CN107308091A - A kind of pure natural sunscreen cream and preparation method thereof - Google Patents

A kind of pure natural sunscreen cream and preparation method thereof Download PDF

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Publication number
CN107308091A
CN107308091A CN201710513477.3A CN201710513477A CN107308091A CN 107308091 A CN107308091 A CN 107308091A CN 201710513477 A CN201710513477 A CN 201710513477A CN 107308091 A CN107308091 A CN 107308091A
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China
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weight
minutes
pure natural
supernatant
sunscreen cream
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CN201710513477.3A
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Chinese (zh)
Inventor
袁国防
李洪
孙明
王亮
宋辉
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Qingdao Haizhixing Biotechnology Co Ltd
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Qingdao Haizhixing Biotechnology Co Ltd
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Priority to CN201710513477.3A priority Critical patent/CN107308091A/en
Publication of CN107308091A publication Critical patent/CN107308091A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/004Aftersun preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/413Nanosized, i.e. having sizes below 100 nm
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

Abstract

The invention belongs to daily cosmetics technical field, more particularly to a kind of pure natural sunscreen cream;The invention further relates to a kind of preparation method of above-mentioned pure natural sunscreen cream.The pure natural sunscreen cream of the present invention is prepared from by following ingredients:Sponge gourd, Green Tea Leachate, tree peony, peach blossom, purslane, folium artemisiae argyi decoction liquor, chlorella powder, enteromorpha powder, dandelion, dragon fruit pericarp, nano-glass pearl powder, purified water, clear water, boiling water, saline solution.It is an advantage of the invention that obtained suncream has good antiultraviolet, repairs skin, the effect of delaying aging, and security is good, can anti-inflammation and sterilization, nourishes rough skin.

Description

A kind of pure natural sunscreen cream and preparation method thereof
Technical field
The invention belongs to daily cosmetics technical field, more particularly to a kind of pure natural sunscreen cream;The invention further relates to one Plant the preparation method of above-mentioned pure natural sunscreen cream.
Background technology
Summer is hot, and the ultraviolet in sunlight is the main cause for causing skin blackening and aging.According to the difference of wavelength, Ultraviolet is divided into three kinds:UVA, UVB and UVC.UVA is a kind of wavelength most long ultraviolet, not by the ozone layer on atmosphere top Absorb, skin corium can be penetrated, skin can be more goed deep into than UVB, make skin tanning, and cause lipid and collagen impaired, draw The light aging even cutaneum carcinoma of skin is played, so UVA can not only excite pigment synthesis and make the colour of skin " blackening ", skin is even more caused The main cause that skin " aging " and microgroove are produced.UVB is ultraviolet B radiation, its reachable skin corium, causes skin sun burn, The phenomenon such as erythema, tanned, but major part UVB absorbed by ozone layer, while can be obstructed by glass, parasols, clothes etc..UVC meetings Almost fully absorbed by atmosphere, only few situation can go up us and run into.
At present out of doors, prevent skin by ultraviolet injury generally by way of wiping suncream.But it is existing anti- It is chemical sunscreen frost to shine frost most, usually contains harmful chemical composition and heavy metal component, is easily caused allergic, is casted off a skin Deng adverse reaction.The sunscreen product containing ultra-violet absorber, which is used for a long time, may make skin sensitivity occur, and shouting pain is dry and astringent, angle Situations such as matter aging.With cosmetics to natural sex, security, scientific direction development, domestic and international manufacturer and consumption Person is increasingly strengthening the interest of natural sun-prevention cosmetics.At present, sun care preparations of the exploitation containing natural material has been hair Exhibition trend.Many natural materials such as pearl, plant etc. can play a part of it is sun-proof, brighten or nti-freckle and remove free radical, The effects such as some components also have anti-inflammation and sterilization, nourishes rough skin, if energy rational exploitation and utilization and compatibility can play good UV resistance Sun-proof interval big, the sensitization rate of line, reparation skin, the effect of delaying aging, and these natural sun-screening agents is low, security is good, because There are good market prospects and research and development to be worth for this.
The content of the invention
It is an object of the invention to provide a kind of pure natural sunscreen cream and preparation method thereof, obtained suncream has fine Antiultraviolet, repair skin, the effect of delaying aging, and security is good, can anti-inflammation and sterilization, nourishes rough skin.
