CN107338104A - Cold pressing processing method of tea seed oil - Google Patents

Cold pressing processing method of tea seed oil Download PDF

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Publication number
CN107338104A
CN107338104A CN201710783065.1A CN201710783065A CN107338104A CN 107338104 A CN107338104 A CN 107338104A CN 201710783065 A CN201710783065 A CN 201710783065A CN 107338104 A CN107338104 A CN 107338104A
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oil
tea
tea seed
processing method
seed oil
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CN201710783065.1A
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陈康健
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F5/00Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
    • C05F5/002Solid waste from mechanical processing of material, e.g. seed coats, olive pits, almond shells, fruit residue, rice hulls
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Microbiology (AREA)
  • Wood Science & Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Botany (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Molecular Biology (AREA)
  • Fats And Perfumes (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a tea seed oil cold pressing processing method, which comprises the following steps: removing impurities from tea seeds, cleaning, air drying until the shells of the tea seeds are cracked, and removing the shells to obtain tea seed kernels A; drying the tea seed kernels A, removing thin coats, and crushing to obtain tea seed powder B; rolling the tea seed powder B into a green body, and adding the green body into a cold squeezer for cold pressing to obtain crude oil C and an oil cake D; adding a decoloring agent into the crude oil C for decoloring, standing and filtering to obtain primary essential oil E; and (4) performing refrigerated centrifugal separation on the primary essential oil E to remove impurities, and finally performing molecular distillation separation to obtain the refined cold-pressed tea seed oil. The invention can effectively reduce the loss of grease, improve the oil yield and the quality of oil products and oil cakes, effectively retains the nutrient components of the tea seed oil by adopting a cold pressing processing method, and the obtained tea seed oil is natural, healthy, good in quality, good in color and luster and good in taste.

