CN107290506B - A kind of method of quantitative assessment reservoir diagenetic evolutionary process porosity Spatio-temporal Evolution - Google Patents
A kind of method of quantitative assessment reservoir diagenetic evolutionary process porosity Spatio-temporal Evolution Download PDFInfo
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Abstract
本发明提供了一种定量评价储层成岩演化过程中孔隙度时空演变的方法。包括:确定储层的成岩序列和孔隙度变化趋势,识别储层经历的主要成岩事件,建立成岩演化过程;分阶段模拟成岩演化过程,确定成岩演化过程、成岩时期和成岩条件;进行不同成岩时期的成岩作用室内实验,测试各成岩时期实验前后的流体成分、岩石样品成分及孔隙结构;与实验完全对应,进行不同成岩时期的成岩作用数值模拟,校正模拟中矿物动力学计算参数和比表面积;将数值模拟时间延长至储层的实际成岩时间,再次校正模型参数,建立孔隙度随时间演变的定量模拟系统;模拟区域范围上储层的演化过程,建立孔隙度随时空演变的定量模拟系统,实现孔隙度在空间随时间的定量评价和预测。
The invention provides a method for quantitatively evaluating the temporal and spatial evolution of porosity in the diagenetic evolution process of reservoirs. Including: determining the diagenetic sequence and porosity change trend of the reservoir, identifying the main diagenetic events experienced by the reservoir, and establishing the diagenetic evolution process; simulating the diagenetic evolution process in stages, determining the diagenetic evolution process, diagenetic period and diagenetic conditions; The laboratory experiment of diagenesis, testing the fluid composition, rock sample composition and pore structure before and after the experiment in each diagenetic period; completely corresponding to the experiment, carried out numerical simulation of diagenesis in different diagenetic periods, and corrected the mineral dynamics calculation parameters and specific surface area in the simulation; Extend the numerical simulation time to the actual diagenesis time of the reservoir, correct the model parameters again, and establish a quantitative simulation system for the evolution of porosity with time; simulate the evolution process of the reservoir on a regional scale, and establish a quantitative simulation system for the evolution of porosity with time and space, Realize the quantitative evaluation and prediction of porosity in space and time.
Description
技术领域technical field
本发明涉及石油勘探领域,具体的说,本发明涉及一种定量评价储层成岩演化过程中孔隙度时空演变的方法。The invention relates to the field of petroleum exploration, in particular, the invention relates to a method for quantitatively evaluating the temporal and spatial evolution of porosity in the diagenetic evolution process of reservoirs.
背景技术Background technique
油气资源已日益成为与国民经济、社会发展和国家安全息息相关的战略资源。无论是传统的、技术已经相对成熟的常规油气,还是新兴的、潜力巨大的页岩气、煤层气等非常规资源,均赋存于储层岩石孔隙或裂隙中。若要对其进行有效的开采,必须明确油气的成藏规律,对储层的孔隙度和渗透率等物性条件进行正确的评价。Oil and gas resources have increasingly become strategic resources closely related to national economy, social development and national security. Whether it is traditional conventional oil and gas with relatively mature technology or emerging unconventional resources such as shale gas and coalbed methane with great potential, they all occur in pores or fractures of reservoir rocks. If it is to be exploited effectively, the law of oil and gas accumulation must be clarified, and the physical properties such as porosity and permeability of the reservoir must be correctly evaluated.
