CN107353772A - A kind of anti-corrosive paints of fire resistant doorsets and preparation method thereof - Google Patents

A kind of anti-corrosive paints of fire resistant doorsets and preparation method thereof Download PDF

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Publication number
CN107353772A
CN107353772A CN201710587320.5A CN201710587320A CN107353772A CN 107353772 A CN107353772 A CN 107353772A CN 201710587320 A CN201710587320 A CN 201710587320A CN 107353772 A CN107353772 A CN 107353772A
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China
Prior art keywords
parts
fire resistant
resistant doorsets
corrosive paints
resin
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Pending
Application number
CN201710587320.5A
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Chinese (zh)
Inventor
姜建磊
陈彬
高金艳
孙傲杰
陈健
姜金然
倪显亮
张恩海
刘雪飞
高俊龙
燕稼富
陈明才
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Funan County Civil Air Defense Engineering Equipment Co Ltd
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Funan County Civil Air Defense Engineering Equipment Co Ltd
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Priority to CN201710587320.5A priority Critical patent/CN107353772A/en
Publication of CN107353772A publication Critical patent/CN107353772A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D127/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
    • C09D127/02Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
    • C09D127/04Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
    • C09D127/06Homopolymers or copolymers of vinyl chloride
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D161/00Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
    • C09D161/04Condensation polymers of aldehydes or ketones with phenols only
    • C09D161/06Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04Polyurethanes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/02Flame or fire retardant/resistant
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

Abstract

A kind of anti-corrosive paints of fire resistant doorsets, it is related to fire resistant doorsets processing and fabricating technical field, it is characterised in that:It is made up of the material of following parts by weight, 18 23 parts of resin, 37 parts of defoamer, 48 parts of coupling agent, 13 parts of aerosil, 14 parts of modified graphene powder, 48 parts of polyvinylpyrrolidone, 13 parts of pigment, 10 14 parts of modification infusorial earth, 13 parts of marble dust, 33 38 parts of clear water.The inventive method is reasonable, manufacture craft is simple and clear, product decay resistance is good.