Description

A kind of tea seed oil cold press processing method
Technical field
The present invention relates to edible oil processing technique field, more particularly to a kind of tea seed oil cold press processing method.
Background technology
China is the native place of tealeaves, and existing tea place area is about 32,000,000 mu.The various in style of tea tree, distribution are wide, From 18 ° to 38 ° of north latitude, 94 ° to 122 ° of east longitude;Vertical distribution scope, highest is distributed to height above sea level 2600m mountain region, minimum to sea Pull out only several meters of low mound.Tea seeds are the fruits of the fruit of plant of theaceae tea, i.e. tea tree, are the by-product of Tea Production at present Product, as any other plant, tea seeds are the parts of whole tea tree most nutritive value in fact, and tea seeds are from blooming fruit It is real ripe, after the autumn, the winter, the spring, the summer, the autumn five seasons, growth cycle is up to more than 400 days, because its flowers and fruits is with the special landscape of branch, In the good reputation among the people for being known as " it is pregnant to embrace son ".Tea seed oil is to select in tea seeds fruit the seed benevolence grain being wrapped in by Pu, is squeezed out A kind of high-end woody health oil come.Detected through national authoritative institution, the unsaturated fatty acid content in tea seed oil is up to More than 82%, wherein linoleic acid content needed by human is about 3-6 times of olive oil, content of vitamin E is about the 5-10 of olive oil Times, also rich in a variety of powerful antioxidants such as Tea Polyphenols, phytosterol, carrotene, squalene, vitamin A, B, E and iron, zinc, The mineral matters such as magnesium, calcium.Tea seed oil is rich in more unrighted acid, is hypertension, heart disease, atherosclerosis, height The preferable health nutrient grease of blood fat patient.Tea seed oil Linoleic acid, linolenic ratio are even more the ratio that needed by human body is wanted. Tea seed oil is the only naturally edible oil rich in Tea Polyphenols, and Tea Polyphenols oxidation resistance is 18 times * 1 of vitamin E, no Only anti-aging, radioresistance, beauty and skin care, product even more are attained to anti arteriosclerosis, the natural of three high cardiovascular and cerebrovascular diseases of prevention.Tea Polyphenol content in leaf seed oil is up to 3000-10000ppm, and one spoonful of oil is equal to the Tea Polyphenols intake of 7 cups of Longjing teas.At present The advanced tea seed oil of listing is largely processed into using milling process, wherein, milling process is divided into low-temperature cold pressing and high-temperature high-pressure again Squeeze.In high temperature squeezing production process, due to the influence of high temperature, be highly vulnerable to breakage, decompose unrighted acid in oil product, oleic acid, A large amount of nutritional ingredients such as vitamin and trace element, and the color and luster for the tea seed oil produced, mouthfeel are not fine;And show Some cold pressing processing technologys, it is big difficulty of processing to be present, the problems such as low production efficiency, oil yield are low.Based on above statement, sheet Invention proposes a kind of tea seed oil cold press processing method.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of tea seed oil cold press proposed adds Work method.
A kind of tea seed oil cold press processing method, comprises the following steps:
S1, will after the fresh tea leaf seed impurity elimination of harvesting clean, be placed under the sun dry burst to tea seeds shell after, utilize stripping Start removes decapsidate, obtains tea seeds benevolence A;
S2, by step S1 gained tea seeds benevolence A be placed in drying box, through 78~95 DEG C of circulating air drying to moisture content After 0~8%, cold decortication removes tea seeds benevolence A thin coat, then adds in disintegrating machine, fully crushes to obtain tea seeds powder B;
S3, by step S2 gained tea seeds powder B add crushing roll in, strip plate be made thickness be 4~12mm green compact, by life Base adds cold press in cold pressing expeller and obtains crude oil C and oil cake D;
S4, in mass ratio 0.08~0.15:1, decolorising agent is added in step S3 in the crude oil C of gained, with 400~600r/ Min rotating speed, after being stirred 18~28min, filtering is stood, obtain just essential oil E processed;
S5, the first essential oil E processed of gained in step S4 added in refrigerated centrifuge, at a temperature of -9~-3 DEG C, freezing 18~ After 24h, centrifuged using rotating speed as 12000~15000r/min and go the removal of impurity, the refined cold press most separated afterwards through molecular distillation Tea seed oil.
Preferably, in the step S1 tea seeds impurity-removing method be magnetic separation, screening, selection by winnowing or specific-gravity winnowing in one kind or It is a variety of.
Preferably, oil cake D processing method processing methods include in the step S3:A, oil cake D is mashed into addition immersion, mistake Filter to obtain decontamination insecticidal solution;B, by oil cake together with fertilizer material retting, fertilizer is made;C, oil cake is mixed together with feedstuff Close, feed is made.
Preferably, the decolorising agent in the step S4 is that mass ratio is 2.2~4.5:1.2~1.8 active fruit shell carbon with The mixture of atlapulgite.
Preferably, the technological parameter of molecular distillation is in the step S5:Vacuum is 10~100Pa, feed rate 3 ~8ml/min, vapo(u)rizing temperature are 85~115 DEG C, and preheating temperature is 58~78 DEG C, and condensation temperature is 5~20 DEG C, and knifing rotating speed is 280~340r/min.
A kind of tea seed oil cold press processing method proposed by the present invention, grease loss can be effectively reduced, is improved fuel-displaced Rate, the quality of oil product and oil cake is improved, using cold press processing method, effectively avoid high temperature squeezing and destroy, decompose in oil product A large amount of nutritional ingredients such as unrighted acid, oleic acid, vitamin and trace element, cause the color and luster of tea seed oil, mouthfeel not The problems such as good, gained tea seed oil nutritional ingredient have obtained sufficient reservation, and the present invention uses active fruit shell carbon and atlapulgite Mixing cold press crude oil is decolourized, deodorizing process, the method then distilled using refrigerated centrifuge impurity elimination and hight atmospheric molecular Cold press crude oil is refined, gained tea seed oil natural health, quality is good, and color and luster is good, and mouthfeel is good, processing method letter of the present invention Single, production efficiency is high, and oil yield is high, and equipment investment is small, and production cost is low, is worthy to be popularized.