油气资源的分布和物性主要受沉积作用和成岩作用的共同影响与控制:①沉积作用是指被运动介质搬运的物质到达适宜的场所后,由于条件改变而发生沉淀、堆积的过程的作用,沉积作用是影响储层质量的“先天”因素,决定着储层的空间分布和原始物性;②成岩作用是指沉积物沉积后至岩石固结的整个过程,沉积物沉积后,由于上覆沉积物的不断堆积,沉积物在埋藏过程中经历了不同类型和不同强度的成岩作用,对储层孔隙的形成、保存、破坏及储层的物性起着极为重要的作用。因此,成岩作用是影响储层质量的“后天”因素,决定着储层的最终物性,现今储层的孔隙度、渗透率等性质是成岩作用对其改造的结果。The distribution and physical properties of oil and gas resources are mainly affected and controlled by sedimentation and diagenesis: ①Sedimentation refers to the process of sedimentation and accumulation due to changes in conditions after the material transported by the moving medium reaches a suitable place. The effect is an "innate" factor affecting the quality of the reservoir, which determines the spatial distribution and original physical properties of the reservoir; ②Diagenesis refers to the whole process from sediment deposition to rock consolidation. During the burial process, the sediment experienced different types and different intensities of diagenesis, which played an extremely important role in the formation, preservation, destruction of reservoir pores and the physical properties of the reservoir. Therefore, diagenesis is an "acquired" factor that affects the quality of the reservoir, and determines the final physical properties of the reservoir. The properties such as porosity and permeability of the current reservoir are the result of its transformation by diagenesis.
成岩过程及其复杂,根据典型的成岩事件,可划分为多个连续的时期,每个时期均对应不同的埋深、温度、压力等条件,同时还有构造运动、外界流体侵入、烃源岩生成等多种因素的影响,在空间上也表现为非均质的特性。储层内主要发生的成岩作用有压实作用、胶结作用、交代作用、结晶作用、淋滤作用、水合作用和生物化学作用等。整个成岩过程基本都在有水的环境中进行,在漫长的成岩过程中,复杂的地下水溶液与围岩矿物长期接触,必然会发生一系列的物理、化学反应,导致矿物发生溶解或沉淀,引发储层孔隙度改变。因此,亟待明确成岩过程中不同的成岩条件下,储层内所发生的物理、化学作用对孔隙度的影响,也就是恢复成岩过程中孔隙度的时空演变过程,从而能准确的评价有利储层的分布,为油气勘探查明方向,提高开采效率。The diagenetic process is extremely complex. According to typical diagenetic events, it can be divided into several consecutive periods. Each period corresponds to different burial depth, temperature, pressure and other conditions. At the same time, there are tectonic movements, external fluid intrusion, source rocks, etc. Influenced by various factors such as generation, it also shows the characteristics of heterogeneity in space. The main diagenetic processes in the reservoir include compaction, cementation, metasomatism, crystallization, leaching, hydration, and biochemical processes. The entire diagenetic process basically takes place in an environment with water. During the long diagenetic process, a series of physical and chemical reactions will inevitably occur in the long-term contact between the complex underground aqueous solution and the surrounding rock minerals, resulting in the dissolution or precipitation of minerals, triggering Reservoir porosity changes. Therefore, it is urgent to clarify the influence of physical and chemical effects on the porosity in the reservoir under different diagenetic conditions, that is, to restore the spatiotemporal evolution of porosity in the diagenetic process, so as to accurately evaluate favorable reservoirs. The distribution of oil and gas can be used to find out the direction for oil and gas exploration and improve the production efficiency.
关于成岩过程中孔隙度的研究,目前的技术方案一方面是基于井点等地质资料,通过理论分析、岩石学测试和物理模拟等手段,模拟沉积充填史、埋藏史、热源演化史,恢复钙质胶结史、硅质胶结史、粘土矿物胶结史、长石矿物溶解史等,确定不同时期的典型成岩作用、强度和储层孔隙度的改变,基于岩石学测试等方法,确定储层原始孔隙保留和次生孔隙增减的情况,属于定性或者半定量的分析,得到的是孔隙度的整体曲线,未有随时间演变的定量分析与评价,未能精确地提供成岩过程中某个时间或某个区域的孔隙度具体数值。Regarding the study of porosity in the diagenetic process, on the one hand, the current technical scheme is based on geological data such as well points, and through theoretical analysis, petrological tests, and physical simulations, to simulate the history of sedimentary filling, burial, and heat source evolution to restore calcium The history of cementation, siliceous cementation, clay mineral cementation, feldspar mineral dissolution, etc., determine the typical diagenesis, strength and reservoir porosity changes in different periods, and determine the original pores of the reservoir based on petrological tests and other methods The increase and decrease of retained and secondary pores belong to qualitative or semi-quantitative analysis, and what is obtained is the overall curve of porosity. There is no quantitative analysis and evaluation of the evolution with time, and it cannot accurately provide a certain time or period during the diagenetic process. The specific value of porosity in a certain area.
