CN107312595A - A kind of grinding steel ball liquid and preparation method thereof - Google Patents
A kind of grinding steel ball liquid and preparation method thereof Download PDFInfo
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- CN107312595A CN107312595A CN201710482960.XA CN201710482960A CN107312595A CN 107312595 A CN107312595 A CN 107312595A CN 201710482960 A CN201710482960 A CN 201710482960A CN 107312595 A CN107312595 A CN 107312595A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/20—Rosin acids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
A kind of grinding steel ball liquid, be by the composition of mass parts：85 94 parts of aviation kerosine；15 parts of colophony powder；5 10 parts of organic corrosion inhibitor；13 parts of inorganic inhibitor；26 parts of triethanolamine；0.08 0.12 parts of white fused alumina.The preparation method of the grinding steel ball liquid is, by the composition of mass parts, aviation kerosine, colophony powder, antirust agent, borax, triethanolamine, white fused alumina are mixed, temperature of reaction kettle is controlled at 25 ± 5 DEG C, mixing control is at 10 20 revs/min, mixing time was controlled at 30 ± 10 minutes, you can grinding steel ball liquid is made.Beneficial effects of the present invention：The grinding steel ball liquid has certain viscosity, and greasy property is good, and cooling velocity is fast, and rust-preventing characteristic is good, easy cleaning, is difficult precipitation, greatlys save milling time, improves grinding efficiency, extends the service life of emery wheel, reduce production cost.Its preparation method is simple to operate, it is desirable to which temperature is low, is appropriate for industrialized production.
Description
Technical field
The present invention relates to a kind of grinding fluid, particularly a kind of steel ball oil base early grind liquid, and preparation method thereof belong to grinding fluid
And its preparing technical field.
Background technology
During grinding fluid is metal removal process, for cooling down and lubricating the industrial type fluid of cutter and workpiece,
It is generally divided into oil base grinding fluid and water-based milling liquid.Oil base grinding fluid is comprising matrix oil, oiliness improver, EP agent and other adds
Plus agent, its lubricity, rust-preventing characteristic be superior, but cooling effect is poor, not easy cleaning.Water-based milling liquid is generally lived by emulsion, surface
Property the chemical reagent such as agent and water composition, the cooling of water-based milling liquid, cleaning be good, but lubricity, rust-preventing characteristic far away from
Oil base grinding fluid.As mechanical industry develops to quick, strength, accurate direction, and also to meet continue to bring out all kinds of
The process requirements of superhard, superpower new material, requirement of the machinery industry to grinding process is improved constantly so that traditional oil base grinding
Liquid and water-based milling liquid can no longer meet requirement, it is necessary to a kind of new mill for having water-based milling liquid and oil base grinding fluid advantage concurrently
Cut liquid.
Steel ball is one of important composition part of ball bearing, is to be formed by the raw material of steel wire by mechanical cold-heading, grinding
's.The processing process of steel ball is from cold-heading, tarry matter, heat treatment, hard grind to early grind, lappingout.The grinding process of steel ball is with common
Work pieces process grinding process it is different, grinding steel ball be pass through under certain squeeze pressure mill template raceway carry out it is public
Turn and the rotation of steel ball itself is completed, so as to which steel ball is constantly polished, rounding, brighten, rather than general clamping is ground
Cut.
The content of the invention
The present invention is in view of the deficienciess of the prior art, i.e. oil base grinding fluid has lubricity good, but cooling is poor, difficult
That cleans has lubricity, rust-preventing characteristic slightly worse shortcoming, and water-based milling liquid, and easily by the shortcoming of bacteria effect.With reference to grinding
The process characteristic of steel ball is ground, by controlling the species of additive and carrying out ratio control, influence grinding process and Ball Mill is solved
The organic coordination of multiple influence factors of quality is cut, a kind of special grinding fluid of steel ball is obtained, the grinding fluid has greasy property good,
Cooling velocity is fast, and rust-preventing characteristic is good, the advantage of easy cleaning, solves above mentioned problem.
