CN107307469A - A kind of component for being capable of quick release moisture in filter stick and preparation method thereof - Google Patents
A kind of component for being capable of quick release moisture in filter stick and preparation method thereof Download PDFInfo
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- CN107307469A CN107307469A CN201710478642.6A CN201710478642A CN107307469A CN 107307469 A CN107307469 A CN 107307469A CN 201710478642 A CN201710478642 A CN 201710478642A CN 107307469 A CN107307469 A CN 107307469A
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- Prior art keywords
- moulding
- component
- sodium
- injection
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/16—Use of materials for tobacco smoke filters of inorganic materials
Abstract
The present invention relates to a kind of component for being capable of quick release moisture in filter stick and preparation method thereof.The component is made up of moulding A with moulding B；Moulding A is trapezoidal cylinder；Moulding B is oblate cylinder；The liquid of pure water, the food grade salts aqueous solution or inorganic base aqueous solution is housed in moulding A.Component of the present invention can directly increase substantially main flume moisture, it will be apparent that ground improves suction effect；The present invention is manufactured using polydactyl acid, modified polycaprolactone, medical PVC food-grade PP materials using the method for injection, therefore suitable industrialized production manufacture.
Description
【Technical field】
The invention belongs to cigarette auxiliary material production technical field.More particularly it relates to one kind energy in filter stick
The component of enough quick release moisture, the preparation method for further relating to the component.
【Background technology】
Cigarette is behind Kaifeng, and moisture in cut tobacco can gradually be lost in.Especially on plateau and Arid Area, moisture in cut tobacco is behind Kaifeng
8-10% can be dropped in 24h.The lost suction quality for directly affecting cigarette of moisture in cut tobacco, the hair especially in aesthetic quality
Thorn sense, peppery sense substantially increase.
Consumer's major consumers are cigarette mainstream flue gas parts.The essence of main flume is aerosol, and main flume exists
Substantially it is an aerosol deposition and the interaction of elution when by cigarette filter.Particulate matter in aerosol is filtered
The diffusional deposition effect retention of rod tow；While the volatile material of aerosol also in elution filter stick.Main flume is in mark
Under conditions of quasi- suction is determined, the volatilizable thing 5 to 12% on filter stick can be eluted.
One section is introduced in filter stick can stablize the component of the present invention for preserving moisture.In consumer's extruded member, component
In water or the aqueous solution, at the easily broken impression in component smallest cross-sectional extrude.Moisture is quickly absorbed by tow, works as main flume
By infiltrated by moisture tow when, the moisture in tow is eluted in main flume, so as to reach directly lifting mainstream smoke
The purpose of air water point.
【The content of the invention】
[technical problem to be solved]
It is an object of the invention to provide a kind of component for being capable of quick release moisture in filter stick.
It is a further object to provide the preparation method for being capable of quick release moisture component in filter stick.
[technical scheme]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of component for being capable of quick release moisture in filter stick.
The component is made up of moulding A with moulding B；Moulding A be a kind of high 4~6mm, 2~4mm of upper section diameter,
5~7mm of lower section diameter trapezoidal cylinder；Moulding B is a kind of high 1~3mm, 5.0~6.8mm of upper section diameter, lower section
5~7mm of diameter oblate cylinder；Moulding A is connected with moulding B using ultrasonic bonding；Filled in moulding A
There are one or more liquid for being selected from pure water, the food grade salts aqueous solution or inorganic base aqueous solution, the amount of this liquid is 20~100
μl。
A preferred embodiment of the invention, has cross on the upper section of the moulding A provided with a kind of
The easy fracture impression of type, hexagon or diamond shape.
According to another preferred embodiment of the present invention, described moulding A and moulding B is by 3.0~6.0 weight
Part is one or more a kind of selected from polycaprolactone, medical grade PVC, food-grade PP or the major ingredient of PLA and 0.4~1.0 parts by weight
Or a variety of auxiliary materials selected from ATBC or glyceryl triacetate are made.
According to another preferred embodiment of the present invention, described food grade salts are one or more selected from bicarbonate
Sodium, sodium carbonate, the salt of sodium citrate or sodium tartrate；Described inorganic base is one or more selected from sodium hydroxide, bicarbonate
The alkali of sodium, sodium carbonate or calcium hydroxide.
According to another preferred embodiment of the present invention, the concentration of the food grade salts solution is 0.1~0.5mol/L；
The concentration of the inorganic alkali solution is 0.08~0.10mol/L.