In order to solve the above-mentioned technical problem, the present invention uses following technical scheme:A kind of preparation side of pure natural sunscreen cream Method, it comprises the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, is soaked 4-5 hours, green tea leaching is filtered to take Liquid;
(3) by tree peony and peach blossom according to 4-5:2 weight is chopped up than mixing, and it is the 25 of mixture gross mass to add weight Clear water again, is cooked by slow fire 20-25 minutes after being heated to boiling, obtains sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20- 25 minutes;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 2-3:1 weight ratio Mixing, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, is cooked by slow fire after being heated to boiling 10-15 minutes, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is that chlorella powder and enteromorpha powder are total to add quality 40% purified water of quality, is put into ultra low temperature freezer after mixing and preserves 12 hours, takes out, grinds on ice, adds in grinding Enter the saline solution that mass fraction is 0.5%, total matter of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition Amount;After grinding 30-40 minutes, the mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube, 5 points are centrifuged Clock, takes supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment grinds 20-30 Ultrasonication 15 minutes after minute, is then transferred in centrifuge tube, centrifuges 5 minutes, takes supernatant, merges the upper of gained twice Clear liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the matter of dragon fruit pericarp and dandelion Amount is than being 5-6:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5) The supernatant obtained by folium artemisiae argyi decoction liquor, step (7) obtained by liquid, step (6) is according to 2:10-12:1:4-5:2 mass ratio is mixed Close, with magnetic stirrer 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) mass ratio of the mixture obtained by the step of mixture obtained by and addition (10) is 1:8-10, magnetic force is used after being well mixed Agitator is stirred 30-40 minutes, is transferred in centrifuge tube, is centrifuged, is abandoned sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 2:At 3-4 ratio mixing, ultrasonic wave Reason 20 minutes, produces object.
The invention also discloses the pure natural sunscreen cream obtained by a kind of above-mentioned preparation method.
It should be noted that:Pure natural sunscreen cream of the pregnant woman especially obtained by the habitual abortion person disabling present invention.
The pure natural sunscreen cream of the present invention has isolation anti-sunlight function well, passes through each component of the above-mentioned steps present invention Between be tightly combined, the effect of antiultraviolet can be played for a long time, sun-proof result is good, and the sun-proof time is long.
The active ingredient of each component can dramatically be played with above-mentioned compatibility and preparation method, with good skin care effect Really, interreaction between the active ingredient of each component, obtained pure natural sunscreen cream has sun-proof and nourishes rough skin effect concurrently.
Pure natural sunscreen cream obtained by the present invention has natural plant flavour, chlorella powder, enteromorpha powder and pearl The fishy smell of powder is covered by the fragrance of tree peony, peach blossom, folium artemisiae argyi, green tea, product -- the pure day of the invention of each component mixing and reaction Right suncream fragrance is without pungent, and compatibility of the present invention is reasonable, the active ingredient in reasonable drawing chlorella powder and enteromorpha powder, Chlorella powder, enteromorpha powder and pearl powder is given full play to act on the maintenance of skin, and tree peony, peach blossom, folium artemisiae argyi, green tea Nourishing anti-allergic effects can greatly play, and can improve the pure natural sun-proof of the present invention in addition with aforementioned proportion compatibility The gas permeability of frost.
Each raw material components Nantural non-toxic side effect of the present invention, is difficult to cause allergic reaction, therefore security is good, can be long-term Use.
Pure natural sunscreen cream obtained by the present invention has the effect of nourishes rough skin, is used for a long time to have and repairs skin, prolongs The effect of slow aging, can be effectively improved skin.
Pure natural sunscreen cream good permeability obtained by the present invention, pure natural plant nourishes composition and easily inhaled by skin Receive, freely breathing for skin is also helped while nourishes rough skin, will not feel greasy and sultry after smearing, use compared with To be salubrious.
By steps such as mixing and ultrasonications, nano-glass pearl powder is sufficiently solubilized in the supernatant obtained by step (11) In liquid, the pure natural sunscreen cream obtained by the present invention is easy to be smeared uniform, using more convenient.
Further, in step (3), tree peony and peach blossom are according to 2:1 weight is than mixing.
Further, in step (9), the mass ratio of dragon fruit pericarp and dandelion is 6:1.
Further, in step (10), by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), step Suddenly the folium artemisiae argyi decoction liquor obtained by supernatant obtained by (5), step (6), the supernatant obtained by step (7) are according to 2:10:1:5:2 Mass ratio was mixed, with magnetic stirrer 30-40 minutes.
