CN107297192A - A kind of gas, solid, liquid reaction unit - Google Patents

A kind of gas, solid, liquid reaction unit Download PDF

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Publication number
CN107297192A
CN107297192A CN201710625377.XA CN201710625377A CN107297192A CN 107297192 A CN107297192 A CN 107297192A CN 201710625377 A CN201710625377 A CN 201710625377A CN 107297192 A CN107297192 A CN 107297192A
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CN
China
Prior art keywords
agitating shaft
rotating ring
solid
reaction unit
cylinder body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201710625377.XA
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Chinese (zh)
Other versions
CN107297192B (en
Inventor
王适之
应茁翔
王帆
王一帆
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Yangtse River Mixers Co Ltd
Original Assignee
Zhejiang Yangtse River Mixers Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Zhejiang Yangtse River Mixers Co Ltd filed Critical Zhejiang Yangtse River Mixers Co Ltd
Priority to CN201710625377.XA priority Critical patent/CN107297192B/en
Publication of CN107297192A publication Critical patent/CN107297192A/en
Application granted granted Critical
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/17Stirrers with additional elements mounted on the stirrer, for purposes other than mixing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/21Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by their rotating shafts
    • B01F27/2122Hollow shafts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/085Feeding reactive fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/10Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention relates to a kind of reaction unit, specifically related to a kind of gas, solid, liquid reaction unit, including reaction cell body, frame, drive device and agitating shaft, the frame is arranged on reaction cell body, the drive device is arranged in frame, and the drive device driving agitating shaft rotation, the agitating shaft is stretched into the inner chamber of reaction cell body, the agitating shaft is hollow structure, and the upper end of the agitating shaft is connected with admission line by swivel joint.By the hollow direct air inlet of agitating shaft, the breather pipe not being additionally inserted into reactive tank has prevented reactive tank breather pipe for often occurring in stirring operation process and has released damage and easy clogging.