The present invention relates to a kind of preparation method for being capable of quick release moisture component in filter stick.
The step of preparation method, is as follows：
A, the modified batch mixing of preparation
3.0~6.0 parts by weight major ingredients and 0.4~1.0 parts by weight auxiliary material are added to the Heat preservation material of hot melt granulation machine
In bucket, the fully heating melting at 150~250 DEG C of temperature, then 30~90min is stirred under 20~200rpm of rotating speed, then squeeze
Go out granulation, obtain a kind of modified batch mixing；
Described major ingredient is one or more material selected from polycaprolactone, medical grade PVC, food-grade PP or PLA；Institute
The auxiliary material stated is one or more material selected from ATBC or glyceryl triacetate；
B, injection piece
The obtained modification batch mixings of step A are put into injection machine hopper, then carried out under conditions of 150~300 DEG C of temperature
Piece is molded, moulding A and moulding B is respectively obtained；Moulding A be a kind of high 4~6mm, 2~4mm of upper section diameter, lower section
Face 5~7mm of diameter trapezoidal cylinder；Moulding B is a kind of high 1~3mm, 5.0~6.8mm of upper section diameter, lower section diameter 5
~7mm oblate cylinder；
C, injection solution
Using calibrated shot equipment, one or more selected from pure water, the food grade salts aqueous solution or inorganic base aqueous solution
Liquid is injected into moulding A；
D, welding
After the completion of step C, moulding A is connected with moulding B using ultrasonic welding method, obtained in filter stick
In be capable of the component of quick release moisture.
According to another preferred embodiment of the present invention, have ten provided with a kind of on the upper section of the moulding A
The easy fracture impression of font, hexagon or diamond shape.
According to another preferred embodiment of the present invention, described food grade salts are one or more selected from bicarbonate
Sodium, sodium carbonate, the salt of sodium citrate or sodium tartrate；Described inorganic base is one or more selected from sodium hydroxide, bicarbonate
The alkali of sodium, sodium carbonate or calcium hydroxide.
According to another preferred embodiment of the present invention, the concentration of the food grade salts solution is 0.1~0.5mol/L；
The concentration of the inorganic alkali solution is 0.08~0.10mol/L.
According to another preferred embodiment of the present invention, the injection rate of the liquid is 20~100 μ l.
The present invention is described in more detail below.
The present invention relates to a kind of component for being capable of quick release moisture in filter stick.
The component is made up of moulding A with moulding B；Moulding A be a kind of high 4~6mm, 2~4mm of upper section diameter,
5~7mm of lower section diameter trapezoidal cylinder；Moulding B is a kind of high 1~3mm, 5.0~6.8mm of upper section diameter, lower section
5~7mm of diameter oblate cylinder；Moulding A is connected with moulding B using ultrasonic bonding；Filled in moulding A
There are one or more liquid for being selected from pure water, the food grade salts aqueous solution or inorganic base aqueous solution, the amount of this liquid is 20~100
μl。
The present invention in filter stick can quick release moisture element structure schematic diagram referring to accompanying drawing 1, wherein A is moulding A,
B is moulding B.
The structure of the moulding A is referring to accompanying drawing 2, and wherein accompanying drawing 2A is the top view of the moulding A；Accompanying drawing 2B is institute
State moulding A sectional view.
Known by accompanying drawing 2, described moulding A is trapezoidal cylinder；Known by accompanying drawing 2A, the moulding A upper section
Face is provided with a kind of easy fracture impression with cross, hexagon or diamond shape.Set on the upper section of the moulding A
Easy fracture impression is put, easily broken impression is end face one crackly mouth of manufacture in moulding, and consumer is in use
Easy fracture impression can be broken off during extruded member, so that the water in component is extruded from component, reach release moisture arrives filter
Effect in rod tow, the moisture of final lifting main flume.
In the present invention, in addition to cross, hexagon or rhombus, this easy fracture impression can also be using other shapes
Shape, simply they will not be processed to it or component of the present invention bring detrimental effect, and these shapes are also all in the protection of the present invention
Within the scope of.
The structure of the moulding B is known that described moulding B is oblate cylinder referring to accompanying drawing 3 by accompanying drawing 3；It is wherein attached
Fig. 3 A are the top views of the moulding B；Accompanying drawing 3B is the sectional view of the moulding B.