Further, in step (11), mixture the step of mixture obtained by step (9) and addition obtained by (10) Mass ratio is 1:9.
Further, in step (12), nano-glass pearl powder is with the supernatant obtained by step (11) according to 2:3 ratio is mixed Close.
Compared with prior art, the beneficial effects of the invention are as follows:
(1) pure natural sunscreen cream of the invention has isolation anti-sunlight function well, passes through each of the above-mentioned steps present invention It is tightly combined between component, the effect of antiultraviolet can be played for a long time, sun-proof result is good, and the sun-proof time is long.
(2) active ingredient of each component can dramatically be played with the compatibility and preparation method of the present invention, with fine Skin effect, interreaction between the active ingredient of each component, obtained pure natural sunscreen cream has concurrently sun-proof and nourishes skin The effect of skin.
(3) pure natural sunscreen cream obtained by the present invention has natural plant flavour, chlorella powder, enteromorpha powder and treasure The fishy smell of pearl powder is covered by the fragrance of tree peony, peach blossom, folium artemisiae argyi, green tea, each component mixing and reaction product -- of the invention is pure Natural sun cream fragrance is without pungent, and compatibility of the present invention is reasonable, in reasonable drawing chlorella powder and enteromorpha powder it is effective into Point, give full play to chlorella powder, enteromorpha powder and pearl powder and the maintenance of skin has been acted on, and it is tree peony, peach blossom, folium artemisiae argyi, green The nourishing anti-allergic effects of tea can be played greatly, can improve the pure natural of the present invention in addition with aforementioned proportion compatibility The gas permeability of suncream.
(4) each raw material components Nantural non-toxic side effect of the invention, is difficult to cause allergic reaction, therefore security is good, can It is used for a long time.
(5) pure natural sunscreen cream obtained by the present invention has the effect of nourishes rough skin, be used for a long time have repair skin, The effect of delaying aging, can be effectively improved skin.
(6) the pure natural sunscreen cream good permeability obtained by the present invention, pure natural plant nourishes composition easily by skin Absorb, freely breathing for skin is also helped while nourishes rough skin, will not feel greasy and sultry after smearing, use It is more salubrious.
(7) by steps such as mixing and ultrasonications, nano-glass pearl powder is sufficiently solubilized obtained by step (11) In supernatant, the pure natural sunscreen cream obtained by the present invention is easy to be smeared uniform, using more convenient.
Embodiment
Following embodiment facilitates a better understanding of the present invention, but does not limit the present invention.Experiment in following embodiments Method, is conventional method unless otherwise specified.
Embodiment 1
A kind of preparation method of pure natural sunscreen cream, it comprises the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, is soaked 4-5 hours, green tea leaching is filtered to take Liquid;
(3) by tree peony and peach blossom according to 2:1 weight is chopped up than mixing, and addition weight is 25 times of mixture gross mass Clear water, be heated to boiling after be cooked by slow fire 20-25 minutes, obtain sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20- 25 minutes;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 2:1 weight is than mixed Close, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, is cooked by slow fire after being heated to boiling 10-15 minutes, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is that chlorella powder and enteromorpha powder are total to add quality 40% purified water of quality, is put into ultra low temperature freezer after mixing and preserves 12 hours, takes out, grinds on ice, adds in grinding Enter the saline solution that mass fraction is 0.5%, total matter of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition Amount;After grinding 30-40 minutes, the mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube, 5 points are centrifuged Clock, takes supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment grinds 20-30 Ultrasonication 15 minutes after minute, is then transferred in centrifuge tube, centrifuges 5 minutes, takes supernatant, merges the upper of gained twice Clear liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the matter of dragon fruit pericarp and dandelion Amount is than being 6:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5) The supernatant obtained by folium artemisiae argyi decoction liquor, step (7) obtained by liquid, step (6) is according to 2:10:1:5:2 mass ratio mixing, uses magnetic Power agitator is stirred 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) mass ratio of the mixture obtained by the step of mixture obtained by and addition (10) is 1:9, use magnetic agitation after being well mixed Device is stirred 30-40 minutes, is transferred in centrifuge tube, is centrifuged, is abandoned sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 2:3 part by weight mixing, ultrasonic wave Processing 20 minutes, produces object.
A kind of pure natural sunscreen cream obtained by above-mentioned preparation method.
