CN107353872A - A kind of ceramic glue and preparation method thereof - Google Patents

A kind of ceramic glue and preparation method thereof Download PDF

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Publication number
CN107353872A
CN107353872A CN201710667538.1A CN201710667538A CN107353872A CN 107353872 A CN107353872 A CN 107353872A CN 201710667538 A CN201710667538 A CN 201710667538A CN 107353872 A CN107353872 A CN 107353872A
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CN
China
Prior art keywords
parts
preparation
fatty acid
titanium dioxide
butanediol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710667538.1A
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Chinese (zh)
Inventor
方碧水
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Individual
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Individual
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Priority to CN201710667538.1A priority Critical patent/CN107353872A/en
Publication of CN107353872A publication Critical patent/CN107353872A/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J201/00—Adhesives based on unspecified macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/04—Non-macromolecular additives inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/06—Non-macromolecular additives organic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2237—Oxides; Hydroxides of metals of titanium
    • C08K2003/2241—Titanium dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

The present invention relates to a kind of ceramic glue and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：20 35 parts of quartz sand, 10 13 parts of synthetic resin, 10 15 parts of butanediol, 59 parts of amino resins, 36 parts of phenolic resin, 68 parts of polyvinyl acetate emulsion, 8 11 parts of butyl p-hydroxybenzoate, 5 10 parts of the fatty acid ester compounded thing of higher alcohols, 35 parts of titanium dioxide.Material of the present invention is easy to get, and preparation method is simple, and cost is cheap, density is small, light weight, and degree of adhesion is high, great efforts are bonded, permeance property is good, waterproof and dampproof, high temperature resistant, there is certain flameproof effect and insulating properties, defoaming or still effect are good, rapid-curing cutback is realized, and can effectively realizes the bonding between the hard materials such as ceramics, metal, scope of application pipe, safe and non-toxic, environment protecting is good.