According to the present invention, described moulding A and moulding B is to be selected to gather oneself by 3.0~6.0 parts by weight one or more
Lactone, medical grade PVC, food-grade PP or the major ingredient of PLA and 0.4~1.0 parts by weight one or more are selected from acetyl tributyl citrate
What the auxiliary material of tri-n-butyl or glyceryl triacetate was made.
In the present invention, because the main function of component is stably to wrap up and preserve moisture, and major ingredient is member of formation
Main material, so the fluid-tight injected plastics material without harmful substance of selection is as major ingredient, described major ingredient is food
The high polymer material of level or medical grade, and do not have and dissolve in water.
The basic role of the auxiliary material is to be used to improve major ingredient performance during hot melt granulation, to make component possess one
Fixed elasticity and rupture performance, wherein elasticity is unlikely to have stiff feel when being and allowing consumer's extruded member, rupture performance is
It can be fractureed in easily broken impression deformation process, so as to discharge moisture.
Polycaprolactone, medical grade PVC, food-grade PP or the PLA that the present invention is used all are the productions sold in the market
Product, the polycaprolactone for example sold by Perstorp companies of Sweden with trade name capa-6800, by LG chemical companies with trade name
The medical grade PVC of LB110 sale.Certainly, it is every have the present invention using major ingredient performance again will not to the present invention in filter stick energy
Enough quick release moisture components produce dysgenic other chemical substances and may be used to the present invention, and these materials are also all at this
Within the protection domain of invention.
ATBC or glyceryl triacetate that the present invention is used all are the products sold in the market,
The ATBC for example sold by Donggang City field chemical company with trade name ATBC-DGT0198, by Tai Ke companies with
The glyceryl triacetate of trade name glyceryl triacetate sale.Certainly, it is every to have the present invention again be right using auxiliary material performance
Other chemical substances that the present invention is capable of quick release moisture component generation negative interaction in filter stick may be used to the present invention, this
A little materials are also all within protection scope of the present invention.
In the present invention, when the supplementary product consumption is in described scope, if the major ingredient consumption is less than 3.0 weight
Part, then material modification can be made to fail, be embodied in material and cross modeling, the intensity of high polymer material declines to a great extent, it is micro on the low side to lead
Construction material is caused to become fragile, a large amount of on the low side result even in can not injection molding；If the major ingredient consumption is more than 6.0 parts by weight,
It then can also material modification is failed, be embodied in that material is really up to the mark, plasticization effect is not obvious.Moulding extruding feel is stiff, very
To that can not crush easily broken impression when causing and extruding, moisture can not be discharged by ultimately resulting in whole component；Therefore, the major ingredient consumption is
3.0~6.0 parts by weight are rational.
Similarly, when the major ingredient consumption is in described scope, if the supplementary product consumption is less than 0.4 parts by weight,
Material modification can be made to fail, be embodied in that material is really up to the mark, plasticization effect is not obvious.Moulding extruding feel is stiff, or even leads
Cause that during extruding easily broken impression can not be crushed, moisture can not be discharged by ultimately resulting in whole component；If the supplementary product consumption is more than 1.0
Parts by weight, then can make material modification fail, and be embodied in material and cross modeling, the intensity of high polymer material declines to a great extent, and causes structure
Part material becomes fragile, and resulting even in can not injection molding；Therefore, the major ingredient consumption is that 0.4~1.0 parts by weight are appropriate.
In the present invention, the basic role of liquid is in consumer's extruded member, from easily broken impression in moulding A
In discharge, infiltrate tow, so as to improve main flume moisture.Described liquid is that one or more are selected from pure water, eaten
The liquid of level saline solution or inorganic base aqueous solution.
According to the present invention, described food grade salts are one or more selected from sodium acid carbonate, sodium carbonate, sodium citrate or wine
The salt of stone acid sodium；Described inorganic base is one or more selected from sodium hydroxide, sodium acid carbonate, sodium carbonate or calcium hydroxide
Alkali.
According to the present invention, the concentration of the food grade salts solution is 0.1~0.5mol/L；The concentration of the inorganic alkali solution
It is 0.08~0.10mol/L.
In the present invention, the concentration of the food grade salts solution and inorganic alkali solution exceed the concentration range be all can not
Take, because salting liquid is added in component primarily to improving the suction mouthfeel of cigarette, therefore low concentration salt solution
It is effective in terms of mouthfeel is suitably improved, but if the concentration of increase salting liquid, moisture effusion effect in solution can be caused
Rate is reduced, so that cause component to increase the effect reduction of main flume moisture, therefore suitable concentration is crucial technical indicator.