Embodiment 2
A kind of preparation method of pure natural sunscreen cream, it comprises the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, is soaked 4-5 hours, green tea leaching is filtered to take Liquid;
(3) by tree peony and peach blossom according to 5:2 weight is chopped up than mixing, and addition weight is 25 times of mixture gross mass Clear water, be heated to boiling after be cooked by slow fire 20-25 minutes, obtain sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20- 25 minutes;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 3:1 weight is than mixed Close, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, is cooked by slow fire after being heated to boiling 10-15 minutes, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is that chlorella powder and enteromorpha powder are total to add quality 40% purified water of quality, is put into ultra low temperature freezer after mixing and preserves 12 hours, takes out, grinds on ice, adds in grinding Enter the saline solution that mass fraction is 0.5%, total matter of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition Amount;After grinding 30-40 minutes, the mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube, 5 points are centrifuged Clock, takes supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment grinds 20-30 Ultrasonication 15 minutes after minute, is then transferred in centrifuge tube, centrifuges 5 minutes, takes supernatant, merges the upper of gained twice Clear liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the matter of dragon fruit pericarp and dandelion Amount is than being 5:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5) The supernatant obtained by folium artemisiae argyi decoction liquor, step (7) obtained by liquid, step (6) is according to 2:12:1:4:2 mass ratio mixing, uses magnetic Power agitator is stirred 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) mass ratio of the mixture obtained by the step of mixture obtained by and addition (10) is 1:8, use magnetic agitation after being well mixed Device is stirred 30-40 minutes, is transferred in centrifuge tube, is centrifuged, is abandoned sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 2:3 part by weight mixing, ultrasonic wave Processing 20 minutes, produces object.
A kind of pure natural sunscreen cream obtained by above-mentioned preparation method.
Embodiment 3
A kind of preparation method of pure natural sunscreen cream, it comprises the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, is soaked 4-5 hours, green tea leaching is filtered to take Liquid;
(3) by tree peony and peach blossom according to 5:2 weight is chopped up than mixing, and addition weight is 25 times of mixture gross mass Clear water, be heated to boiling after be cooked by slow fire 20-25 minutes, obtain sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20- 25 minutes;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 2:1 weight is than mixed Close, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, is cooked by slow fire after being heated to boiling 10-15 minutes, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is that chlorella powder and enteromorpha powder are total to add quality 40% purified water of quality, is put into ultra low temperature freezer after mixing and preserves 12 hours, takes out, grinds on ice, adds in grinding Enter the saline solution that mass fraction is 0.5%, total matter of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition Amount;After grinding 30-40 minutes, the mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube, 5 points are centrifuged Clock, takes supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment grinds 20-30 Ultrasonication 15 minutes after minute, is then transferred in centrifuge tube, centrifuges 5 minutes, takes supernatant, merges the upper of gained twice Clear liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the matter of dragon fruit pericarp and dandelion Amount is than being 5:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5) The supernatant obtained by folium artemisiae argyi decoction liquor, step (7) obtained by liquid, step (6) is according to 2:10:1:5:2 mass ratio mixing, uses magnetic Power agitator is stirred 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) mass ratio of the mixture obtained by the step of mixture obtained by and addition (10) is 1:10, stirred after being well mixed with magnetic force Mix device to stir 30-40 minutes, be transferred in centrifuge tube, centrifuge, abandon sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 1:2 part by weight mixing, ultrasonic wave Processing 20 minutes, produces object.
A kind of pure natural sunscreen cream obtained by above-mentioned preparation method.
Embodiment 4
A kind of preparation method of pure natural sunscreen cream, it comprises the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, is soaked 4-5 hours, green tea leaching is filtered to take Liquid;
(3) by tree peony and peach blossom according to 2:1 weight is chopped up than mixing, and addition weight is 25 times of mixture gross mass Clear water, be heated to boiling after be cooked by slow fire 20-25 minutes, obtain sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20- 25 minutes;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 3:1 weight is than mixed Close, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, is cooked by slow fire after being heated to boiling 10-15 minutes, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is that chlorella powder and enteromorpha powder are total to add quality 40% purified water of quality, is put into ultra low temperature freezer after mixing and preserves 12 hours, takes out, grinds on ice, adds in grinding Enter the saline solution that mass fraction is 0.5%, total matter of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition Amount;After grinding 30-40 minutes, the mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube, 5 points are centrifuged Clock, takes supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment grinds 20-30 Ultrasonication 15 minutes after minute, is then transferred in centrifuge tube, centrifuges 5 minutes, takes supernatant, merges the upper of gained twice Clear liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the matter of dragon fruit pericarp and dandelion Amount is than being 6:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5) The supernatant obtained by folium artemisiae argyi decoction liquor, step (7) obtained by liquid, step (6) is according to 2:12:1:5:2 mass ratio mixing, uses magnetic Power agitator is stirred 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) mass ratio of the mixture obtained by the step of mixture obtained by and addition (10) is 1:8-10, magnetic force is used after being well mixed Agitator is stirred 30-40 minutes, is transferred in centrifuge tube, is centrifuged, is abandoned sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 2:3 ratio mixing, ultrasonication 20 minutes, produce object.
