CN107311607A - A kind of fire-proof mud and preparation method thereof - Google Patents
A kind of fire-proof mud and preparation method thereof Download PDFInfo
- Publication number
- CN107311607A CN107311607A CN201710667540.9A CN201710667540A CN107311607A CN 107311607 A CN107311607 A CN 107311607A CN 201710667540 A CN201710667540 A CN 201710667540A CN 107311607 A CN107311607 A CN 107311607A
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- China
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- parts
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- fire
- clay
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/30—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing magnesium cements or similar cements
- C04B28/32—Magnesium oxychloride cements, e.g. Sorel cement
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/90—Electrical properties
- C04B2111/92—Electrically insulating materials
Abstract
The present invention relates to a kind of fire-proof mud and preparation method thereof, raw material constituent is made up of following ratio by weight：30 50 parts of algae clay, 12 18 parts of magnesia, 38 parts of magnesium chloride, 15 20 parts of chlorinated paraffin, 8 10 parts of TBHQ, 10 20 parts of clay powder, 10 15 parts of photosensitive resin, 6 12 parts of floating bead, 38 parts of anti-flammability silica gel, 59 parts of synthetic mica, 6 10 parts of talcum powder, 35 parts of boron carbide, 10 18 parts of deionized water.Material of the present invention is easy to get, and preparation method is simple, with low cost, and fire endurance is high, drop low-smoke, postpones fuming rate, and good insulation preformance, viscosity is big, and density is small, hole-closing structure, and gas permeability is high, and moisture effect is good, applied widely.
Description
Technical field
The present invention relates to a kind of fire-proof mud and preparation method thereof.
Background technology
Continuing to develop and applying for electric energy is, double-edged sword, irreplaceable superiority to be brought to facilitate, another
Be convenient for people to must the fiery residence of vigilant generation, either relevant regulations, or people change inwardly, safety utilization of electric power
The topics common in epoch is had become, fire-proof mud is arisen at the historic moment, although technology is growing day by day, but fire-proof mud is in time, temperature
And certain limitation is still suffered from effect, while also there is the moisture absorption, smoke amount.
The content of the invention
A kind of fire-proof mud and preparation method thereof is provided the invention aims to overcome the shortcomings of the above.
Technical scheme includes：A kind of fire-proof mud and preparation method thereof, raw material constituent by weight by
Following ratio composition：30-50 parts of algae clay, 12-18 parts of magnesia, 3-8 parts of magnesium chloride, 15-20 parts of chlorinated paraffin, TBHQ 8-
10 parts, 10-20 parts of clay powder, 10-15 parts of photosensitive resin, 6-12 parts of floating bead, 3-8 parts of anti-flammability silica gel, 5-9 parts of synthetic mica,
6-10 parts of talcum powder, 3-5 parts of boron carbide, 10-18 parts of deionized water.
It is preferred that, its preparation method is as follows：
Under A, normal temperature and pressure, magnesia, magnesium chloride, chlorinated paraffin are mixed, stir speed (S.S.) is 800-850r/min,
Obtain mixture A；
B, clay powder, floating bead, synthetic mica, talcum powder and boron carbide mixed with deionized water, stir speed (S.S.) is 600-
Ultrasound in 700r/min, input ultrasonic machine, supersonic frequency is 2000-2500HZ, obtains mixture B；
C, will mixture B add algae clay in be stirred, add the photosensitive resin dissolved at 1000-1100 DEG C and anti-flammability
Silica gel, obtains mixture C；
D, mixture C added into TBHQ, add mixture A, be stirred, stir speed (S.S.) is 800-900r/min, compacting, drawn
Extend thick, obtain final product.