Food grade salts and inorganic base that the present invention is used all are the products sold in the market.
The present invention relates to a kind of preparation method for being capable of quick release moisture component in filter stick.
The step of preparation method, is as follows：
A, the modified batch mixing of preparation
3.0~6.0 parts by weight major ingredients and 0.4~1.0 parts by weight auxiliary material are added to the Heat preservation material of hot melt granulation machine
In bucket, the fully heating melting at 150~250 DEG C of temperature, then 30~90min is stirred under 20~200rpm of rotating speed, then squeeze
Go out granulation, obtain a kind of modified batch mixing；
Described major ingredient is one or more material selected from polycaprolactone, medical grade PVC, food-grade PP or PLA；Institute
The auxiliary material stated is one or more material selected from ATBC or glyceryl triacetate；Described major ingredient and auxiliary material
It has been be described previously that, therefore will not be repeated here.
According to the present invention, there is cross, hexagon or diamond shape provided with a kind of on the upper section of the moulding A
Easy fracture impression.
According to the present invention, described food grade salts are one or more selected from sodium acid carbonate, sodium carbonate, sodium citrate or wine
The salt of stone acid sodium；Described inorganic base is one or more selected from sodium hydroxide, sodium acid carbonate, sodium carbonate or calcium hydroxide
Alkali.The concentration of the food grade salts solution is 0.1~0.5mol/L；The concentration of the inorganic alkali solution is 0.08~0.10mol/
L.The injection rate of the liquid is 20~100 μ l.
The hot melt granulation machine that the present invention is used is the product sold in the market, such as by Zhejiang Pin Bo companies with commodity
The comminutor of name PYM120-100 sale, in practical operation, is operated according to the mode of operation described in its specification.
B, injection piece
The obtained modification batch mixings of step A are put into injection machine hopper, then carried out under conditions of 150~300 DEG C of temperature
Piece is molded, moulding A and moulding B is respectively obtained；Moulding A be a kind of high 4~6mm, 2~4mm of upper section diameter, lower section
Face 5~7mm of diameter trapezoidal cylinder；Moulding B is a kind of high 1~3mm, 5.0~6.8mm of upper section diameter, lower section diameter 5
~7mm oblate cylinder；
The injection machine that the present invention is used is the product sold in the market, such as by Hai Tian companies with the horizontal song of trade name
The injection machine of elbow injection machine sale, in practical operation, is operated according to the mode of operation described in its specification.
Moulding A and moulding B situation have been described previously, therefore will not be repeated here.
C, injection solution
Using calibrated shot equipment, one or more selected from pure water, the food grade salts aqueous solution or inorganic base aqueous solution
Liquid is injected into moulding A；
The calibrated shot equipment is, for example, point gum machine, is the product sold in the market.
D, welding
After the completion of step C, moulding A is connected with moulding B using ultrasonic welding method, obtained in filter stick
In be capable of the component of quick release moisture.
Ultrasonic bonding is the body surface that two need welding are delivered to using dither ripple, in the case of pressurization,
The fusion for making two body surface phase mutual friction and being formed between molecular layer.
The ultrasonic welding machine that the present invention is used is the product sold in the market, such as by Hai Tian companies with trade name
The injection machine of horizontal toggle injection machine, in practical operation, is operated according to the mode of operation described in its specification.
The component of the present invention is introduced after filter stick, and moisture, which can be stablized, to be housed in filter stick.In consumer's extruding filter stick
During component, water or food grade salts or inorganic base aqueous solution in component are extruded at the easily broken impression in component smallest cross-sectional, water
Point quickly absorbed by tow, when main flume passes through the tow infiltrated by moisture, the moisture in tow is eluted to mainstream smoke
In gas, so as to reach the purpose of directly lifting main flume moisture.
The experiment of moisture content detection is as follows in main flume：
Test specimen：10,20,30,40, the 50 different amounts of pure water of μ l are injected separately into moulding A；
Control sample：Pure water is not injected into moulding A；
Experimental condition：GB5606.5-2005 Part V main flumes；
Water content detection：GB5606.5-2005 Part V main flumes.
Result of the test is listed in the table below in 1：
Table 1：Main flume elutes filter tip moisture measurement result
The result that table 1 is listed shows that the flue gas moisture of laboratory sample is lifted clearly compared with the flue gas moisture of control sample.