A kind of pure natural sunscreen cream obtained by above-mentioned preparation method.
Embodiment 5
A kind of preparation method of pure natural sunscreen cream, it comprises the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, is soaked 4-5 hours, green tea leaching is filtered to take Liquid;
(3) by tree peony and peach blossom according to 5:2 weight is chopped up than mixing, and addition weight is 25 times of mixture gross mass Clear water, be heated to boiling after be cooked by slow fire 20-25 minutes, obtain sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20- 25 minutes;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 3:1 weight is than mixed Close, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, is cooked by slow fire after being heated to boiling 10-15 minutes, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is that chlorella powder and enteromorpha powder are total to add quality 40% purified water of quality, is put into ultra low temperature freezer after mixing and preserves 12 hours, takes out, grinds on ice, adds in grinding Enter the saline solution that mass fraction is 0.5%, total matter of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition Amount;After grinding 30-40 minutes, the mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube, 5 points are centrifuged Clock, takes supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment grinds 20-30 Ultrasonication 15 minutes after minute, is then transferred in centrifuge tube, centrifuges 5 minutes, takes supernatant, merges the upper of gained twice Clear liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the matter of dragon fruit pericarp and dandelion Amount is than being 5:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5) The supernatant obtained by folium artemisiae argyi decoction liquor, step (7) obtained by liquid, step (6) is according to 2:10:1:5:2 mass ratio mixing, uses magnetic Power agitator is stirred 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) mass ratio of the mixture obtained by the step of mixture obtained by and addition (10) is 1:9, use magnetic agitation after being well mixed Device is stirred 30-40 minutes, is transferred in centrifuge tube, is centrifuged, is abandoned sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 2:3 ratio mixing, ultrasonication 20 minutes, produce object.
A kind of pure natural sunscreen cream obtained by above-mentioned preparation method.
Described above is only the preferred embodiment of the present invention, it should be pointed out that:For the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvement can also be made, these improvement should be regarded as the guarantor of the present invention Protect scope.

Claims (7)

1. a kind of preparation method of pure natural sunscreen cream, it is characterised in that:Comprise the following steps:
(1) by fresh loofah peeling, clean, squeeze the juice, obtain Sucus Luffae;
(2) 30 times of the boiling water that weight is green tea weight is added into green tea, soaks 4-5 hours, filters to take Green Tea Leachate;
(3) by tree peony and peach blossom according to 4-5:2 weight is chopped up than mixing, and addition weight is 25 times of mixture gross mass Clear water, is cooked by slow fire 20-25 minutes after being heated to boiling, obtains sticky juice;
(4) fresh purslane is cleaned, chopped up, added 12 times of the clear water that weight is purslane weight, be cooked by slow fire 20-25 points Clock;
(5) by the decoction mixture obtained by the sticky juice obtained by step (3) and step (4) according to 2-3:1 weight ratio mixing, 4 DEG C are kept in dark place taking-up after 24 hours, are put into centrifuge tube, centrifuge 5 minutes, take supernatant;
(6) 30 times of the clear water that weight is folium artemisiae argyi weight is added into the folium artemisiae argyi dried, 10-15 is cooked by slow fire after being heated to boiling Minute, filter to take folium artemisiae argyi decoction liquor;
