CN107345103A - Preparation method for the anti-flaming dope of fire resisting timber door - Google Patents
Preparation method for the anti-flaming dope of fire resisting timber door Download PDFInfo
- Publication number
- CN107345103A CN107345103A CN201610301852.3A CN201610301852A CN107345103A CN 107345103 A CN107345103 A CN 107345103A CN 201610301852 A CN201610301852 A CN 201610301852A CN 107345103 A CN107345103 A CN 107345103A
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- CN
- China
- Prior art keywords
- preparation
- parts
- water
- fire resisting
- flaming dope
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D131/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
- C09D131/02—Homopolymers or copolymers of esters of monocarboxylic acids
- C09D131/04—Homopolymers or copolymers of vinyl acetate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/08—Polyesters modified with higher fatty oils or their acids, or with natural resins or resin acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/22—Halogen free composition
Abstract
The invention discloses the preparation method of the anti-flaming dope for fire resisting timber door, by water-base resin, two kinds of fire retardants, melamine, ammonium polyphosphate modifying, nano silicon, organic-silicon-modified styrene-acrylic emulsion, dispersant, defoamer, stabilizer, filler and water, which are prepared, to be formed, coating VOC content is low, not halogen-containing flame retardant, fire protecting performance is excellent, physicochemical property is excellent, strong carcinogenicity and poisonous gas and smog will not be produced by meeting fire, coating layer thickness is small, preparing raw material Environmental Safety, preparation method is simple and quick, can industrialization degree it is high, and apply it in the covering with paint of timber, on the premise of Environmental Safety, effectively increase the anti-flaming thermal-insulation fire protecting performance of wooden door, application of the wooden door in some places high to fire protection requirement is expanded significantly.
Description
Technical field
The present invention relates to the preparation field of wooden door, is especially for the preparation of the anti-flaming dope of fire resisting timber door
Method.
Background technology
As people's living standard improves constantly, to wooden door from basic decoration and demand for security gradually to more work(
It can seek development, common wooden door should also add some specific functions for specific field of employment, due to wood
This material of door is all wood, and its fire retardant performance is general all very poor, can increase when fire occurs
Danger, and heat-proof quality is poor.
Have at present and carry out making fire resistant doorsets using the timber of the preferable material of fire protecting performance, but its anti-flaming thermal-insulation performance
Or it is not good enough, and cost of material itself is also higher, carries out having the water-based of anti-flaming thermal-insulation performance on timber surface
The use of coating will solve the above problems.
Therefore, the water paint available for timber of a kind of anti-flaming thermal-insulation excellent performance and Environmental Safety how is prepared,
A kind of new technical scheme is needed to solve the above problems.
The content of the invention
Goal of the invention：The application demand that its anti-flaming thermal-insulation can not be expired to solve the timber material of prior art is asked
Topic, the present invention proposes that a kind of fire protection flame retarding heat-proof quality is all good and Environmental Safety is used for the fire-retardant of fire resisting timber door
The preparation method of coating.
Technical scheme：To achieve these objectives, the present invention takes following technical scheme：It is a kind of for fire resisting timber door
The preparation method of anti-flaming dope, it is characterised in that comprise the following steps：
(1) preparation of raw material：The preparing raw material calculated by mass for preparing following number：Water-base resin 20-40
Part, nano-meter flame retardantses 12-15 parts of polymer overmold, nitrogenated flame retardant 12-15 parts, melamine 6-10
Part, ammonium polyphosphate modifying 2-5 parts, nano silicon 1-3 parts, organic-silicon-modified styrene-acrylic emulsion 1-3
Part, dispersant 2-4 parts, defoamer 0.5-1 parts, stabilizer 1-2 parts, filler 4-6 parts, water 20-30
Part；
(2) it is water-base resin, the nano-meter flame retardantses of polymer overmold and nitrogenated flame retardant is first in a kettle
It is well mixed, the water of half amount is added, starts agitating function, disperses 10-15min；
(3) organic-silicon-modified styrene-acrylic emulsion is added into reactor to continue to be dispersed with stirring 10-15min, is heated
To 50-60 DEG C, cooled down after maintenance 20-30min stand-by；
(4) melamine, ammonium polyphosphate modifying, nano silicon, dispersant and filler are used into ball
Grinding machine carries out speed lapping and obtains powder mixture, rotating speed 3500r/min；
(5) it will be heated at 40-50 DEG C of the water of defoamer, stabilizer and surplus and be added to step after being well mixed
Suddenly in the reactor of the stand-by mixed solution of (3), and the powder mixture of step (4) is added, divided at a high speed
Required coating can be obtained by dissipating discharging packaging after disperseing 1-2h under machine.