Beneficial effects of the present invention：
Material of the present invention is easy to get, and preparation method is simple, with low cost, and fire endurance is high, drop low-smoke, postpones fuming rate,
Good insulation preformance, viscosity is big, and density is small, hole-closing structure, and sealing is high, and moisture effect is good, and tensile capacity is strong, and hardness is big, is applicable
Scope is wide.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used
In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of fire-proof mud and preparation method thereof, raw material constituent is made up of following ratio by weight：35 parts of algae clay, oxygen
Change 16 parts of magnesium, 5 parts of magnesium chloride, 18 parts of chlorinated paraffin, 9 parts of TBHQ, 20 parts of clay powder, 14 parts of photosensitive resin, 10 parts of floating bead, resistance
5 parts of silica gel of combustion property, 4 parts of synthetic mica, 7 parts of talcum powder, 5 parts of boron carbide, 14 parts of deionized water.
Its preparation method is as follows：
Under A, normal temperature and pressure, magnesia, magnesium chloride, chlorinated paraffin are mixed, stir speed (S.S.) is 830r/min, obtain mixed
Compound A；
B, clay powder, floating bead, synthetic mica, talcum powder and boron carbide mixed with deionized water, stir speed (S.S.) is 620r/
Ultrasound in min, input ultrasonic machine, supersonic frequency is 2400HZ, obtains mixture B；
C, will mixture B add algae clay in be stirred, add the photosensitive resin dissolved at 1000 DEG C and anti-flammability silica gel,
Obtain mixture C；
D, mixture C added into TBHQ, add mixture A, be stirred, stir speed (S.S.) is 850r/min, suppress, be stretched to
It is thick, obtain final product.
Embodiment 2
A kind of fire-proof mud and preparation method thereof, raw material constituent is made up of following ratio by weight：30 parts of algae clay, oxygen
Change 13 parts of magnesium, it is 3 parts of magnesium chloride, 15 parts of chlorinated paraffin, 8 parts of TBHQ, 12 parts of clay powder, 13 parts of photosensitive resin, 8 parts of floating bead, fire-retardant
5 parts of silica gel of property, 6 parts of synthetic mica, 8 parts of talcum powder, 4 parts of boron carbide, 14 parts of deionized water.
Its preparation method is as follows：
Under A, normal temperature and pressure, magnesia, magnesium chloride, chlorinated paraffin are mixed, stir speed (S.S.) is 810r/min, obtain mixed
Compound A；
B, clay powder, floating bead, synthetic mica, talcum powder and boron carbide mixed with deionized water, stir speed (S.S.) is 660r/
Ultrasound in min, input ultrasonic machine, supersonic frequency is 2300HZ, obtains mixture B；
C, will mixture B add algae clay in be stirred, add the photosensitive resin dissolved at 1030 DEG C and anti-flammability silica gel,
Obtain mixture C；
D, mixture C added into TBHQ, add mixture A, be stirred, stir speed (S.S.) is 840r/min, suppress, be stretched to
It is thick, obtain final product.
Embodiment 3
A kind of fire-proof mud and preparation method thereof, raw material constituent is made up of following ratio by weight：40 parts of algae clay, oxygen
Change 14 parts of magnesium, 6 parts of magnesium chloride, 18 parts of chlorinated paraffin, 9 parts of TBHQ, 18 parts of clay powder, 15 parts of photosensitive resin, 12 parts of floating bead, resistance
8 parts of silica gel of combustion property, 9 parts of synthetic mica, 10 parts of talcum powder, 3 parts of boron carbide, 18 parts of deionized water.
Its preparation method is as follows：
Under A, normal temperature and pressure, magnesia, magnesium chloride, chlorinated paraffin are mixed, stir speed (S.S.) is 840r/min, obtain mixed
Compound A；
B, clay powder, floating bead, synthetic mica, talcum powder and boron carbide mixed with deionized water, stir speed (S.S.) is 620r/
Ultrasound in min, input ultrasonic machine, supersonic frequency is 2000HZ, obtains mixture B；
C, will mixture B add algae clay in be stirred, add the photosensitive resin dissolved at 1100 DEG C and anti-flammability silica gel,
Obtain mixture C；
D, mixture C added into TBHQ, add mixture A, be stirred, stir speed (S.S.) is 850r/min, suppress, be stretched to
It is thick, obtain final product.