[beneficial effect]
The beneficial effects of the invention are as follows：The component of quick increase filter stick water release of the invention can be increased substantially directly
Main flume moisture, it will be apparent that ground improves suction effect；The present invention uses polydactyl acid, modified polycaprolactone, medical PVC
Food-grade PP materials, are manufactured using the method for injection, therefore suitable industrialized production manufacture.
【Brief description of the drawings】
Fig. 1 is the structural representation that the present invention is capable of quick release moisture component in filter stick；
In figure：
1A- component top views of the present invention；1B- is equipped with the component longitudinal sectional view of the present invention of liquid；
Fig. 2 is moulding A of the present invention structural representation；
In figure：
2A- moulding A top views；2B- moulding A longitudinal sectional views；
Fig. 3 is moulding B of the present invention structural representation；
In figure：
3A- moulding B top views；3B- moulding B longitudinal sectional views；
【Embodiment】
The present invention is will be better understood that by following embodiments.
Embodiment 1：The present invention being capable of quick release moisture structure manufacture in filter stick
The implementation steps of the embodiment are as follows：
A, the modified batch mixing of preparation
By 3.0 parts by weight polycaprolactones, medical grade PVC and food-grade PP, (weight compares 1:1:1) with 0.8 parts by weight acetyl lemon
Lemon acid tri-n-butyl auxiliary material is added to by Zhejiang Pin Bo companies with the Heat preservation hopper of trade name PYM120-100 comminutors,
The fully heating melting at 220 DEG C of temperature, then stir under rotating speed 140rpm 50min, the condition then described in its specification
Lower extruding pelletization, obtains a kind of modified batch mixing；
B, injection piece
The obtained modification batch mixings of step A are put into by Hai Tian companies with the injection machine of the horizontal toggle injection machine sale of trade name
Hopper in, then under conditions of 250 DEG C of temperature carry out injection piece, respectively obtain moulding A and moulding B；Moulding A is
A kind of high 4mm, upper section diameter 3mm, lower section diameter 6mm trapezoidal cylinder；Moulding B is a kind of high 1mm, upper section diameter
5.6mm, lower section diameter 6mm oblate cylinder；Provided with a kind of with cross-type shape on the upper section of the moulding A
Easy fracture impression.
C, injection solution
Using the KSL point gum machine calibrated shot equipment sold by Shenzhen Jian Feng companies with trade name point gum machine, a kind of or
A variety of to be injected into selected from pure water in moulding A, the injection rate of the water is 80 μ l；
D, welding
After the completion of step C, the ultrasound sold by the southern mechanical stiffness company in Guangzhou with trade name mechanical stiffness supersonic welder is used
Wave soldering, which picks, is connected moulding A with moulding B under conditions of the description of its specification, and obtaining can be quick in filter stick
Discharge the component of moisture.
Embodiment 2：The present invention being capable of quick release moisture structure manufacture in filter stick
The implementation steps of the embodiment are as follows：
A, the modified batch mixing of preparation
By 4.0 parts by weight polycaprolactones, medical grade PVC and food-grade PP, (weight compares 1:1:1.5) major ingredient and 0.4 parts by weight
Glyceryl triacetate auxiliary material is added to by Zhejiang Pin Bo companies with the Heat preservation hopper of trade name PYM120-100 comminutors,
The fully heating melting at 250 DEG C of temperature, then 70min is stirred under rotating speed 20rpm, then under conditions of the description of its specification
Extruding pelletization, obtains a kind of modified batch mixing；
B, injection piece
The obtained modification batch mixings of step A are put into by Hai Tian companies with the injection machine of the horizontal toggle injection machine sale of trade name
Hopper in, then under conditions of 150 DEG C of temperature carry out injection piece, respectively obtain moulding A and moulding B；Moulding A is
A kind of high 5mm, upper section diameter 2mm, lower section diameter 5mm trapezoidal cylinder；Moulding B is a kind of high 2mm, upper section diameter
5.0mm, lower section diameter 5mm oblate cylinder；Provided with a kind of with hexagonal shape on the upper section of the moulding A
Easy fracture impression.
C, injection solution
Using the KSL point gum machine calibrated shot equipment sold by Shenzhen Jian Feng companies with trade name point gum machine, a kind of or
A variety of to be injected into selected from the 0.1mol/L sodium acid carbonate food grade salts aqueous solution in moulding A, the injection rate of the liquid is 50 μ l；
D, welding
After the completion of step C, the ultrasound sold by the southern mechanical stiffness company in Guangzhou with trade name mechanical stiffness supersonic welder is used
Wave soldering, which picks, is connected moulding A with moulding B under conditions of the description of its specification, and obtaining can be quick in filter stick
Discharge the component of moisture.