Description

A kind of anti-corrosive paints of fire resistant doorsets and preparation method thereof
Technical field
The present invention relates to fire resistant doorsets processing and fabricating technical field, and in particular to a kind of anti-corrosive paints of fire resistant doorsets and its Preparation method.
Background technology
Smoke-stop door, also known as fire resistant doorsets are fire integrities for maintaining escape route and provide the door of means of escape.Its Purpose was ensured that within one section of reasonable time (being typically escape time), protected the people to be escaped in escape route from fire The threat of calamity, including barrier dense smoke and heating power.
Accredited laboratory is specified by Ministry of Economic Affaris, according to the new edition fire resistant doorsets standard GB/T of implementation from 1 day January in 2009 _ 12955-2008, fire resistant doorsets fire resistance test method test passes, and obtain BSMI core hair checking login certificate and Authorize mark the knowledgeable, referred to as fire resistant doorsets.Fire resistant doorsets defined in U.S.'s NFPA and IBC specification are that " can provide opening portion jointly The combination of any fire-proof door leaf of a certain degree of flameproof protection, door cheek, hardware and other accessories.
Fire resistant doorsets refer to the door that can meet fire stability, integrality and thermal insulation requirement within a certain period of time.It is to set There are the fire protection separators of certain fire resistance in fire protection interval, emergency staircase, vertical shaft etc..
Fire resistant doorsets, can be one with more the effect for preventing fire spreading and flue gas diffusion in addition to having the function that common door The sprawling for the interior prevention intensity of a fire of fixing time, it is ensured that evacuating personnel.
And fire resistant doorsets are a kind of defense equipments, generally defense equipment will not all be changed often, thus Ask the waterproof, antidetonation, pressure-resistant, corrosion-resistant, corrosion resistant of equipment etc. various performances very good, but due to many Equipment is under some unconventional environment, such as extremely cold, very hot or ground end, due to environmental factor, often durability It is not just unusual height, is so easy for bringing potential safety hazard, causes many unnecessary troubles and danger.
The content of the invention
The technical problems to be solved by the invention be to overcome existing technological deficiency provide a kind of method rationally, make work Anti-corrosive paints of a kind of fire resistant doorsets that skill is simple and clear, product decay resistance is good and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme:
A kind of anti-corrosive paints of fire resistant doorsets, it is characterised in that:It is made up of the material of following parts by weight,
Resin 18-23 parts, defoamer 3-7 parts, coupling agent 4-8 parts, aerosil 1-3 parts, modified graphene powder 1-4 Part, polyvinylpyrrolidone 4-8 parts, pigment 1-3 parts, modification infusorial earth 10-14 parts, marble dust 1-3 parts, clear water 33-38 Part;
The resin is one kind in epoxy resin, phenolic resin, amino acid methyl ester, Corvic;
The defoamer is silicone emulsion, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polydimethylsiloxanes One kind in alkane;
The coupling agent is silane resin acceptor kh-550;
The pigment is one kind in titanium white, iron oxide red, aluminium powder, zinc powder;
The preparation method of the modification infusorial earth is:Diatomite is ground, 400-500 mesh sieves is crossed, adds 1.5 times of its weight Pure water, ester gum is added, 12-15 hour is stirred at room temperature, then dried, grind, obtain modification infusorial earth powder End;
The ester gum is 1 with diatomaceous mass ratio:1.2;
A kind of preparation method of the anti-corrosive paints of fire resistant doorsets is,
Resin, coupling agent, meteorological silica, modified graphene powder, modification infusorial earth and clear water are stirred 10 by I Minute, it is then placed in reactor and stirs at normal temperatures 20 minutes;
Material left after II stirring 5 minutes, then adds polyvinylpyrrolidone, marble dust, continues stirring 15 Minute;
Material left after III stirring 10 minutes, then adds pigment, is warming up to 40-45 DEG C, be stirred 2 hours i.e. Can;
The speed of the stirring is 2000-2500r/min.
Beneficial effects of the present invention are:Product, the corrosion resistance of product is made in material in the case of a series of mixing Can be superior, and there is certain fire protecting performance and humidity resistance, adhesive force is good, does not allow in the presence of external force easy to fall off. The inventive method is reasonable, manufacture craft is simple and clear, product decay resistance is good.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, enter below One step illustrates the present invention.
Embodiment 1
A kind of anti-corrosive paints of fire resistant doorsets, it is characterised in that:It is made up of the material of following parts by weight,
18 parts of resin, 3 parts of defoamer, 4 parts of coupling agent, 1 part of aerosil, 1 part of modified graphene powder, polyethylene pyrrole 4 parts of pyrrolidone, 1 part of pigment, 10 parts of modification infusorial earth, 1 part of marble dust, 33 parts of clear water;