The technical scheme that the present invention solves above-mentioned technical problem is as follows：A kind of grinding steel ball liquid, be by the composition of mass parts：
85-94 parts of aviation kerosine；
1-5 parts of colophony powder；
5-10 parts of organic corrosion inhibitor；
1-3 parts of inorganic inhibitor；
2-6 parts of triethanolamine；
0.08-0.12 parts of white fused alumina.
Further,
88-92 parts of aviation kerosine；
2-3 parts of colophony powder；
7.5-8.5 parts of organic corrosion inhibitor；
1.2-2.5 parts of inorganic inhibitor；
3.5-4.4 parts of triethanolamine；
0.1-0.11 parts of white fused alumina.
Further, the organic corrosion inhibitor is one or both of BTA or decanedioic acid, preferably benzo three
Nitrogen azoles.
Further, the inorganic inhibitor is one or both of borax, 12 phosphomolybdate sodium, preferably borax.
Further, the white fused alumina particle diameter is 2.0-2.5um.Particle size is suitable, play suitable ablation and
Not free settling.
It is preferred that, a kind of grinding steel ball liquid is by the composition of mass parts：
90 parts of aviation kerosine；
2 parts of colophony powder；
8 parts of BTA；
2 parts of borax；
4 parts of triethanolamine；
0.1 part of white fused alumina.
The preparation method of grinding steel ball liquid of the present invention is, by the composition of mass parts, by aviation kerosine, colophony powder,
Antirust agent, borax, triethanolamine, white fused alumina mixing, temperature of reaction kettle are controlled at 25 ± 5 DEG C, and mixing control is at 10-20 revs/min
Clock, mixing time was controlled at 30 ± 10 minutes, you can grinding steel ball liquid is made.
Different composition roles and synergy in grinding steel ball liquid of the present invention：
(1) aviation kerosine, has permanent service life because of its efficient disinfection system；Good erosion resistance is low
Foam；Suitable for hard water and soft water, be conducive to extending life tools；Smell is gentle, can be received by majority operation personnel；Viscosity and profit
Slip can be good.
(2) work of white fused alumina always works under the rotation of high speed, can be to the cylindrical, interior of metal or non-metal workpiece
Circle, plane and various type faces etc. are roughly ground, half refines and fine grinding and fluting and cut-out etc..Existing steel ball grinding technology is usual
Using water-based milling liquid --- lapping liquid.We are dissolved into white fused alumina abrasive material particles micro mist in lapping liquid, due to white fused alumina
Grain abrasive micro-powder is difficult to be dissolved in the water, and is easily deposited to abrasive material bottom portion, and the particle washed away in steel ball surface is fewer, so
Steel ball grinding overlong time can be caused, not only wasted, and it is less efficient.Because this grinding fluid has certain viscosity, Bai Gang
Jade can suspend not free settling well.
(3) colophony powder, mainly containing rosin acid, to human body fanout free region, aviation kerosine is dissolved in this grinding fluid.It had been ground
Cheng Zhong, produces substantial amounts of heat, colophony powder absorbs and melted after heat, and is fully infiltrated into the microgroove of the higher steel ball surface of temperature, has
There is certain film forming, thus with certain waterproof action, viscosity is added in addition.But usage amount should not excessively or mistake
Few, when very few, using effect is not good, when excessive, and cementation is too big.
(4) organic corrosion inhibitor, BTA is dissolved in aviation kerosine in this grinding fluid, need not be added again when using
Emulsifying agent, greatly reduces the side effect that addition BTA is derived, is also more convenient cleaning.
(5) inorganic inhibitor, such as borax have antirust, antibacterial, extreme pressure, thickening effect in this grinding fluid.
(6) triethanolamine can effectively prevent from getting rusty in a short time.The appropriate amount of addition, with organic corrosion inhibitor, such as benzo three
Nitrogen azoles has collaboration anti-rust action, has with aviation kerosine and borax and cooperates with wear-resistant effect well.Triethanolamine is in this grinding fluid
In, the infiltration of this grinding fluid is can help to, is permeated in ground interface, so as to play the cooling and cleaning action of grinding fluid.