(7) by chlorella powder and enteromorpha powder according to 2:1 weight is than mixing, and it is chlorella powder and enteromorpha powder gross mass to add quality 40% purified water, be put into after mixing in ultra low temperature freezer preserve 12 hours, take out, grind on ice, while grinding while add matter Measure the saline solution that fraction is 0.5%, gross mass of the quality equivalent to chlorella, Enteromorpha and purified water of the saline solution of addition;Grind The mixture of chlorella, Enteromorpha, purified water and saline solution is transferred in centrifuge tube by mill after 30-40 minutes, is centrifuged 5 minutes, is taken Supernatant;Sediment after centrifugation is transferred in mortar, the purified water of the quality such as addition and sediment is ground 20-30 minutes Ultrasonication 15 minutes, are then transferred in centrifuge tube afterwards, centrifuge 5 minutes, take supernatant, merge the supernatant of gained twice Liquid;
(8) dandelion is cleaned, dried, crush;
(9) it is dragon fruit pericarp is finely ground, mixed with the dandelion obtained by step (8), the mass ratio of dragon fruit pericarp and dandelion For 5-6:1;
(10) by the Sucus Luffae obtained by step (1), the Green Tea Leachate obtained by step (2), the supernatant obtained by step (5), step Suddenly the supernatant obtained by folium artemisiae argyi decoction liquor obtained by (6), step (7) is according to 2:10-12:1:4-5:2 mass ratio mixing, uses magnetic Power agitator is stirred 30-40 minutes;
(11) mixture obtained by step (10) is added in the mixture obtained by step (9), stirring while adding, step (9) institute The mass ratio of mixture obtained by the step of mixture obtained and addition (10) is 1:8-10, magnetic stirring apparatus is used after being well mixed Stirring 30-40 minutes, is transferred in centrifuge tube, centrifuges, abandons sediment, stay supernatant;
(12) by the supernatant obtained by nano-glass pearl powder and step (11) according to 2:3-4 ratio mixing, ultrasonication 20 Minute, produce object.
2. the preparation method of pure natural sunscreen cream according to claim 1, it is characterised in that:In step (3), tree peony and peach Flower is according to 2:1 weight is than mixing.
3. the preparation method of pure natural sunscreen cream according to claim 1, it is characterised in that:In step (9), dragon fruit fruit Skin and the mass ratio of dandelion are 6:1.
4. the preparation method of pure natural sunscreen cream according to claim 1, it is characterised in that:In step (10), by step (1) Green Tea Leachate obtained by Sucus Luffae, step (2) obtained by, the supernatant obtained by step (5), the folium artemisiae argyi obtained by step (6) Supernatant obtained by decoction liquor, step (7) is according to 2:10:1:5:2 mass ratio mixing, is divided with magnetic stirrer 30-40 Clock..
5. the preparation method of pure natural sunscreen cream according to claim 1, it is characterised in that:In step (11), step (9) The mass ratio of mixture obtained by the step of mixture of gained and addition (10) is 1:9.
6. the preparation method of pure natural sunscreen cream according to claim 1, it is characterised in that:In step (12), nanoscale Pearl powder is with the supernatant obtained by step (11) according to 2:3 ratio mixing.
7. it is pure natural sun-proof obtained by a kind of preparation method of the pure natural sunscreen cream any one of claim 1-6 Frost.
CN201710513477.3A 2017-06-29 2017-06-29 A kind of pure natural sunscreen cream and preparation method thereof Withdrawn CN107308091A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103405363A (en) * 2013-07-29 2013-11-27 朱耀灯 Sun-proof repair combination
CN105213271A (en) * 2015-11-03 2016-01-06 重庆小丸科贸有限公司 A kind of preparation method containing the sunscreen cream of repair function microcapsule after solarization
CN105456158A (en) * 2015-12-11 2016-04-06 饶雅琴 Amaranthus mangostanus sunscreen cream and preparation method thereof
CN106309314A (en) * 2016-08-25 2017-01-11 周荣 Preparation method of natural sunscreen cream
CN106691977A (en) * 2017-03-06 2017-05-24 济南大学 Preparation method for natural compound plant extract sunscreen cream

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103405363A (en) * 2013-07-29 2013-11-27 朱耀灯 Sun-proof repair combination
CN105213271A (en) * 2015-11-03 2016-01-06 重庆小丸科贸有限公司 A kind of preparation method containing the sunscreen cream of repair function microcapsule after solarization
CN105456158A (en) * 2015-12-11 2016-04-06 饶雅琴 Amaranthus mangostanus sunscreen cream and preparation method thereof
CN106309314A (en) * 2016-08-25 2017-01-11 周荣 Preparation method of natural sunscreen cream
CN106691977A (en) * 2017-03-06 2017-05-24 济南大学 Preparation method for natural compound plant extract sunscreen cream

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Application publication date: 20171103