另一方面,目前有少量文献基于地球化学理论研究成岩作用,运用热力学计算或数值模拟手段,评价某一成岩作用对孔隙度的改造,但是这些研究都是拘泥于单一的典型成岩作用,如白云石化作用、伊利石化作用,属于机理研究,并不能预测实际成岩过程中孔隙度的改变。然而,实际成岩作用包含多个成岩作用,过程及其复杂。目前,尚未有一种技术方案能够基于地质学、地球化学和计算机等综合知识,定量地评价和预测成岩过程中储层孔隙度随时空的演变。On the other hand, there are currently a small number of literatures that study diagenesis based on geochemical theories, and use thermodynamic calculations or numerical simulation methods to evaluate the transformation of porosity by a certain diagenesis, but these studies are all limited to a single typical diagenesis, such as the Baiyun Petrification and illite petrification belong to the study of mechanism, and cannot predict the change of porosity in the actual diagenesis process. However, the actual diagenesis includes multiple diagenesis, and the process is extremely complicated. At present, there is no technical solution that can quantitatively evaluate and predict the temporal and spatial evolution of reservoir porosity during diagenesis based on comprehensive knowledge of geology, geochemistry, and computers.
发明内容Contents of the invention
本发明的目的在于提供一种定量评价储层成岩演化过程中孔隙度时空演变的方法;该方法能够利用实验和数值模拟相结合的手段,准确地复制储层成岩演化过程,并定量恢复孔隙度随时间的演变曲线。The purpose of the present invention is to provide a method for quantitatively evaluating the temporal and spatial evolution of porosity in the diagenetic evolution of reservoirs; the method can accurately replicate the diagenetic evolution of reservoirs and quantitatively restore the porosity by means of combining experiments and numerical simulations evolution curve over time.
本发明通过系统性实验与数值模拟技术相结合,建立成岩演化过程中孔隙度的时空演变模拟系统,从而明确储层漫长复杂的成岩演化过程中储层孔隙度的演变规律,定量评价储层孔隙度随时间的演变趋势和在空间上的分布特征,揭示有利储层的形成机制和空间展布特征,该技术将为油气资源的勘探指明方向,提高油气的开采效率。The present invention combines systematic experiments with numerical simulation techniques to establish a simulation system for the temporal and spatial evolution of porosity in the diagenetic evolution process, thereby clarifying the evolution law of reservoir porosity in the long and complex diagenetic evolution process of the reservoir, and quantitatively evaluating the reservoir porosity The evolution trend of degree over time and the distribution characteristics in space reveal the formation mechanism and spatial distribution characteristics of favorable reservoirs. This technology will point out the direction for the exploration of oil and gas resources and improve the efficiency of oil and gas recovery.
本技术方案基于岩石学测试分析等定性化的数据,充分运用地球化学数值模拟技术,实现了孔隙度随时间和在空间上演变的定量化评价。This technical solution is based on qualitative data such as petrological test and analysis, and fully utilizes geochemical numerical simulation technology to realize quantitative evaluation of porosity evolution with time and space.