Be more highly preferred to, in the step (1) water-base resin be water-based acrylic resin, aqueous acetic acid ethene-
One kind in acrylic resin, aqueous alkide resin.
It is more highly preferred to, dispersant is sodium polyphosphate, both wetting dispersing agent W-519 in the step (1)
Mass ratio is 3:1 mixture.
It is more highly preferred to, defoamer is defoamer A34 in the step (1).
It is more highly preferred to, the filler is that oxide powder and zinc, iron oxide red and titanium dioxide mass ratio are 1:2:1 it is mixed
Compound.
It is more highly preferred to, stabilizer is titanate coupling agent in the step (1).
It is more highly preferred to, the speed of stirring is 1000-1500r/min in the step (2).
It is more highly preferred to, jitter time is 2h in the step (4).
It is more highly preferred to, rate of dispersion is 4000r/min in the step (5).
Beneficial effect：The preparation method of a kind of anti-flaming dope for fire resisting timber door provided by the invention, by water-based
It is resin, two kinds of fire retardants, melamine, ammonium polyphosphate modifying, nano silicon, organic-silicon-modified
Styrene-acrylic emulsion, dispersant, defoamer, stabilizer, filler and water, which are prepared, to be formed, coating VOC content
Low, not halogen-containing flame retardant, fire protecting performance is excellent, and physicochemical property is excellent, and strong carcinogenicity will not be produced by meeting fire
With poisonous gas and smog, coating layer thickness is small, and preparing raw material Environmental Safety, preparation method is simple and quick, can work
Industry degree is high, and applies it in the covering with paint of timber, on the premise of Environmental Safety, effectively increases
The anti-flaming thermal-insulation fire protecting performance of wooden door, wooden door answering in some places high to fire protection requirement is expanded significantly
With.
Embodiment
Embodiment 1：
A kind of preparation method of anti-flaming dope for fire resisting timber door, comprises the following steps：
(1) preparation of raw material：The preparing raw material calculated by mass for preparing following number：20 parts of water-base resin,
6 parts of 12 parts of 12 parts of nano-meter flame retardantses, nitrogenated flame retardant, the melamine of polymer overmold, modified poly- phosphorus
Sour 2 parts of ammonium, 1 part of nano silicon, 1 part organic-silicon-modified of styrene-acrylic emulsion, 2 parts of dispersant, disappears
0.5 part of infusion, 1 part of stabilizer, 4 parts of filler, 20 parts of water；
(2) it is water-base resin, the nano-meter flame retardantses of polymer overmold and nitrogenated flame retardant is first in a kettle
It is well mixed, the water of half amount is added, starts agitating function, the speed of stirring is 1000r/min, disperses 15min；
(3) organic-silicon-modified styrene-acrylic emulsion is added into reactor to continue to be dispersed with stirring 10min, is heated to
50 DEG C, maintain 30min after cool down it is stand-by；
(4) melamine, ammonium polyphosphate modifying, nano silicon, dispersant and filler are used into ball
Grinding machine carries out speed lapping and obtains powder mixture, rotating speed 3500r/min, jitter time 2h；
(5) it will be heated at 40 DEG C of the water of defoamer, stabilizer and surplus and be added to step (3) after being well mixed
Stand-by mixed solution reactor in, and the powder mixture of step (4) is added, under high speed dispersor
Discharging packaging can obtain required coating, rate of dispersion 4000r/min after scattered 1h.
Wherein, water-base resin is that water-base resin is water-based acrylic resin in the step (1)；Dispersant is
Sodium polyphosphate, both wetting dispersing agent W-519 mass ratioes are 3:1 mixture；The defoamer is defoamer
A34；Filler is that oxide powder and zinc, iron oxide red and titanium dioxide mass ratio are 1:2:1 mixture；The stabilization
Agent is titanate coupling agent.