Description

A kind of gas, solid, liquid reaction unit
Technical field
The present invention relates to a kind of reaction unit, and in particular to Yi Zhongqi, solid, liquid reaction unit.
Background technology
Often there are oxidation or the operation of other gas-solid-liquid phase reaction units, usual air inlet in fields such as chemical industry, metallurgy, environmental protection Mode is all to use breather pipe infix form, and often difficult in the equipment fixed and be blocked in large-scale or Pot Lining of air inlet pipe To solve, under the intense impact of stirred fluid, air inlet pipe easily releases damage, and when parking is restarted, air inlet tube end is easy Block.
The content of the invention
The present invention is in view of the above-mentioned problems, provide a kind of gas, solid, liquid reaction unit.
The technical solution used in the present invention is as follows:A kind of gas, solid, liquid reaction unit, including reaction cell body, frame, drive Dynamic device and agitating shaft, the frame are arranged on reaction cell body, and the drive device is arranged in frame, the drive device Agitating shaft rotation is driven, the agitating shaft is stretched into the inner chamber of reaction cell body, the agitating shaft is hollow structure, the agitating shaft Upper end admission line is connected with by swivel joint.
The agitating shaft lower end is connected with escape pipe, and the gas outlet is provided with check valve.
The gas outlet is arranged on the side of escape pipe, and the axle center for deviateing the agitating shaft is set, and the check valve includes The connector that is fixedly connected with the escape pipe, the flap being hinged with the connector, the flap are relative with the connector The jointed shaft rotation being hinged can block gas outlet or be separated with the gas outlet, and the flap surface is provided with seal.
The gas outlet is set obliquely.
The escape pipe is fixedly connected with agitating shaft using bolt.
The swivel joint includes housing, spring, stationary ring, rotating ring, the rotating ring cylinder body being linked with the rotating ring, described Spring, stationary ring, rotating ring, rotating ring cylinder body are pressed into housing successively from top to bottom, O-shaped close provided with first between the stationary ring and housing The second O-ring seal is provided between seal, rotating ring and the rotating ring cylinder body, bearing, Y are provided between the rotating ring cylinder body and housing Type sealing ring, the 3rd sealing ring, the y-type seal ring, bearing, the 3rd sealing ring are set gradually from top to bottom, and the housing enters Feed channel is with being fixedly connected, and the rotating ring cylinder body is connected with agitating shaft.
The rotating ring cylinder body is threadedly coupled with agitating shaft, and seal washer is provided between the rotating ring cylinder body and agitating shaft.
Beneficial effects of the present invention are as follows:By the hollow direct air inlet of agitating shaft, it is not additionally inserted into reactive tank Breather pipe, has prevented reactive tank breather pipe for often occurring in stirring operation process and has released damage and easy clogging.
Brief description of the drawings
Fig. 1 is structural representation of the invention.
The enlarged diagram that Fig. 2 is A in Fig. 1.
The enlarged diagram that Fig. 3 is B in Fig. 1.
In figure, 1, react cell body;2, frame;3, drive device;4, agitating shaft;5, swivel joint;501, housing;502, bullet Spring;503, stationary ring;504, rotating ring;505, rotating ring cylinder body;506, the first O-ring seal;507, the second O-ring seal;508, axle Hold;509, y-type seal ring;510, the 3rd sealing ring;6, admission line;7, escape pipe;701, gas outlet;8, check valve;801, Connector;802, flap;803, seal;11, seal washer.
Embodiment
Below in conjunction with the accompanying drawings and embodiment, the present invention can be better described.
A kind of gas, solid, liquid reaction unit, including reaction cell body 1, frame 2, drive device 3 and agitating shaft 4, the frame 2 On reaction cell body 1, the drive device 3 is arranged in frame 2, and the driving of drive device 3 agitating shaft 4 rotates, institute State agitating shaft 4 to stretch into the inner chamber of reaction cell body 1, the agitating shaft 4 is hollow structure, the upper end of the agitating shaft 4 passes through rotation Adapter 5 is connected with admission line 6.By the hollow direct air inlet of agitating shaft, the breather pipe not being additionally inserted into reactive tank, Prevent reactive tank breather pipe for often occurring in stirring operation process and release damage and easy clogging.
The lower end of agitating shaft 4 is connected with escape pipe 7, and the gas outlet 701 is provided with check valve 8.The setting of check valve Prevent material from being overflowed by agitating paddle, correspondence harmful substance can play protection.
The gas outlet 701 is arranged on the side of escape pipe 7, and the axle center for deviateing the agitating shaft 4 is set, the check valve 8 include the connector 801 being fixedly connected with the escape pipe 7, the flap 802 being hinged with the connector 801, the flap 802 can block gas outlet 701 relative to the jointed shaft rotation being hinged with the connector 801 or be separated with the gas outlet 701, institute The surface of flap 802 is stated provided with seal 803.Conventional check valve is the pressure differential driving by flap both sides to open or close Close, play a part of preventing adverse current.And gas outlet 701 is arranged on side, flap opposite outlets are set, such agitating shaft rotation Turn to drive flap rotation to contribute to flap to open the centrifugal force of flap formation, that is, in normal operation, by centrifugal force Check valve can be opened with gas pressure, and air taking port can be closed by the backflow of liquid when stopping operation, so more Reliably, the pressure of gas is relied solely on, then can not ensure the lasting conveying of gas, unless kept gas high pressure.
The gas outlet 701 is set obliquely.The gravity of flap itself contributes to closed check valve.
The escape pipe 7 is fixedly connected with agitating shaft 4 using bolt.It is easily installed, dismantles and repairs, clears up.
The swivel joint 5 include housing 501, spring 502, stationary ring 503, rotating ring 504, with the rotating ring 504 link match somebody with somebody The rotating ring cylinder body 505 of conjunction, the spring 502, stationary ring 503, rotating ring 504, rotating ring cylinder body 505 are pressed into housing successively from top to bottom In 501, be provided with the first O-ring seal 506 between the stationary ring 503 and housing 501, the rotating ring 504 and rotating ring cylinder body 505 it Between be provided with the second O-ring seal 507, between the rotating ring cylinder body 505 and housing 501 provided with bearing 508, y-type seal ring 509, 3rd sealing ring 510, the y-type seal ring 509, bearing 508, the 3rd sealing ring 510 are set gradually from top to bottom, the housing 501 admission lines 6 are with being fixedly connected, and the rotating ring cylinder body 505 is connected with agitating shaft 4.Swivel joint is using built-in sealing, it is ensured that Quiet dynamic junction is air tight.Wherein, housing 501 is that some parts connect to be formed, and facilitates the installation of inner body.
The rotating ring cylinder body 505 is threadedly coupled with agitating shaft 4, provided with sealing between the rotating ring cylinder body 505 and agitating shaft 4 Packing ring 11.It is detachably connected, while ensureing sealing.
A kind of embodiment of the present invention is the foregoing is only, not for limiting the scope of the invention;The present invention's Protection domain is limited by the claim in claims, and every equivalence changes made according to invention and modification, is all existed Within the protection domain of patent of the present invention.