为达上述目的,一方面,本发明提供了一种定量评价储层成岩演化过程中孔隙度时空演变的方法,所述方法包括如下步骤:In order to achieve the above object, on the one hand, the present invention provides a method for quantitatively evaluating the temporal and spatial evolution of porosity in the process of reservoir diagenetic evolution, said method comprising the following steps:
(1)确定储层的成岩序列和孔隙度变化趋势,识别储层经历的成岩事件,选取对孔隙度有影响的成岩事件(如有机酸充注、二氧化碳侵入、异常高温高压等),划定多个典型的、连续的成岩时期(每个成岩时期存在多种可能的成岩条件,如有机酸充注的速率、充注量等),建立1种或多种可能的成岩演化过程;(1) Determine the diagenetic sequence and porosity change trend of the reservoir, identify the diagenetic events experienced by the reservoir, select the diagenetic events that affect the porosity (such as organic acid charging, carbon dioxide intrusion, abnormal high temperature and high pressure, etc.), delineate Multiple typical and continuous diagenetic periods (each diagenetic period has many possible diagenetic conditions, such as the rate and amount of organic acid charging, etc.), and establish one or more possible diagenetic evolution processes;
(2)分别模拟步骤(1)中所推测的成岩演化过程,将各成岩演化过程的模拟结果与储层实际的成岩序列和孔隙度变化趋势进行对比,选择其中的模拟结果与实际数据一致的成岩演过过程,则确定储层所经历的成岩演化过程、成岩时期和每个成岩时期的成岩条件;(2) Simulate the diagenetic evolution process inferred in step (1), compare the simulation results of each diagenetic evolution process with the actual diagenetic sequence and porosity change trend of the reservoir, and select the one whose simulation results are consistent with the actual data Diagenetic evolution process, then determine the diagenetic evolution process, diagenetic period and diagenetic conditions of each diagenetic period experienced by the reservoir;
(3)根据步骤(2)中所确定的成岩演化过程、成岩时期和每个成岩时期的成岩条件,开展不同成岩时期的高温高压成岩作用室内实验,测试各成岩时期实验前后的流体成分、岩石样品成分及孔隙结构;(3) According to the diagenetic evolution process, diagenetic period and diagenetic conditions of each diagenetic period determined in step (2), carry out laboratory experiments of high temperature and high pressure diagenesis in different diagenetic periods, and test the fluid composition and rock composition before and after the experiment in each diagenetic period. Sample composition and pore structure;
(4)与步骤(3)中的实验条件完全一致,进行不同成岩时期的成岩作用数值模拟,将每个成岩时期的模拟结果与实验结果进行对比,校正模拟中矿物动力学计算参数和比表面积;(4) The experimental conditions in step (3) are exactly the same, and the numerical simulation of diagenesis in different diagenetic periods is carried out, the simulation results of each diagenetic period are compared with the experimental results, and the mineral dynamics calculation parameters and specific surface area in the simulation are corrected ;
(5)将步骤(3)、(4)中的每个成岩时期的模拟时间(5-8天)延长至储层的实际成岩时间尺度(数十万年至数百万年),基于步骤(4)中校正过的模拟参数,进行实际成岩演化过程的数值模拟(数百万年),将模拟结果与步骤(1)中的储层成岩序列和孔隙度变化趋势进行对比,再次校正模型参数,建立孔隙度随时间演变的定量模拟系统;(5) Extend the simulation time (5-8 days) of each diagenetic period in steps (3) and (4) to the actual diagenetic time scale of the reservoir (hundreds of thousands to millions of years), based on the (4) Perform numerical simulation of the actual diagenetic evolution process (millions of years) with the corrected simulation parameters, compare the simulation results with the reservoir diagenetic sequence and porosity change trend in step (1), and calibrate the model again parameters to establish a quantitative simulation system of porosity evolution with time;
(6)基于区域范围内的地质和成岩数据,用已建立的孔隙度随时间演变的定量模拟系统,构建三维模型,模拟区域范围上储层的演化过程,与实际数据对比,最终建立孔隙度随时空演变的定量模拟系统,实现孔隙度在空间上随时间的定量评价和预测。(6) Based on the regional geological and diagenetic data, use the established quantitative simulation system of porosity evolution over time to construct a three-dimensional model to simulate the evolution process of the reservoir on the regional scale, compare with the actual data, and finally establish the porosity The quantitative simulation system of temporal and spatial evolution can realize the quantitative evaluation and prediction of porosity in space and time.