Embodiment
The present invention is made with reference to specific embodiment further to explain.
Embodiment one
A kind of tea seed oil cold press processing method proposed by the present invention, comprises the following steps:
S1, by the fresh tea leaf seed of harvesting after magnetic separation impurity elimination clean, be placed under the sun dry burst to tea seeds shell after, Decapsidate is removed using stripper, obtains tea seeds benevolence A;
S2, by step S1 gained tea seeds benevolence A be placed in drying box, through 78 DEG C of circulating air drying to moisture content be 3% Afterwards, cold decortication removes tea seeds benevolence A thin coat, then adds in disintegrating machine, fully crushes to obtain tea seeds powder B;
S3, the tea seeds powder B of gained in step S2 added in crushing roll, the green compact that thickness is 4mm are made in strip plate, by green compact plus Enter cold press in cold pressing expeller and obtain crude oil C and oil cake D;
S4, in mass ratio 0.08:1, it is 2.2 by mass ratio:1.2 active fruit shell carbon and the mixture of atlapulgite are added to step In rapid S3 in the crude oil C of gained, with 400r/min rotating speed, after being stirred 18min, filtering is stood, obtains just essential oil E processed;
S5, the first essential oil E processed of gained in step S4 added in refrigerated centrifuge, at a temperature of -9 DEG C, after freezing 18h, with Rotating speed is that the removal of impurity is gone in 12000r/min centrifugations, is finally 10Pa, feed rate 3ml/min in vacuum, distillation is warm Spend for 85 DEG C, preheating temperature is 58 DEG C, and condensation temperature is 5 DEG C, under conditions of knifing rotating speed is 280r/min, through molecular distillation point From refined cold press tea seed oil.
Embodiment two
A kind of tea seed oil cold press processing method proposed by the present invention, comprises the following steps:
S1, the fresh tea leaf seed of harvesting cleaned after specific-gravity winnowing impurity elimination, be placed in drying to tea seeds shell under the sun and fry After splitting, decapsidate is removed using stripper, obtains tea seeds benevolence A;
S2, by step S1 gained tea seeds benevolence A be placed in drying box, through 85 DEG C of circulating air drying to moisture content be 5% Afterwards, cold decortication removes tea seeds benevolence A thin coat, then adds in disintegrating machine, fully crushes to obtain tea seeds powder B;
S3, by step S2 gained tea seeds powder B add crushing roll in, strip plate be made thickness be 4~12mm green compact, by life Base adds cold press in cold pressing expeller and obtains crude oil C and oil cake D;
S4, in mass ratio 0.12:1, it is 3.2 by mass ratio:1.5 active fruit shell carbon and the mixture of atlapulgite are added to step In rapid S3 in the crude oil C of gained, with 500r/min rotating speed, after being stirred 24min, filtering is stood, obtains just essential oil E processed;
S5, the first essential oil E processed of gained in step S4 added in refrigerated centrifuge, at a temperature of -6 DEG C, after freezing 21h, with Rotating speed is that the removal of impurity is gone in 13500r/min centrifugations, is finally 50Pa, feed rate 5ml/min in vacuum, distillation is warm Spend for 100 DEG C, preheating temperature is 68 DEG C, and condensation temperature is 12 DEG C, under conditions of knifing rotating speed is 310r/min, through molecular distillation The refined cold press tea seed oil of separation.
Embodiment three
A kind of tea seed oil cold press processing method proposed by the present invention, comprises the following steps:
S1, by the fresh tea leaf seed of harvesting after screening impurity elimination clean, be placed under the sun dry burst to tea seeds shell after, Decapsidate is removed using stripper, obtains tea seeds benevolence A;
S2, by step S1 gained tea seeds benevolence A be placed in drying box, through 95 DEG C of circulating air drying to moisture content be 8% Afterwards, cold decortication removes tea seeds benevolence A thin coat, then adds in disintegrating machine, fully crushes to obtain tea seeds powder B;
S3, by step S2 gained tea seeds powder B add crushing roll in, strip plate be made thickness be 12mm green compact, by green compact Add cold press in cold pressing expeller and obtain crude oil C and oil cake D;
S4, in mass ratio 0.15:1, it is 4.5 by mass ratio:1.8 active fruit shell carbon and the mixture of atlapulgite are added to step In rapid S3 in the crude oil C of gained, with 600r/min rotating speed, after being stirred 28min, filtering is stood, obtains just essential oil E processed;
S5, the first essential oil E processed of gained in step S4 added in refrigerated centrifuge, at a temperature of -3 DEG C, after freezing 24h, with Rotating speed is that the removal of impurity is gone in 15000r/min centrifugations, is finally 100Pa, feed rate 8ml/min in vacuum, distillation is warm Spend for 115 DEG C, preheating temperature is 78 DEG C, and condensation temperature is 20 DEG C, under conditions of knifing rotating speed is 340r/min, through molecular distillation The refined cold press tea seed oil of separation.
It is existing with certain that a kind of tea seed oil cold press processing method proposed in the embodiment of the present invention one~tri- is respectively adopted Cold pressing processing technology, cold press processing is carried out to the tea seeds of phase homogenous quantities, oil yield is calculated respectively, draws following parameter:
Embodiment One Two Three Comparative example
Oil yield(%) 89.6 93.1 91.5 43.2
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, it is any Those familiar with the art the invention discloses technical scope in, technique according to the invention scheme and its invention Design is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (5)