Embodiment 3：The present invention being capable of quick release moisture structure manufacture in filter stick
The implementation steps of the embodiment are as follows：
A, the modified batch mixing of preparation
By 6.0 parts by weight PLAs, polycaprolactone, medical grade PVC and food-grade PP9, (weight compares 1:2:1:0.5) major ingredient
(weight compares 1 with glyceryl triacetate with 1.0 parts by weight ATBCs:2) auxiliary material is added to wins public affairs by Zhejiang product
Department is with the Heat preservation hopper of trade name PYM120-100 comminutors, the fully heating melting at 150 DEG C of temperature, then in rotating speed
90min is stirred under 80rpm, then extruding pelletization, obtain a kind of modified batch mixing；
B, injection piece
The obtained modification batch mixings of step A are put into by Hai Tian companies with the injection of the horizontal toggle injection machine sale of trade name
In the hopper of machine, then under conditions of 200 DEG C of temperature injection piece is carried out, respectively obtain moulding A and moulding B；Moulding A
It is a kind of high 6mm, upper section diameter 4mm, lower section diameter 6mm trapezoidal cylinder；Moulding B is that a kind of high 2mm, upper section are straight
Footpath 5.6mm, lower section diameter 7mm oblate cylinder；Provided with a kind of with diamond shape on the upper section of the moulding A
Easy fracture impression.
C, injection solution
Using the KSL point gum machine calibrated shot equipment sold by Shenzhen Jian Feng companies with trade name point gum machine, a kind of or
A variety of to be injected into selected from the 0.5mol/L sodium tartrate food grade salts aqueous solution in moulding A, the injection rate of the liquid is 20 μ l；
D, welding
After the completion of step C, the ultrasound sold by the southern mechanical stiffness company in Guangzhou with trade name mechanical stiffness supersonic welder is used
Wave soldering, which picks, is connected moulding A with moulding B under conditions of the description of its specification, and obtaining can be quick in filter stick
Discharge the component of moisture.
Embodiment 4：The present invention being capable of quick release moisture structure manufacture in filter stick
The implementation steps of the embodiment are as follows：
A, the modified batch mixing of preparation
By 5.0 parts by weight polycaprolactones, medical grade PVC, food-grade PP or PLA, (weight compares 0.5:0.8:1:1.2) it is main
Material is added to by Zhejiang Pin Bo companies with trade name PYM120-100 comminutors with 0.6 parts by weight glyceryl triacetate auxiliary material
In Heat preservation hopper, the fully heating melting at 180 DEG C of temperature, then 30min is stirred under rotating speed 200rpm, then extrusion is made
Grain, obtains a kind of modified batch mixing；
B, injection piece
The obtained modification batch mixings of step A are put into by Hai Tian companies with the injection of the horizontal toggle injection machine sale of trade name
In the hopper of machine, then under conditions of 300 DEG C of temperature injection piece is carried out, respectively obtain moulding A and moulding B；Moulding A
It is a kind of high 5mm, upper section diameter 3mm, lower section diameter 7mm trapezoidal cylinder；Moulding B is that a kind of high 3mm, upper section are straight
Footpath 5.8mm, lower section diameter 6mm oblate cylinder；There is cross-type shape provided with a kind of on the upper section of the moulding A
Easy fracture impression.
C, injection solution
Using the KSL point gum machine calibrated shot equipment sold by Shenzhen Jian Feng companies with trade name point gum machine, a kind of or
A variety of liquid selected from 0.08mol/L sodium acid carbonate inorganic base aqueous solutions are injected into moulding A, and the injection rate of the liquid is
100μl；
D, welding
After the completion of step C, the ultrasound sold by the southern mechanical stiffness company in Guangzhou with trade name mechanical stiffness supersonic welder is used
Wave soldering, which picks, is connected moulding A with moulding B under conditions of the description of its specification, and obtaining can be quick in filter stick
Discharge the component of moisture.
