方案的范围内。
Claims (9)
1.一种发质调理免洗喷雾，其特征在于，包括以下质量百分比的组分：落地生根黄酮0.5-2.0％、凌霄花挥发油2.0-5.0％、老鹳草鞣质0.5-3.0％。
2.根据权利要求1所述的一种发质调理免洗喷雾，其特征在于，包括以下质量百分比的组分：落地生根黄酮0.8-1.5％、凌霄花挥发油2.5-4.0％％、老鹳草鞣质0.8-2.5％。
3.根据权利要求2所述的一种发质调理免洗喷雾，其特征在于，包括以下质量百分比的组分：落地生根黄酮1.2％、凌霄花挥发油3.5％、老鹳草鞣质1.8％。
4.根据权利要求1-3任一项所述的一种发质调理免洗喷雾，其特征在于，所述的落地生根黄酮的制备方法包括：采集新鲜落地生根，洗净，烘干，切碎片用粉碎机粉碎得落地生根粉；按照1：(12-15)的比例将落地生根粉加入30-60℃石油醚中，采用超声处理25-35min，取出放冷，过滤，弃去石油醚；待药渣挥干石油醚后，加入70-70％乙醇溶液中75-85W，48-53kHz下超声辅助下浸提，过滤，合并滤液；药渣用70-70％乙醇洗涤2-3次，滤液合并；用70-70％乙醇定容滤液，得落地生根黄酮。
5.根据权利要求1-3任一项所述的一种发质调理免洗喷雾，其特征在于，所述的凌霄花挥发油的制备方法包括：将新鲜凌霄花洗净，烘干，切碎片用粉碎机成凌霄花粉；将上述所得花粉用1-5倍重量份的60～80％乙醇浸泡10～30分钟，萃取采用36～43℃恒温萃取的方式，萃取压力27～30MPa，CO2流速3.5～4kg/h，分离压力4～6MPa，萃取时间1.5～2h；分离提纯，得凌霄花挥发油。
6.根据权利要求1-3任一项所述的一种发质调理免洗喷雾，其特征在于，所述的老鹳草鞣质的制备方法包括：将新鲜老鹳草洗净，烘干，切碎片用粉碎机成老鹳草粉末；按照重量比1:4的比例将老鹳草粉末加入溶剂水浴浸提，过滤；滤液进行活性炭脱色，过滤，得粗提液；将上述所得粗提液，按照2:1比例加入乙酸乙酯，40-45℃摇床水浴保温28-35min，静置分层，得老鹳草鞣质。
7.根据权利要求6所述的一种发质调理免洗喷雾，其特征在于，所述的老鹳草鞣质制备方法中，水浴浸提使用的溶剂为水、丙酮、乙酸乙酯复配溶剂。
8.根据权利要求1-7任一项所述的一种发质调理免洗喷雾，其特征在于，所述喷雾还包括以下质量百分比的组分：库拉索芦荟汁0.1-0.5％、甘油3.0-5.0％、玉米淀粉0.1-0.5％、苯甲酸钠0.01-0.1％、山梨酸钾0.01-0.1、聚乙二醇-400.2-0.8％、聚季铵盐-110.2-0.6％、变性乙醇5.0-10％、去离子水余量。
9.一种发质调理免洗喷雾的制备方法，包括以下步骤：
(1)将甘油、玉米淀粉、苯甲酸钠、山梨酸钾、聚乙二醇-40、聚季铵盐-11、去离子水搅拌微加热至55-60℃，溶解均匀，制得A相；
(2)将落地生根黄酮、凌霄花挥发油、老鹳草鞣质、变性乙醇混合溶解完全，制得B相；
(3)将B相加入A相，800-1300r/min速度下搅拌3-5min，搅拌均匀，出料。
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