1. a kind of tea seed oil cold press processing method, it is characterised in that comprise the following steps:
S1, will after the fresh tea leaf seed impurity elimination of harvesting clean, be placed under the sun dry burst to tea seeds shell after, utilize stripping Start removes decapsidate, obtains tea seeds benevolence A;
S2, by step S1 gained tea seeds benevolence A be placed in drying box, through 78~95 DEG C of circulating air drying to moisture content After 0~8%, cold decortication removes tea seeds benevolence A thin coat, then adds in disintegrating machine, fully crushes to obtain tea seeds powder B;
S3, by step S2 gained tea seeds powder B add crushing roll in, strip plate be made thickness be 4~12mm green compact, by life Base adds cold press in cold pressing expeller and obtains crude oil C and oil cake D;
S4, in mass ratio 0.08~0.15:1, decolorising agent is added in step S3 in the crude oil C of gained, with 400~600r/ Min rotating speed, after being stirred 18~28min, filtering is stood, obtain just essential oil E processed;
S5, the first essential oil E processed of gained in step S4 added in refrigerated centrifuge, at a temperature of -9~-3 DEG C, freezing 18~ After 24h, centrifuged using rotating speed as 12000~15000r/min and go the removal of impurity, the refined cold press most separated afterwards through molecular distillation Tea seed oil.
A kind of 2. tea seed oil cold press processing method according to claim 1, it is characterised in that tealeaves in the step S1 Seed impurity-removing method is the one or more in magnetic separation, screening, selection by winnowing or specific-gravity winnowing.
A kind of 3. tea seed oil cold press processing method according to claim 1, it is characterised in that oil cake in the step S3 D processing method processing methods include:A, oil cake D is mashed into addition immersion, filters to obtain decontamination insecticidal solution;B, it is oil cake and fertilizer is former Expect retting together, fertilizer is made;C, oil cake is mixed together with feedstuff, feed is made.
4. a kind of tea seed oil cold press processing method according to claim 1, it is characterised in that de- in the step S4 Toner is that mass ratio is 2.2~4.5:1.2~1.8 active fruit shell carbon and the mixture of atlapulgite.
A kind of 5. tea seed oil cold press processing method according to claim 1, it is characterised in that molecule in the step S5 The technological parameter of distillation is:Vacuum is 10~100Pa, and feed rate is 3~8ml/min, and vapo(u)rizing temperature is 85~115 DEG C, Preheating temperature is 58~78 DEG C, and condensation temperature is 5~20 DEG C, and knifing rotating speed is 280~340r/min.
CN201710783065.1A 2017-09-03 2017-09-03 Cold pressing processing method of tea seed oil Pending CN107338104A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109576049A (en) * 2018-11-30 2019-04-05 华南农业大学 A kind of tasteless tea oil and the preparation method and application thereof with high active ingredient

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102504938A (en) * 2011-11-08 2012-06-20 浙江省林业科学研究院 Cold pressing and physical refining process of camellia oil
CN103113987A (en) * 2013-03-06 2013-05-22 曹庸 Method for removing free fatty acid in tea oil by molecular distillation
CN103773594A (en) * 2014-01-20 2014-05-07 金华市农业科学研究院 Tea seed oil cold pressing method
CN105166088A (en) * 2015-08-09 2015-12-23 查光圣 Production technology of linseed oil

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102504938A (en) * 2011-11-08 2012-06-20 浙江省林业科学研究院 Cold pressing and physical refining process of camellia oil
CN103113987A (en) * 2013-03-06 2013-05-22 曹庸 Method for removing free fatty acid in tea oil by molecular distillation
CN103773594A (en) * 2014-01-20 2014-05-07 金华市农业科学研究院 Tea seed oil cold pressing method
CN105166088A (en) * 2015-08-09 2015-12-23 查光圣 Production technology of linseed oil

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109576049A (en) * 2018-11-30 2019-04-05 华南农业大学 A kind of tasteless tea oil and the preparation method and application thereof with high active ingredient

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Application publication date: 20171110