Claims (7)

1. a kind of gas, solid, liquid reaction unit, including reaction cell body(1), frame(2), drive device(3)And agitating shaft(4), institute State frame(2)Installed in reaction cell body(1)On, the drive device(3)Installed in frame(2)On, the drive device(3)Drive Dynamic agitating shaft(4)Rotation, the agitating shaft(4)Stretch into reaction cell body(1)Inner chamber in, it is characterised in that:The agitating shaft(4) For hollow structure, the agitating shaft(4)Upper end pass through swivel joint(5)It is connected with admission line(6).
2. gas according to claim 1, solid, liquid reaction unit, it is characterised in that:The agitating shaft(4)Lower end is connected with Escape pipe(7), the gas outlet(701)It is provided with check valve(8).
3. gas according to claim 2, solid, liquid reaction unit, it is characterised in that:The gas outlet(701)It is arranged on out Tracheae(7)Side, deviate the agitating shaft(4)Axle center set, the check valve(8)Including with the escape pipe(7)Gu Surely the connector connected(801)And the connector(801)The flap being hinged(802), the flap(802)It is relative with it is described Connector(801)The jointed shaft rotation being hinged can block gas outlet(701)Or with the gas outlet(701)Separation, the flap (802)Surface is provided with seal(803).
4. gas according to claim 3, solid, liquid reaction unit, it is characterised in that:The gas outlet(701)Set obliquely Put.
5. gas according to claim 3, solid, liquid reaction unit, it is characterised in that:The escape pipe(7)With agitating shaft(4) It is fixedly connected using bolt.
6. gas according to claim 1, solid, liquid reaction unit, it is characterised in that:The swivel joint(5)Including housing (501), spring(502), stationary ring(503), rotating ring(504)And the rotating ring(504)The rotating ring cylinder body being linked(505), institute State spring(502), stationary ring(503), rotating ring(504), rotating ring cylinder body(505)It is pressed into housing successively from top to bottom(501)It is interior, it is described Stationary ring(503)With housing(501)Between be provided with the first O-ring seal(506), the rotating ring(504)With rotating ring cylinder body(505)It Between be provided with the second O-ring seal(507), the rotating ring cylinder body(505)With housing(501)Between be provided with bearing(508), Y types it is close Seal(509), the 3rd sealing ring(510), the y-type seal ring(509), bearing(508), the 3rd sealing ring(510)From up to Under set gradually, the housing(501)Admission line(6)With being fixedly connected, the rotating ring cylinder body(505)With agitating shaft(4)Even Connect.
7. gas according to claim 1, solid, liquid reaction unit, it is characterised in that:The rotating ring cylinder body(505)With stirring Axle(4)Screw thread or flange connection, the rotating ring cylinder body(505)With agitating shaft(4)Between be provided with seal washer(11).
CN201710625377.XA 2017-07-27 2017-07-27 Gas, solid and liquid reaction device Active CN107297192B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710625377.XA CN107297192B (en) 2017-07-27 2017-07-27 Gas, solid and liquid reaction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710625377.XA CN107297192B (en) 2017-07-27 2017-07-27 Gas, solid and liquid reaction device