The resin is one kind in epoxy resin, phenolic resin, amino acid methyl ester, Corvic;
The defoamer is silicone emulsion, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polydimethylsiloxanes One kind in alkane;
The coupling agent is silane resin acceptor kh-550;
The pigment is one kind in titanium white, iron oxide red, aluminium powder, zinc powder;
The preparation method of the modification infusorial earth is:Diatomite is ground, 400-500 mesh sieves is crossed, adds 1.5 times of its weight Pure water, ester gum is added, 12-15 hour is stirred at room temperature, then dried, grind, obtain modification infusorial earth powder End;
The ester gum is 1 with diatomaceous mass ratio:1.2;
A kind of preparation method of the anti-corrosive paints of fire resistant doorsets is,
Resin, coupling agent, meteorological silica, modified graphene powder, modification infusorial earth and clear water are stirred 10 by I Minute, it is then placed in reactor and stirs at normal temperatures 20 minutes;
Material left after II stirring 5 minutes, then adds polyvinylpyrrolidone, marble dust, continues stirring 15 Minute;
Material left after III stirring 10 minutes, then adds pigment, is warming up to 40-45 DEG C, be stirred 2 hours i.e. Can;
The speed of the stirring is 2000-2500r/min.
Embodiment 2
A kind of anti-corrosive paints of fire resistant doorsets, it is characterised in that:It is made up of the material of following parts by weight,
23 parts of resin, 7 parts of defoamer, 8 parts of coupling agent, 3 parts of aerosil, 4 parts of modified graphene powder, polyethylene pyrrole 8 parts of pyrrolidone, 3 parts of pigment, 14 parts of modification infusorial earth, 3 parts of marble dust, 38 parts of clear water;
The resin is one kind in epoxy resin, phenolic resin, amino acid methyl ester, Corvic;
The defoamer is silicone emulsion, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polydimethylsiloxanes One kind in alkane;
The coupling agent is silane resin acceptor kh-550;
The pigment is one kind in titanium white, iron oxide red, aluminium powder, zinc powder;
The preparation method of the modification infusorial earth is:Diatomite is ground, 400-500 mesh sieves is crossed, adds 1.5 times of its weight Pure water, ester gum is added, 12-15 hour is stirred at room temperature, then dried, grind, obtain modification infusorial earth powder End;
The ester gum is 1 with diatomaceous mass ratio:1.2;
A kind of preparation method of the anti-corrosive paints of fire resistant doorsets is,
Resin, coupling agent, meteorological silica, modified graphene powder, modification infusorial earth and clear water are stirred 10 by I Minute, it is then placed in reactor and stirs at normal temperatures 20 minutes;
Material left after II stirring 5 minutes, then adds polyvinylpyrrolidone, marble dust, continues stirring 15 Minute;
Material left after III stirring 10 minutes, then adds pigment, is warming up to 40-45 DEG C, be stirred 2 hours i.e. Can;
The speed of the stirring is 2000-2500r/min.
Embodiment 3
A kind of anti-corrosive paints of fire resistant doorsets, it is characterised in that:It is made up of the material of following parts by weight,
20 parts of resin, 5 parts of defoamer, 6 parts of coupling agent, 2 parts of aerosil, 3 parts of modified graphene powder, polyethylene pyrrole 7 parts of pyrrolidone, 1 part of pigment, 12 parts of modification infusorial earth, 3 parts of marble dust, 36 parts of clear water;
The resin is one kind in epoxy resin, phenolic resin, amino acid methyl ester, Corvic;
The defoamer is silicone emulsion, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polydimethylsiloxanes One kind in alkane;
The coupling agent is silane resin acceptor kh-550;
The pigment is one kind in titanium white, iron oxide red, aluminium powder, zinc powder;
The preparation method of the modification infusorial earth is:Diatomite is ground, 400-500 mesh sieves is crossed, adds 1.5 times of its weight Pure water, ester gum is added, 12-15 hour is stirred at room temperature, then dried, grind, obtain modification infusorial earth powder End;
The ester gum is 1 with diatomaceous mass ratio:1.2;
A kind of preparation method of the anti-corrosive paints of fire resistant doorsets is,
Resin, coupling agent, meteorological silica, modified graphene powder, modification infusorial earth and clear water are stirred 10 by I Minute, it is then placed in reactor and stirs at normal temperatures 20 minutes;
Material left after II stirring 5 minutes, then adds polyvinylpyrrolidone, marble dust, continues stirring 15 Minute;
Material left after III stirring 10 minutes, then adds pigment, is warming up to 40-45 DEG C, be stirred 2 hours i.e. Can;
The speed of the stirring is 2000-2500r/min.
Comparative example
A kind of coating includes:15 parts of epoxy resin, 5 parts of polyoxyethylene polyoxy propyl alcohol amidogen ether, 3 parts of silane coupler, poly- second 5 parts of alkene pyrrolidone, 1 part of pigment, 10 parts of diatomite, 30 parts of clear water;
Preparation method:Above-mentioned material is put into reactor and stirred at a temperature of 50-60 DEG C with 1000-1500r/min Mix 2 hours.
Determine performance, the effect such as following table of 1-3 of the embodiment of the present invention and comparative example:
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (8)