Description

A kind of ceramic glue and preparation method thereof
Technical field
The present invention relates to a kind of ceramic glue and preparation method thereof.
Background technology
Ceramic glue species in existing market is various, but all contains harmful substance in most ceramic adhesive, Complex manufacturing technology, achievable modern production cost is big, high into production cost, in addition, existing ceramic glue also has cohesive force not By force, the defects of permeance property difference.
The content of the invention
A kind of ceramic glue and preparation method thereof is provided the invention aims to overcome the shortcomings of the above.
Technical scheme includes：A kind of ceramic glue and preparation method thereof, raw material constituent in parts by weight by Following ratio composition：Quartz sand 20-35 parts, synthetic resin 10-13 parts, butanediol 10-15 parts, amino resins 5-9 parts, phenolic aldehyde Resin 3-6 parts, polyvinyl acetate emulsion 6-8 parts, butyl p-hydroxybenzoate 8-11 parts, the fatty acid ester compounded thing 5-10 of higher alcohols Part, titanium dioxide 3-5 parts.
Further improvement of the present invention is：Preferable raw material components, which match, is：32 parts of quartz sand, 12 parts of synthetic resin, 13 parts of butanediol, 7 parts of amino resins, 6 parts of phenolic resin, 8 parts of polyvinyl acetate emulsion, 10 parts of butyl p-hydroxybenzoate, height 6 parts of carbon polyol fatty acid ester complexes, 4 parts of titanium dioxide.
Further improvement of the present invention is：Its preparation method is as follows：
A, synthetic resin, amino resins and phenolic resin are subjected to high-temperature digestion stretching mixing establishment, temperature is set to 600-800 DEG C, it is cooled to after adding butanediol after room temperature, is stirred in the quartz sand added after crushing, stir speed (S.S.) 500-600r/ Min, obtain mixture A；
B, mixture A polyvinyl acetate emulsions are mixed, after stirring, is slowly added to middle addition P-hydroxybenzoic acid fourth Ester, add in three times to thick, obtain mixture B；
C, the fatty acid ester compounded thing of higher alcohols will be added in mixture B, adds titanium dioxide and carry out mixing to milky, Stir speed (S.S.) is 700-900r/min, carries out compacting packaging, obtains final product.
Beneficial effects of the present invention：
Material of the present invention is easy to get, and preparation method is simple, and cost is cheap, and density is small, light weight, and degree of adhesion is high, bonds great efforts, oozes Good, waterproof and dampproof, the high temperature resistant of permeability energy, has certain flameproof effect and insulating properties, and defoaming or still effect are good, realize speed Dry, and can effectively realizes the bonding between the hard materials such as ceramics, metal, and scope of application pipe is safe and non-toxic, and environment protecting is good.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of ceramic glue and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：20 parts of quartz sand, 10 parts of synthetic resin, 15 parts of butanediol, 7 parts of amino resins, 5 parts of phenolic resin, 8 parts of polyvinyl acetate emulsion, para hydroxybenzene first 6 parts of the fatty acid ester compounded thing of 8 parts of acid butyl ester, higher alcohols, 4 parts of titanium dioxide.
Its preparation method is as follows：
A, synthetic resin, amino resins and phenolic resin are subjected to high-temperature digestion stretching mixing establishment, temperature is set to 800 DEG C, cold But to after adding butanediol after room temperature, it is stirred, stir speed (S.S.) 580r/min, must mixes in the quartz sand added after crushing Thing A；
B, mixture A polyvinyl acetate emulsions are mixed, after stirring, is slowly added to middle addition P-hydroxybenzoic acid fourth Ester, add in three times to thick, obtain mixture B；
C, the fatty acid ester compounded thing of higher alcohols will be added in mixture B, adds titanium dioxide and carry out mixing to milky, Stir speed (S.S.) is 700r/min, carries out compacting packaging, obtains final product.
Embodiment 2
A kind of ceramic glue and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：32 parts of quartz sand, 12 parts of synthetic resin, 13 parts of butanediol, 7 parts of amino resins, 6 parts of phenolic resin, 8 parts of polyvinyl acetate emulsion, para hydroxybenzene first 6 parts of the fatty acid ester compounded thing of 10 parts of acid butyl ester, higher alcohols, 4 parts of titanium dioxide.
Its preparation method is as follows：
A, synthetic resin, amino resins and phenolic resin are subjected to high-temperature digestion stretching mixing establishment, temperature is set to 620 DEG C, cold But to after adding butanediol after room temperature, it is stirred, stir speed (S.S.) 540r/min, must mixes in the quartz sand added after crushing Thing A；
B, mixture A polyvinyl acetate emulsions are mixed, after stirring, is slowly added to middle addition P-hydroxybenzoic acid fourth Ester, add in three times to thick, obtain mixture B；
C, the fatty acid ester compounded thing of higher alcohols will be added in mixture B, adds titanium dioxide and carry out mixing to milky, Stir speed (S.S.) is 820r/min, carries out compacting packaging, obtains final product.
Embodiment 3
A kind of ceramic glue and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：25 parts of quartz sand, 11 parts of synthetic resin, 13 parts of butanediol, 7 parts of amino resins, 4 parts of phenolic resin, 7 parts of polyvinyl acetate emulsion, para hydroxybenzene first 6 parts of the fatty acid ester compounded thing of 9 parts of acid butyl ester, higher alcohols, 4 parts of titanium dioxide.
Its preparation method is as follows：
A, synthetic resin, amino resins and phenolic resin are subjected to high-temperature digestion stretching mixing establishment, temperature is set to 700 DEG C, cold But to after adding butanediol after room temperature, it is stirred, stir speed (S.S.) 520r/min, must mixes in the quartz sand added after crushing Thing A；
B, mixture A polyvinyl acetate emulsions are mixed, after stirring, is slowly added to middle addition P-hydroxybenzoic acid fourth Ester, add in three times to thick, obtain mixture B；
C, the fatty acid ester compounded thing of higher alcohols will be added in mixture B, adds titanium dioxide and carry out mixing to milky, Stir speed (S.S.) is 800r/min, carries out compacting packaging, obtains final product.
Embodiment 4
A kind of ceramic glue and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：35 parts of quartz sand, 13 parts of synthetic resin, 10 parts of butanediol, 5 parts of amino resins, 4 parts of phenolic resin, 7 parts of polyvinyl acetate emulsion, para hydroxybenzene first 6 parts of the fatty acid ester compounded thing of 9 parts of acid butyl ester, higher alcohols, 4 parts of titanium dioxide.
Its preparation method is as follows：
A, synthetic resin, amino resins and phenolic resin are subjected to high-temperature digestion stretching mixing establishment, temperature is set to 600 DEG C, cold But to after adding butanediol after room temperature, it is stirred, stir speed (S.S.) 600r/min, must mixes in the quartz sand added after crushing Thing A；
B, mixture A polyvinyl acetate emulsions are mixed, after stirring, is slowly added to middle addition P-hydroxybenzoic acid fourth Ester, add in three times to thick, obtain mixture B；
C, the fatty acid ester compounded thing of higher alcohols will be added in mixture B, adds titanium dioxide and carry out mixing to milky, Stir speed (S.S.) is 800r/min, carries out compacting packaging, obtains final product.
In above example, embodiment 2 is most preferred embodiment, bonds great efforts, and viscosity is high, and higher alcohols are fatty acid ester compounded Thing and and the order of addition of titanium dioxide is immutable, the quality, viscosity, usage time of product are had a certain impact, caused Quality it is dim, transparency is low, and viscosity is small, the set time length；Phenolic resin polyvinyl acetate emulsion is used cooperatively, and increase is viscous Degree, rapid-curing cutback is realized, foam time is fast after adding the fatty acid ester compounded thing of higher alcohols, and emulsifiability is good.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in Within protection scope of the present invention.