Embodiment 2：
A kind of preparation method of anti-flaming dope for fire resisting timber door, comprises the following steps：
(1) preparation of raw material：The preparing raw material calculated by mass for preparing following number：40 parts of water-base resin,
10 parts of 15 parts of 15 parts of nano-meter flame retardantses, nitrogenated flame retardant, the melamine of polymer overmold, modified poly- phosphorus
Sour 5 parts of ammonium, 3 parts of nano silicon, 3 parts organic-silicon-modified of styrene-acrylic emulsion, 4 parts of dispersant, disappears
1 part of infusion, 2 parts of stabilizer, 6 parts of filler, 30 parts of water；
(2) it is water-base resin, the nano-meter flame retardantses of polymer overmold and nitrogenated flame retardant is first in a kettle
It is well mixed, the water of half amount is added, starts agitating function, the speed of stirring is 1500r/min, disperses 10min；
(3) organic-silicon-modified styrene-acrylic emulsion is added into reactor to continue to be dispersed with stirring 15min, is heated to
60 DEG C, maintain 20min after cool down it is stand-by；
(4) melamine, ammonium polyphosphate modifying, nano silicon, dispersant and filler are used into ball
Grinding machine carries out speed lapping and obtains powder mixture, rotating speed 3500r/min, jitter time 2h；
(5) it will be heated at 50 DEG C of the water of defoamer, stabilizer and surplus and be added to step (3) after being well mixed
Stand-by mixed solution reactor in, and the powder mixture of step (4) is added, under high speed dispersor
Discharging packaging can obtain required coating, rate of dispersion 4000r/min after scattered 2h.
Wherein, water-base resin is that water-base resin is aqueous acetic acid ethylene-propylene acid resin in the step (1)；
Dispersant is sodium polyphosphate, both wetting dispersing agent W-519 mass ratioes are 3:1 mixture；The defoamer
For defoamer A34；Filler is that oxide powder and zinc, iron oxide red and titanium dioxide mass ratio are 1:2:1 mixture；
The stabilizer is titanate coupling agent.
Embodiment 3：
A kind of preparation method of anti-flaming dope for fire resisting timber door, comprises the following steps：
(1) preparation of raw material：The preparing raw material calculated by mass for preparing following number：30 parts of water-base resin,
7 parts of 14 parts of 13 parts of nano-meter flame retardantses, nitrogenated flame retardant, the melamine of polymer overmold, modified poly- phosphorus
Sour 4 parts of ammonium, 2 parts of nano silicon, 2 parts organic-silicon-modified of styrene-acrylic emulsion, 3 parts of dispersant, disappears
0.8 part of infusion, 1.5 parts of stabilizer, 5 parts of filler, 25 parts of water；
(2) it is water-base resin, the nano-meter flame retardantses of polymer overmold and nitrogenated flame retardant is first in a kettle
It is well mixed, the water of half amount is added, starts agitating function, the speed of stirring is 1200r/min, disperses 13min；
(3) organic-silicon-modified styrene-acrylic emulsion is added into reactor to continue to be dispersed with stirring 13min, is heated to
55 DEG C, maintain 25min after cool down it is stand-by；
(4) melamine, ammonium polyphosphate modifying, nano silicon, dispersant and filler are used into ball
Grinding machine carries out speed lapping and obtains powder mixture, rotating speed 3500r/min, jitter time 2h；
(5) it will be heated at 45 DEG C of the water of defoamer, stabilizer and surplus and be added to step (3) after being well mixed
Stand-by mixed solution reactor in, and the powder mixture of step (4) is added, under high speed dispersor
Discharging packaging can obtain required coating, rate of dispersion 4000r/min after scattered 1.5h.
Wherein, water-base resin is that water-base resin is aqueous alkide resin in the step (1)；Dispersant is more
Sodium phosphate, both wetting dispersing agent W-519 mass ratioes are 3:1 mixture；The defoamer is defoamer
A34；Filler is that oxide powder and zinc, iron oxide red and titanium dioxide mass ratio are 1:2:1 mixture；The stabilization
Agent is titanate coupling agent.
The anti-flaming dope prepared using the preparation method of the embodiment 1-3 anti-flaming dope for fire resisting timber door and general
It is applied in the covering with paint of timber, on the premise of Environmental Safety, effectively increases the anti-flaming thermal-insulation of wooden door
Fire protecting performance, application of the wooden door in some places high to fire protection requirement is expanded significantly.
It should be pointed out that for those skilled in the art, before the principle of the invention is not departed from
Put, some improvement can also be made, these improvement also should be regarded as protection scope of the present invention.