Publications (2)

Publication Number Publication Date
CN107297192A true CN107297192A (en) 2017-10-27
CN107297192B CN107297192B (en) 2023-06-27

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110813214A (en) * 2019-11-03 2020-02-21 安徽安丰堂动物药业有限公司 Production reaction kettle for improving uniformity of veterinary drug intermediates

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1043565A (en) * 1996-08-06 1998-02-17 Kubota Corp Agitator
CN2649203Y (en) * 2003-07-10 2004-10-20 上海恒永实业有限公司 Single-tube rotary joint for cooling rolls
CN101007997A (en) * 2007-01-04 2007-08-01 王书堂 Axial center aeration and jet-booster type stirring fermenter
CN201342344Y (en) * 2008-12-02 2009-11-11 中昊晨光化工研究院 Device for gas-liquid reactions/gas-liquid-solid reactions
CN201897027U (en) * 2010-07-16 2011-07-13 四川什邡东润制造有限公司 Rotary joint
US20120012597A1 (en) * 2010-07-19 2012-01-19 Caesar Rossitto Check Valve Drinking Device
CN102836665A (en) * 2012-09-19 2012-12-26 常州大学 Mixing stirrer with paddle with airflow driven by air pressure
CN103341336A (en) * 2013-06-17 2013-10-09 济南卡博唐生物科技有限公司 Stirrer of stirred tank
CN105289854A (en) * 2014-06-26 2016-02-03 湖北三宁化工股份有限公司 Mining flotation stirring paddle inflating device
CN205517495U (en) * 2016-04-27 2016-08-31 郑晓宁 Rotatory agitating unit
CN205627861U (en) * 2016-05-27 2016-10-12 泰和县飞尚林产有限公司 A agitating unit for middle level fat liquid recycle
CN206072347U (en) * 2016-09-30 2017-04-05 营口康辉石化有限公司 A kind of swivel joint mechanically-sealing apparatus
CN207126521U (en) * 2017-07-27 2018-03-23 浙江长江搅拌设备有限公司 A kind of gas, solid, liquid reaction unit

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1043565A (en) * 1996-08-06 1998-02-17 Kubota Corp Agitator
CN2649203Y (en) * 2003-07-10 2004-10-20 上海恒永实业有限公司 Single-tube rotary joint for cooling rolls
CN101007997A (en) * 2007-01-04 2007-08-01 王书堂 Axial center aeration and jet-booster type stirring fermenter
CN201342344Y (en) * 2008-12-02 2009-11-11 中昊晨光化工研究院 Device for gas-liquid reactions/gas-liquid-solid reactions
CN201897027U (en) * 2010-07-16 2011-07-13 四川什邡东润制造有限公司 Rotary joint
US20120012597A1 (en) * 2010-07-19 2012-01-19 Caesar Rossitto Check Valve Drinking Device
CN102836665A (en) * 2012-09-19 2012-12-26 常州大学 Mixing stirrer with paddle with airflow driven by air pressure
CN103341336A (en) * 2013-06-17 2013-10-09 济南卡博唐生物科技有限公司 Stirrer of stirred tank
CN105289854A (en) * 2014-06-26 2016-02-03 湖北三宁化工股份有限公司 Mining flotation stirring paddle inflating device
CN205517495U (en) * 2016-04-27 2016-08-31 郑晓宁 Rotatory agitating unit
CN205627861U (en) * 2016-05-27 2016-10-12 泰和县飞尚林产有限公司 A agitating unit for middle level fat liquid recycle
CN206072347U (en) * 2016-09-30 2017-04-05 营口康辉石化有限公司 A kind of swivel joint mechanically-sealing apparatus
CN207126521U (en) * 2017-07-27 2018-03-23 浙江长江搅拌设备有限公司 A kind of gas, solid, liquid reaction unit

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110813214A (en) * 2019-11-03 2020-02-21 安徽安丰堂动物药业有限公司 Production reaction kettle for improving uniformity of veterinary drug intermediates

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