  1. A kind of 1. anti-corrosive paints of fire resistant doorsets, it is characterised in that:It is made up of the material of following parts by weight,
    Resin 18-23 parts, defoamer 3-7 parts, coupling agent 4-8 parts, aerosil 1-3 parts, modified graphene powder 1-4 parts, Polyvinylpyrrolidone 4-8 parts, pigment 1-3 parts, modification infusorial earth 10-14 parts, marble dust 1-3 parts, clear water 33-38 parts.
  2. A kind of 2. anti-corrosive paints of fire resistant doorsets according to claim 1, it is characterised in that:The resin is asphalt mixtures modified by epoxy resin One kind in fat, phenolic resin, amino acid methyl ester, Corvic.
  3. A kind of 3. anti-corrosive paints of fire resistant doorsets according to claim 1, it is characterised in that:The defoamer is emulsification One kind in silicone oil, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, dimethyl silicone polymer.
  4. A kind of 4. anti-corrosive paints of fire resistant doorsets according to claim 1, it is characterised in that:The coupling agent is silane Coupling agent KH-550.
  5. A kind of 5. anti-corrosive paints of fire resistant doorsets according to claim 1, it is characterised in that:The pigment be titanium white, One kind in iron oxide red, aluminium powder, zinc powder.
  6. A kind of 6. anti-corrosive paints of fire resistant doorsets according to claim 1, it is characterised in that:The modification infusorial earth Preparation method is:Diatomite is ground, 400-500 mesh sieves is crossed, adds 1.5 times of pure water of its weight, add ester gum, 12-15 hour is stirred at room temperature, then dries, grind, obtain modification infusorial earth powder.
  7. A kind of 7. anti-corrosive paints of fire resistant doorsets according to claim 6, it is characterised in that:The ester gum with Diatomaceous mass ratio is 1:1.2.
  8. A kind of 8. preparation method of the anti-corrosive paints of fire resistant doorsets according to claim 1, it is characterised in that:
    Resin, coupling agent, meteorological silica, modified graphene powder, modification infusorial earth and clear water are stirred 10 points by I Clock, it is then placed in reactor and stirs at normal temperatures 20 minutes;
    Material left after II stirring 5 minutes, then adds polyvinylpyrrolidone, marble dust, continues stirring 15 minutes;
    Material left after III stirring 10 minutes, then adds pigment, is warming up to 40-45 DEG C, be stirred 2 hours;
    The speed of the stirring is 2000-2500r/min.
CN201710587320.5A 2017-07-18 2017-07-18 A kind of anti-corrosive paints of fire resistant doorsets and preparation method thereof Pending CN107353772A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108410296A (en) * 2018-04-19 2018-08-17 合肥博创机械制造有限公司 A kind of mechanical equipment anticorrosive paint and preparation method thereof
CN110616033A (en) * 2019-10-30 2019-12-27 马鞍山市谷庆门业有限公司 Preparation method of flame-retardant low-odor wooden door coating
CN110643268A (en) * 2019-11-14 2020-01-03 陈保 Environment-friendly anticorrosive paint and preparation method thereof
CN113683949A (en) * 2021-09-16 2021-11-23 厦门铜宁消防材料有限公司 Preparation method of corrosion-resistant microporous fireproof coating

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106752576A (en) * 2016-12-13 2017-05-31 天长市巨龙车船涂料有限公司 A kind of watersoluble plumbago alkene metal anti-corrosive primer of UV resistant irradiation and preparation method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106752576A (en) * 2016-12-13 2017-05-31 天长市巨龙车船涂料有限公司 A kind of watersoluble plumbago alkene metal anti-corrosive primer of UV resistant irradiation and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108410296A (en) * 2018-04-19 2018-08-17 合肥博创机械制造有限公司 A kind of mechanical equipment anticorrosive paint and preparation method thereof
CN110616033A (en) * 2019-10-30 2019-12-27 马鞍山市谷庆门业有限公司 Preparation method of flame-retardant low-odor wooden door coating
CN110643268A (en) * 2019-11-14 2020-01-03 陈保 Environment-friendly anticorrosive paint and preparation method thereof
CN113683949A (en) * 2021-09-16 2021-11-23 厦门铜宁消防材料有限公司 Preparation method of corrosion-resistant microporous fireproof coating

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Application publication date: 20171117