In summary, the invention has the advantages that：Grinding steel ball liquid of the present invention has certain viscosity,
Greasy property is good, and cooling velocity is fast, and rust-preventing characteristic is good, easy cleaning；White fused alumina micro powder granule is difficult precipitation in grinding fluid of the present invention,
Steel ball surface can be washed away repeatedly, the milling time of steel ball is greatlyd save, and improved steel ball grinding efficiency, reduced and be produced into
This.This oil base grinding fluid formation lubricating film so that the friction at interface mitigates, and prevents emery wheel friction wear and adhesion, extends sand
The service life of wheel, compared to water-based milling liquid, can preferably prevent steel ball surface degree of roughness from deteriorating.Steel of the present invention
The preparation method of ball grinding fluid, it is simple to operate, it is desirable to which that temperature is low, it is appropriate for industrialized production.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
The preparation method of grinding steel ball liquid of the present invention is, by the composition of mass parts, by aviation kerosine, colophony powder, organic
Antirust agent, inorganic inhibitor, triethanolamine, white fused alumina mixing, temperature of reaction kettle are controlled at 25 ± 5 DEG C, and mixing control is in 10-20
Rev/min, mixing time was controlled at 30 ± 10 minutes, you can grinding steel ball liquid is made.
Embodiment 1
A kind of grinding steel ball liquid, be by the composition of mass parts：
85 parts of aviation kerosine；
1 part of colophony powder；
5 parts of BTA；
2 parts of 12 phosphomolybdate sodium；
2 parts of triethanolamine；
0.12 part of white fused alumina, white fused alumina particle diameter is 2.0um.
Embodiment 2
A kind of grinding steel ball liquid, be by the composition of mass parts：
87 parts of aviation kerosine；
3 parts of colophony powder；
6 parts of BTA；
1 part of 12 phosphomolybdate sodium；
5 parts of triethanolamine；
0.08 part of white fused alumina, white fused alumina particle diameter is 2.2um.
Embodiment 3
A kind of grinding steel ball liquid, be by the composition of mass parts：
89 parts of aviation kerosine；
4 parts of colophony powder；
7 parts of decanedioic acid；
3 parts of borax；
6 parts of triethanolamine；
0.09 part of white fused alumina, white fused alumina particle diameter is 2.4um.
Embodiment 4
A kind of grinding steel ball liquid, be by the composition of mass parts：
94 parts of aviation kerosine；
5 parts of colophony powder；
10 parts of decanedioic acid；
1 part of borax；
3 parts of triethanolamine；
0.1 part of white fused alumina, white fused alumina particle diameter is 2.5um.
Embodiment 5
A kind of grinding steel ball liquid, be by the composition of mass parts：
90 parts of aviation kerosine；
2 parts of colophony powder；
8 parts of BTA；
2 parts of borax；
4 parts of triethanolamine；
0.1 part of white fused alumina, white fused alumina particle diameter is 2.3um.
Steel ball rotates the dynamic pressure for producing centrifugal force and air-flow during due to grinding so that grinding fluid is not easily accessible grinding
Area, it is therefore desirable to wash away steel ball surface repeatedly and be ground.This grinding fluid should have preferably cooling and lubrication, and be easy to
Emery wheel and steel ball are rinsed.Preferable lubrication is directly connected to the surface roughness and precision of steel ball and making for emery wheel
Use the life-span.In process of lapping cooling effect is played by the substantial amounts of heat of convection current and vaporization outflow of grinding fluid；Pass through addition
Other auxiliary agents complete the functions such as cleaning, antirust.
During using grinding fluid, scraper plate can be used, it would however also be possible to employ high pressure grinding fluid simultaneously passes through gas with higher jet velocity
Barrier, such as using less injection nozzle of sectional area, to ensure to have higher jet velocity under conditions of same traffic.
The test performance of above-mentioned 5 embodiments is as follows,
Viscosity (40 DEG C), mm2/s：102-130, modest viscosity.
Store security：Without layering, phase transformation and glue etc..
Rust-preventing characteristic is tested：The experiment of one-level grey cast-iron rust-preventing characteristic, the knot of 5 embodiments are carried out with reference to GB/T 6144-2010
Fruit is that the equal non-corroding phenomenon of one-level grey cast-iron piece, lustrous surface is for example new, reaches A grades of criterion of acceptability, and wherein embodiment 5 is anti-
Rust property is best.