根据本发明一些具体实施方案,其中,步骤(1)是基于岩石学和地球化学,结合岩样薄片鉴定、岩样X射线衍射数据、流体包裹体和成熟度分析测试,确定储层的成岩序列和孔隙度变化趋势,识别储层经历的主要成岩作用,划分典型的、连续的成岩时期,建立成岩演化过程。According to some specific embodiments of the present invention, wherein, step (1) is based on petrology and geochemistry, combined with rock sample thin section identification, rock sample X-ray diffraction data, fluid inclusions and maturity analysis tests, to determine the diagenetic sequence of the reservoir and porosity change trends, identify the main diagenesis experienced by the reservoir, divide typical and continuous diagenetic periods, and establish the diagenetic evolution process.
根据本发明一些具体实施方案,其中,步骤(1)是通过室内岩石学测试分析、流体包裹体测试、同位素测试,明确储层的物源条件和热演化史,基于矿物转化关系和不同成岩时间节点的测试数据,确定储层的成岩序列和孔隙度变化趋势,推测储层的成岩演化过程,并根据对孔隙度的影响程度,将每种可能的成岩演化过程概化为连续的数个成岩时期。According to some specific embodiments of the present invention, wherein, step (1) is to clarify the provenance conditions and thermal evolution history of the reservoir through indoor petrological test analysis, fluid inclusion test, and isotope test, based on mineral transformation relationships and different diagenetic times According to the test data of the nodes, the diagenetic sequence and porosity change trend of the reservoir are determined, the diagenetic evolution process of the reservoir is inferred, and each possible diagenetic evolution process is generalized into several consecutive diagenetic evolution processes according to the degree of influence on the porosity. period.
根据本发明一些具体实施方案,其中,步骤(1)是根据对孔隙度的影响程度,将每种可能的成岩演化过程概化为连续的4-6个时期。According to some specific embodiments of the present invention, the step (1) is to generalize each possible diagenetic evolution process into 4-6 consecutive periods according to the degree of influence on porosity.
根据本发明一些具体实施方案,其中,步骤(1)是划定4-6个典型的、连续的成岩时期。According to some specific embodiments of the present invention, step (1) is to delineate 4-6 typical and continuous diagenetic periods.
根据本发明一些具体实施方案,其中,步骤(1)是建立3-5种可能的成岩演化过程。According to some specific embodiments of the present invention, step (1) is to establish 3-5 possible diagenetic evolution processes.
根据本发明一些具体实施方案,其中,步骤(2)是用模拟软件,分阶段模拟步骤(1)中所推测的成岩演化过程。According to some specific embodiments of the present invention, the step (2) uses simulation software to simulate the diagenetic evolution process estimated in the step (1) step by step.
根据本发明一些具体实施方案,其中,步骤(2)的模拟软件是多相流反应溶质运移模拟软件。According to some specific embodiments of the present invention, wherein the simulation software in step (2) is multiphase flow reaction solute migration simulation software.
所述多相流反应溶质运移模拟软件可以为目前市售常规的相应软件,譬如TOUGHREACT、TOUCHSTONE等。The multiphase flow reaction solute migration simulation software can be conventional corresponding software currently available on the market, such as TOUGHREACT, TOUCHSTONE and the like.
根据本发明一些具体实施方案,其中,步骤(2)的模拟结果包括岩石矿物成分、矿物沉淀/溶解趋势和孔隙度中的一种或多种。According to some specific embodiments of the present invention, wherein the simulation results of step (2) include one or more of rock mineral composition, mineral precipitation/dissolution tendency, and porosity.
根据本发明一些具体实施方案,其中,步骤(3)是用室内成岩作用物理模拟实验装置,进行不同成岩时期的高温高压反应实验,测试每个时期实验前后的流体成分、岩石样品成分及孔隙结构。According to some specific embodiments of the present invention, wherein, step (3) is to use the indoor diagenesis physical simulation experiment device to carry out high temperature and high pressure reaction experiments in different diagenetic periods, and test the fluid composition, rock sample composition and pore structure before and after the experiment in each period .
根据本发明一些具体实施方案,其中,步骤(3)每个时期实验时间为5-8天,共20-48天。According to some specific embodiments of the present invention, wherein, the experimental time of each period of step (3) is 5-8 days, a total of 20-48 days.