Embodiment 5：The present invention being capable of quick release moisture structure manufacture in filter stick
The implementation steps of the embodiment are as follows：
A, the modified batch mixing of preparation
3.5 parts by weight polycaprolactone major ingredients and 0.42 parts by weight ATBC auxiliary material are added to by Zhejiang
Pin Bo companies are with the Heat preservation hopper of trade name PYM120-100 comminutors, the fully heating melting at 200 DEG C of temperature, then
60min is stirred under rotating speed 160rpm, then extruding pelletization, obtain a kind of modified batch mixing；
B, injection piece
The obtained modification batch mixings of step A are put into by Hai Tian companies with the injection of the horizontal toggle injection machine sale of trade name
In the hopper of machine, then under conditions of 260 DEG C of temperature injection piece is carried out, respectively obtain moulding A and moulding B；Moulding A
It is a kind of high 6mm, upper section diameter 3mm, lower section diameter 6mm trapezoidal cylinder；Moulding B is that a kind of high 2mm, upper section are straight
Footpath 6.2mm, lower section diameter 6.5mm oblate cylinder；There is hexagon shape provided with a kind of on the upper section of the moulding A
The easy fracture impression of shape.
C, injection solution
Using the KSL point gum machine calibrated shot equipment sold by Shenzhen Jian Feng companies with trade name point gum machine, a kind of or
A variety of liquid selected from 0.10mol/L sodium carbonate inorganic base aqueous solutions are injected into moulding A, and the injection rate of the liquid is 40
μl；
D, welding
After the completion of step C, the ultrasound sold by the southern mechanical stiffness company in Guangzhou with trade name mechanical stiffness supersonic welder is used
Wave soldering, which picks, is connected moulding A with moulding B under conditions of the description of its specification, and obtaining can be quick in filter stick
Discharge the component of moisture.
Embodiment 6：The present invention being capable of quick release moisture structure manufacture in filter stick
The implementation steps of the embodiment are as follows：
A, the modified batch mixing of preparation
5.2 parts by weight food-grade PP major ingredients and 0.88 parts by weight glyceryl triacetate auxiliary material are added to and win by Zhejiang product
Company is with the Heat preservation hopper of trade name PYM120-100 comminutors, the fully heating melting at 160 DEG C of temperature, then is turning
80min is stirred under fast 170rpm, then extruding pelletization, obtain a kind of modified batch mixing；
B, injection piece
The obtained modification batch mixings of step A are put into by Hai Tian companies with the injection of the horizontal toggle injection machine sale of trade name
In the hopper of machine, then under conditions of 190 DEG C of temperature injection piece is carried out, respectively obtain moulding A and moulding B；Moulding A
It is a kind of high 5mm, upper section diameter 2mm, lower section diameter 5mm trapezoidal cylinder；Moulding B is that a kind of high 1mm, upper section are straight
Footpath 6.4mm, lower section diameter 6.6mm oblate cylinder；There is diamond shape provided with a kind of on the upper section of the moulding A
Easy fracture impression.
C, injection solution
Using the KSL point gum machine calibrated shot equipment sold by Shenzhen Jian Feng companies with trade name point gum machine, a kind of or
A variety of to be injected into selected from pure water, the 0.3mol/L sodium citrate food grade salts aqueous solution in moulding A, the injection rate of the liquid is
805020100μl；
D, welding
After the completion of step C, the ultrasound sold by the southern mechanical stiffness company in Guangzhou with trade name mechanical stiffness supersonic welder is used
Wave soldering, which picks, is connected moulding A with moulding B under conditions of the description of its specification, and obtaining can be quick in filter stick
Discharge the component of moisture.
Using the method described in this specification, prepared by embodiment 1-6 being capable of quick release moisture structure in filter stick
Part has carried out main flume elution filter tip moisture measurement, and the results are shown in Table 2 for it.
The sample that pure water is not injected into moulding A is control sample, and its corresponding testing result is also shown in Table 2 below.
Table 2：Prepared by embodiment 1-6 being capable of the elution filter tip moisture survey of quick release moisture component main flume in filter stick
Examination
The result that table 2 is listed shows that aqueous firmware is obviously improved amplitude up to more than 70% to the hydraulic lift of main flume
Meanwhile, expert group of smokeing panel test is organized, suck standards of grading according to conventional flue gas carries out aesthetic quality to above-mentioned sample
Evaluation, determines that control sample is sent out thoroughly for cigarette perfume, pleasant impression is clean, throat has stimulation, miscellaneous gas to slightly have；Sample prepared by embodiment 1-6
Sent out thoroughly for cigarette perfume, flue gas is soft, pleasant impression is clean, throat's stimulation slightly has, miscellaneous gas slightly has, these results show component of the present invention to volume
Mouth sense lifting is obvious, is mainly shown as that excitant weakens, pleasant impression improves comfortable.