Claims (9)
1. the preparation method of the anti-flaming dope for fire resisting timber door, it is characterised in that comprise the following steps：
(1) preparation of raw material：The preparing raw material calculated by mass for preparing following number：Water-base resin 20-40
Part, nano-meter flame retardantses 12-15 parts of polymer overmold, nitrogenated flame retardant 12-15 parts, melamine 6-10
Part, ammonium polyphosphate modifying 2-5 parts, nano silicon 1-3 parts, organic-silicon-modified styrene-acrylic emulsion 1-3
Part, dispersant 2-4 parts, defoamer 0.5-1 parts, stabilizer 1-2 parts, filler 4-6 parts, water 20-30
Part；
(2) it is water-base resin, the nano-meter flame retardantses of polymer overmold and nitrogenated flame retardant is first in a kettle
It is well mixed, the water of half amount is added, starts agitating function, disperses 10-15min；
(3) organic-silicon-modified styrene-acrylic emulsion is added into reactor to continue to be dispersed with stirring 10-15min, is heated
To 50-60 DEG C, cooled down after maintenance 20-30min stand-by；
(4) melamine, ammonium polyphosphate modifying, nano silicon, dispersant and filler are used into ball
Grinding machine carries out speed lapping and obtains powder mixture, rotating speed 3500r/min；
(5) it will be heated at 40-50 DEG C of the water of defoamer, stabilizer and surplus and be added to step after being well mixed
Suddenly in the reactor of the stand-by mixed solution of (3), and the powder mixture of step (4) is added, divided at a high speed
Required coating can be obtained by dissipating discharging packaging after disperseing 1-2h under machine.
2. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：In the step (1) water-base resin be water-based acrylic resin, aqueous acetic acid ethylene-propylene acid resin,
One kind in aqueous alkide resin.
3. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：In the step (1) dispersant be sodium polyphosphate, both wetting dispersing agent W-519 mass ratioes be 3:1
Mixture.
4. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：Defoamer is defoamer A34 in the step (1).
5. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：The filler is that oxide powder and zinc, iron oxide red and titanium dioxide mass ratio are 1:2:1 mixture.
6. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：Stabilizer is titanate coupling agent in the step (1).
7. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：The speed of stirring is 1000-1500r/min in the step (2).
8. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：Jitter time is 2h in the step (4).
9. the preparation method of the anti-flaming dope according to claim 1 for fire resisting timber door, its feature exist
In：Rate of dispersion is 4000r/min in the step (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610301852.3A CN107345103A (en) | 2016-05-04 | 2016-05-04 | Preparation method for the anti-flaming dope of fire resisting timber door |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610301852.3A CN107345103A (en) | 2016-05-04 | 2016-05-04 | Preparation method for the anti-flaming dope of fire resisting timber door |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107345103A true CN107345103A (en) | 2017-11-14 |
Family
ID=60254256
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610301852.3A Withdrawn CN107345103A (en) | 2016-05-04 | 2016-05-04 | Preparation method for the anti-flaming dope of fire resisting timber door |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107345103A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109135577A (en) * | 2018-08-30 | 2019-01-04 | 湖州华尚家具有限公司 | A kind of fireproof coating of environmental wood door |
| CN109666189A (en) * | 2018-11-14 | 2019-04-23 | 芜湖市元奎新材料科技有限公司 | A kind of preparation process of flame-resistant resin material |
| CN111851070A (en) * | 2020-07-07 | 2020-10-30 | 巩义市泛锐熠辉复合材料有限公司 | Heat-insulating flame-retardant sheet and preparation method thereof |
| CN112647818A (en) * | 2020-12-17 | 2021-04-13 | 安徽银禾木业有限公司 | Preparation process of fireproof door |
-
2016
- 2016-05-04 CN CN201610301852.3A patent/CN107345103A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109135577A (en) * | 2018-08-30 | 2019-01-04 | 湖州华尚家具有限公司 | A kind of fireproof coating of environmental wood door |
| CN109666189A (en) * | 2018-11-14 | 2019-04-23 | 芜湖市元奎新材料科技有限公司 | A kind of preparation process of flame-resistant resin material |
| CN111851070A (en) * | 2020-07-07 | 2020-10-30 | 巩义市泛锐熠辉复合材料有限公司 | Heat-insulating flame-retardant sheet and preparation method thereof |
| CN112647818A (en) * | 2020-12-17 | 2021-04-13 | 安徽银禾木业有限公司 | Preparation process of fireproof door |
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Application publication date: 20171114 |
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