Claims (3)

  1. A kind of 1. ceramic glue and preparation method thereof, it is characterised in that：Raw material constituent is made up of following ratio in parts by weight： Quartz sand 20-35 parts, synthetic resin 10-13 parts, butanediol 10-15 parts, amino resins 5-9 parts, phenolic resin 3-6 parts, poly-vinegar Sour vac emulsion 6-8 parts, butyl p-hydroxybenzoate 8-11 parts, the fatty acid ester compounded thing 5-10 parts of higher alcohols, titanium dioxide 3-5 Part.
  2. A kind of 2. ceramic glue according to claim 1 and preparation method thereof, it is characterised in that：Preferable raw material components proportioning For：32 parts of quartz sand, 12 parts of synthetic resin, 13 parts of butanediol, 7 parts of amino resins, 6 parts of phenolic resin, polyvinyl acetate emulsion 8 parts, 10 parts of butyl p-hydroxybenzoate, 6 parts of the fatty acid ester compounded thing of higher alcohols, 4 parts of titanium dioxide.
  3. A kind of 3. ceramic glue according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method is as follows：
    A, synthetic resin, amino resins and phenolic resin are subjected to high-temperature digestion stretching mixing establishment, temperature is set to 600-800 DEG C, it is cooled to after adding butanediol after room temperature, is stirred in the quartz sand added after crushing, stir speed (S.S.) 500-600r/ Min, obtain mixture A；
    B, mixture A polyvinyl acetate emulsions are mixed, after stirring, is slowly added to middle addition P-hydroxybenzoic acid fourth Ester, add in three times to thick, obtain mixture B；
    C, the fatty acid ester compounded thing of higher alcohols will be added in mixture B, adds titanium dioxide and carry out mixing to milky, Stir speed (S.S.) is 700-900r/min, carries out compacting packaging, obtains final product.
CN201710667538.1A 2017-08-07 2017-08-07 A kind of ceramic glue and preparation method thereof Pending CN107353872A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710667538.1A CN107353872A (en) 2017-08-07 2017-08-07 A kind of ceramic glue and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710667538.1A CN107353872A (en) 2017-08-07 2017-08-07 A kind of ceramic glue and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107353872A true CN107353872A (en) 2017-11-17

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108341696A (en) * 2018-04-16 2018-07-31 广东金意陶陶瓷集团有限公司 A kind of surface is equipped with the porous ceramics dalle of lacquer coating
CN108374535A (en) * 2018-04-16 2018-08-07 广东金意陶陶瓷集团有限公司 A kind of ink-jet decorative porcelain plank and preparation method thereof
CN108382011A (en) * 2018-04-16 2018-08-10 广东金意陶陶瓷集团有限公司 A kind of film decorative porcelain plank and preparation method thereof
CN108396929A (en) * 2018-04-16 2018-08-14 广东金意陶陶瓷集团有限公司 A kind of composite ceramics plank and preparation method thereof
CN108396924A (en) * 2018-04-16 2018-08-14 广东金意陶陶瓷集团有限公司 A kind of porous ceramics dalle
CN108554752A (en) * 2018-04-16 2018-09-21 广东金意陶陶瓷集团有限公司 A kind of porous ceramics dalle and preparation method thereof with lacquer

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102408852A (en) * 2011-10-12 2012-04-11 厦门市金泰祥新科技有限公司 Multicomponent environment-friendly high temperature resistant adhesive used for energy saving lamp caps
CN106336845A (en) * 2016-08-22 2017-01-18 桂林新艺制冷设备有限责任公司 High temperature resistant adhesive and preparation method thereof
CN106366953A (en) * 2016-08-28 2017-02-01 梁乔保 High-temperature-resistant environment-friendly glue

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102408852A (en) * 2011-10-12 2012-04-11 厦门市金泰祥新科技有限公司 Multicomponent environment-friendly high temperature resistant adhesive used for energy saving lamp caps
CN106336845A (en) * 2016-08-22 2017-01-18 桂林新艺制冷设备有限责任公司 High temperature resistant adhesive and preparation method thereof
CN106366953A (en) * 2016-08-28 2017-02-01 梁乔保 High-temperature-resistant environment-friendly glue

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108341696A (en) * 2018-04-16 2018-07-31 广东金意陶陶瓷集团有限公司 A kind of surface is equipped with the porous ceramics dalle of lacquer coating
CN108374535A (en) * 2018-04-16 2018-08-07 广东金意陶陶瓷集团有限公司 A kind of ink-jet decorative porcelain plank and preparation method thereof
CN108382011A (en) * 2018-04-16 2018-08-10 广东金意陶陶瓷集团有限公司 A kind of film decorative porcelain plank and preparation method thereof
CN108396929A (en) * 2018-04-16 2018-08-14 广东金意陶陶瓷集团有限公司 A kind of composite ceramics plank and preparation method thereof
CN108396924A (en) * 2018-04-16 2018-08-14 广东金意陶陶瓷集团有限公司 A kind of porous ceramics dalle
CN108554752A (en) * 2018-04-16 2018-09-21 广东金意陶陶瓷集团有限公司 A kind of porous ceramics dalle and preparation method thereof with lacquer
CN108341696B (en) * 2018-04-16 2023-09-01 广东金意陶陶瓷集团有限公司 Porous ceramic decorative plate with real stone paint coating on surface
CN108396929B (en) * 2018-04-16 2023-09-29 广东金意陶陶瓷集团有限公司 Composite ceramic plate and preparation method thereof

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