Claims (10)
1. a kind of component for being capable of quick release moisture in filter stick, it is characterised in that the component is by moulding A and moulding B structures
Into；Moulding A is a kind of high 4~6mm, 2~4mm of upper section diameter, 5~7mm of lower section diameter trapezoidal cylinder；Moulding B
It is a kind of high 1~3mm, 5.0~6.8mm of upper section diameter, 5~7mm of lower section diameter oblate cylinder；Moulding A and injection
Part B is connected using ultrasonic bonding；Equipped with one or more water-soluble selected from pure water, food grade salts in moulding A
The liquid of liquid or inorganic base aqueous solution, the amount of this liquid is 20~100 μ l.
2. component according to claim 1, it is characterised in that have ten provided with a kind of on the upper section of the moulding A
The easy fracture impression of font, hexagon or diamond shape.
3. component according to claim 1, it is characterised in that described moulding A and moulding B is by 3.0~6.0 weights
Measure major ingredient and 0.4~1.0 parts by weight one of part one or more selected from polycaprolactone, medical grade PVC, food-grade PP or PLA
What kind or a variety of auxiliary materials selected from ATBC or glyceryl triacetate were made.
4. component according to claim 1, it is characterised in that described food grade salts are one or more selected from bicarbonate
Sodium, sodium carbonate, the salt of sodium citrate or sodium tartrate；Described inorganic base is one or more selected from sodium hydroxide, bicarbonate
The alkali of sodium, sodium carbonate or calcium hydroxide.
5. component according to claim 1, it is characterised in that the concentration of the food grade salts solution is 0.1~0.5mol/
L；The concentration of the inorganic alkali solution is 0.08~0.10mol/L.
6. a kind of preparation method for being capable of quick release moisture component in filter stick, it is characterised in that the step of the preparation method such as
Under：
A, the modified batch mixing of preparation
3.0~6.0 parts by weight major ingredients and 0.4~1.0 parts by weight auxiliary material are added in the Heat preservation hopper of hot melt granulation machine,
The fully heating melting at 150~250 DEG C of temperature, then 30~90min is stirred under 20~200rpm of rotating speed, then extrusion is made
Grain, obtains a kind of modified batch mixing；
Described major ingredient is one or more material selected from polycaprolactone, medical grade PVC, food-grade PP or PLA；Described
Auxiliary material is one or more material selected from ATBC or glyceryl triacetate；
B, injection piece
The obtained modification batch mixings of step A are put into injection machine hopper, then are molded under conditions of 150~300 DEG C of temperature
Piece, respectively obtains moulding A and moulding B；Moulding A is that a kind of high 4~6mm, 2~4mm of upper section diameter, lower section are straight
5~7mm of footpath trapezoidal cylinder；Moulding B be a kind of high 1~3mm, 5.0~6.8mm of upper section diameter, lower section diameter 5~
7mm oblate cylinder；
C, injection solution
Using calibrated shot equipment, one or more liquid for being selected from pure water, the food grade salts aqueous solution or inorganic base aqueous solution
It is injected into moulding A；
D, welding
After the completion of step C, moulding A is connected with moulding B using ultrasonic welding method, the energy in filter stick is obtained
The component of enough quick release moisture.
7. production method according to claim 6, it is characterised in that provided with a kind of tool on the upper section of the moulding A
There are cross, hexagon or the easy fracture impression of diamond shape.
8. production method according to claim 6, it is characterised in that described food grade salts are one or more selected from carbon
Sour hydrogen sodium, sodium carbonate, the salt of sodium citrate or sodium tartrate；Described inorganic base is one or more selected from sodium hydroxide, carbon
The alkali of sour hydrogen sodium, sodium carbonate or calcium hydroxide.
9. preparation method according to claim 6, it is characterised in that the concentration of the food grade salts solution is 0.1~
0.5mol/L；The concentration of the inorganic alkali solution is 0.08~0.10mol/L.
10. preparation method according to claim 6, it is characterised in that the injection rate of the liquid is 20~100 μ l.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109430936A (en) * | 2018-11-20 | 2019-03-08 | 湖北中烟工业有限责任公司 | A kind of filter stick for cigarettes and cigarette including L-Cups cup firmware |
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|---|---|
| CN107307469B (en) | 2020-10-30 |
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