Embodiment 4
A kind of fire-proof mud and preparation method thereof, raw material constituent is made up of following ratio by weight：45 parts of algae clay, oxygen
Change 12 parts of magnesium, 8 parts of magnesium chloride, 20 parts of chlorinated paraffin, 10 parts of TBHQ, 20 parts of clay powder, 10 parts of photosensitive resin, 12 parts of floating bead, resistance
8 parts of silica gel of combustion property, 9 parts of synthetic mica, 10 parts of talcum powder, 4 parts of boron carbide, 16 parts of deionized water.
Its preparation method is as follows：
Under A, normal temperature and pressure, magnesia, magnesium chloride, chlorinated paraffin are mixed, stir speed (S.S.) is 830r/min, obtain mixed
Compound A；
B, clay powder, floating bead, synthetic mica, talcum powder and boron carbide mixed with deionized water, stir speed (S.S.) is 680r/
Ultrasound in min, input ultrasonic machine, supersonic frequency is 2500HZ, obtains mixture B；
C, will mixture B add algae clay in be stirred, add 1000 time dissolve photosensitive resin and anti-flammability silica gel, obtain
Mixture C；
D, mixture C added into TBHQ, add mixture A, be stirred, stir speed (S.S.) is 900r/min, suppress, be stretched to
It is thick, obtain final product.
In above example, the order in step D can not be random, is related to the final result of experiment, such order product
Viscosity, fire protecting performance is more preferably；The combination of talcum powder and floating bead, not only improves self-lubricity, moreover it is possible to preferably extend fuming rate,
Fire protecting performance is improved, the addition of synthetic mica and boron carbide increases the hardness and tensile resistance of product, and insulation fire resistance property is carried
It is high.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area
For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc. should be included in
Within protection scope of the present invention.
Claims (2)
1. a kind of fire-proof mud and preparation method thereof, it is characterised in that：Raw material constituent is made up of following ratio by weight：
30-50 parts of algae clay, 12-18 parts of magnesia, 3-8 parts of magnesium chloride, 15-20 parts of chlorinated paraffin, 8-10 parts of TBHQ, clay powder 10-
20 parts, 10-15 parts of photosensitive resin, 6-12 parts of floating bead, 3-8 parts of anti-flammability silica gel, 5-9 parts of synthetic mica, 6-10 parts of talcum powder, carbon
Change 3-5 parts of boron, 10-18 parts of deionized water.
2. a kind of fire-proof mud according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method is as follows：
Under A, normal temperature and pressure, magnesia, magnesium chloride, chlorinated paraffin are mixed, stir speed (S.S.) is 800-850r/min,
Obtain mixture A；
B, clay powder, floating bead, synthetic mica, talcum powder and boron carbide mixed with deionized water, stir speed (S.S.) is 600-
Ultrasound in 700r/min, input ultrasonic machine, supersonic frequency is 2000-2500HZ, obtains mixture B；
C, will mixture B add algae clay in be stirred, add the photosensitive resin dissolved at 1000-1100 DEG C and anti-flammability
Silica gel, obtains mixture C；
D, mixture C added into TBHQ, add mixture A, be stirred, stir speed (S.S.) is 800-900r/min, compacting, drawn
Extend thick, obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710667540.9A CN107311607A (en) | 2017-08-07 | 2017-08-07 | A kind of fire-proof mud and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710667540.9A CN107311607A (en) | 2017-08-07 | 2017-08-07 | A kind of fire-proof mud and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107311607A true CN107311607A (en) | 2017-11-03 |
Family
ID=60170191
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710667540.9A Withdrawn CN107311607A (en) | 2017-08-07 | 2017-08-07 | A kind of fire-proof mud and preparation method thereof |
Country Status (1)
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| CN (1) | CN107311607A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108706924A (en) * | 2018-06-20 | 2018-10-26 | 江苏汉兴电缆有限公司 | A kind of cable insulation fire-proof mud |
-
2017
- 2017-08-07 CN CN201710667540.9A patent/CN107311607A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108706924A (en) * | 2018-06-20 | 2018-10-26 | 江苏汉兴电缆有限公司 | A kind of cable insulation fire-proof mud |
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Application publication date: 20171103 |