Friction-wear test：Coefficient of friction on friction and wear tester (SRV-4) is equal<0.1500, lubricity is excellent,
When testing the service life of emery wheel, the processing quantity of 5 embodiment medium plain emery wheels reaches more than 1000.Wherein, embodiment 5
Coefficient of friction<0.1300, and the service life of emery wheel reaches more than 1500.
The foregoing is only presently preferred embodiments of the present invention, be not intended to limit the invention, it is all the present invention spirit and
Within principle, any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (6)
1. a kind of grinding steel ball liquid, it is characterised in that be by the composition of mass parts：
85-94 parts of aviation kerosine；
1-5 parts of colophony powder；
5-10 parts of organic corrosion inhibitor；
1-3 parts of inorganic inhibitor；
2-6 parts of triethanolamine；
0.08-0.12 parts of white fused alumina.
2. a kind of grinding steel ball liquid according to claim 1, it is characterised in that
88-92 parts of aviation kerosine；
2-3 parts of colophony powder；
7.5-8.5 parts of organic corrosion inhibitor；
1.2-2.5 parts of inorganic inhibitor；
3.5-4.4 parts of triethanolamine；
0.1-0.11 parts of white fused alumina.
3. a kind of grinding steel ball liquid according to claim 1, it is characterised in that the organic corrosion inhibitor is BTA
One or both of or decanedioic acid.
4. a kind of grinding steel ball liquid according to claim 1, it is characterised in that the inorganic inhibitor is borax, 12
One or both of sodium phosphomolybdate.
5. a kind of grinding steel ball liquid according to claim 1, it is characterised in that the white fused alumina particle diameter is 2.0-2.5um.
6. the preparation method of a kind of grinding steel ball liquid according to claim 1, it is characterised in that by the composition of mass parts,
Aviation kerosine, colophony powder, antirust agent, borax, triethanolamine, white fused alumina are mixed, temperature of reaction kettle is controlled at 25 ± 5 DEG C, is stirred
Control is mixed at 10-20 revs/min, mixing time was controlled at 30 ± 10 minutes, you can grinding steel ball liquid is made.
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| CN201710482960.XA CN107312595B (en) | 2017-06-22 | 2017-06-22 | Steel ball grinding fluid and preparation method thereof |
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| CN201710482960.XA CN107312595B (en) | 2017-06-22 | 2017-06-22 | Steel ball grinding fluid and preparation method thereof |
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| CN107312595B CN107312595B (en) | 2020-07-24 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107838424A (en) * | 2017-10-13 | 2018-03-27 | 苏州莱特复合材料有限公司 | A kind of processing method of the glossy decorations of ferrous based powder metallurgical |
| CN113403150A (en) * | 2021-06-22 | 2021-09-17 | 河南省紫风养护发展有限公司 | Method for cleaning, eliminating and killing air-conditioning pipeline of cigarette factory |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101139517A (en) * | 2007-07-24 | 2008-03-12 | 河南科技大学 | Bearing vibration-reducing chemical milling agent and method for using same |
| CN101423748A (en) * | 2008-12-10 | 2009-05-06 | 沈阳黎明航空发动机(集团)有限责任公司 | Liquid abrasive and preparation method thereof |
-
2017
- 2017-06-22 CN CN201710482960.XA patent/CN107312595B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101139517A (en) * | 2007-07-24 | 2008-03-12 | 河南科技大学 | Bearing vibration-reducing chemical milling agent and method for using same |
| CN101423748A (en) * | 2008-12-10 | 2009-05-06 | 沈阳黎明航空发动机(集团)有限责任公司 | Liquid abrasive and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107838424A (en) * | 2017-10-13 | 2018-03-27 | 苏州莱特复合材料有限公司 | A kind of processing method of the glossy decorations of ferrous based powder metallurgical |
| CN113403150A (en) * | 2021-06-22 | 2021-09-17 | 河南省紫风养护发展有限公司 | Method for cleaning, eliminating and killing air-conditioning pipeline of cigarette factory |
| CN113403150B (en) * | 2021-06-22 | 2022-07-05 | 河南省紫风养护发展有限公司 | Method for cleaning, killing and killing air-conditioning pipeline of cigarette factory |
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