根据本发明一些具体实施方案,其中,步骤(3)是测量流体pH值及流体中典型离子的浓度。According to some specific embodiments of the present invention, wherein, step (3) is to measure the pH value of the fluid and the concentration of typical ions in the fluid.
根据本发明一些具体实施方案,其中,步骤(3)所述典型离子包括K+、Ca2+、Na+、Mg2 +、Al3+、Fe(含所有价态)、Cl-、Si(全Si测定)和SO4 2-中的一种或多种的组合。According to some specific embodiments of the present invention, wherein the typical ions in step (3) include K + , Ca 2+ , Na + , Mg 2 + , Al 3+ , Fe (including all valence states), Cl - , Si ( A combination of one or more of total Si measurement) and SO 4 2- .
其中可以理解的是,在本领域中,Fe的浓度测定是指各价态的铁离子总量;Si的浓度测定是指水溶液中全Si的测定。It can be understood that, in this field, the determination of the concentration of Fe refers to the total amount of iron ions in each valence state; the determination of the concentration of Si refers to the determination of the total Si in the aqueous solution.
根据本发明一些具体实施方案,其中,步骤(3)测试岩石样品成分包括对岩样进行了以下测试:①X射线衍射和光谱分析;②扫描电镜和薄片鉴定;③铸体薄片;④X射线微米CT。According to some specific embodiments of the present invention, wherein, step (3) testing rock sample composition includes carrying out following test to rock sample: 1. X-ray diffraction and spectral analysis; 2. scanning electron microscope and thin section identification; 3. casting thin section; .
根据本发明一些具体实施方案,其中,步骤(4)是基于步骤(3)中室内实验的条件,进行不同成岩时期的数值模拟,将模拟结果与实验结果进行对比,校正模拟参数。According to some specific embodiments of the present invention, wherein, step (4) is based on the conditions of the indoor experiment in step (3), numerical simulations of different diagenetic periods are carried out, the simulation results are compared with the experimental results, and the simulation parameters are corrected.
根据本发明一些具体实施方案,其中,步骤(4)进行不同成岩时期的成岩作用数值模拟,每个成岩时期的温度、压力、时间均与步骤(3)中相对应成岩时期的条件一致,将每个成岩时期的模拟结果与实验结果进行对比,校正模拟中矿物动力学计算参数和比表面积。According to some specific embodiments of the present invention, wherein, step (4) carries out the numerical simulation of diagenesis of different diagenetic periods, and the temperature, pressure, and time of each diagenetic period are all consistent with the conditions of corresponding diagenetic periods in step (3), and The simulation results of each diagenetic period were compared with the experimental results, and the mineral dynamics calculation parameters and specific surface area in the simulation were corrected.
根据本发明一些具体实施方案,其中,步骤(4)的模拟结果包括各矿物的相对含量、各离子的浓度和孔隙度。According to some specific embodiments of the present invention, the simulation results of step (4) include the relative content of each mineral, the concentration of each ion and the porosity.
综上所述,本发明提供了一种定量评价储层成岩演化过程中孔隙度时空演变的方法。本发明的方法具有如下优点:In summary, the present invention provides a method for quantitatively evaluating the spatiotemporal evolution of porosity during the diagenetic evolution of reservoirs. Method of the present invention has following advantage:
(1)以往关于成岩作用的研究大多是基于岩石学测试分析手段,定性或半定量地研究成岩序列和孔隙度演变。然而,地球化学作用在成岩过程中发挥着巨大的作用,尤其是对储层孔隙度有着直接的影响,甚至可以说决定了孔隙度的演变过程,因此用于计算地球化学作用的热力学及动力学理论极为重要。本发明将地球化学数值模拟技术运用到了成岩过程的研究中,结合热力学计算、室内实验、岩石学测试分析和天然类比等手段,相互验证,不仅恢复了孔隙度随时间的演变曲线,而且结合区域范围内的地质成岩特点,评价和预测区域范围内孔隙度的时空演变特征,从时间域和空间域两个方面研究成岩过程中孔隙度的演变特征,彻底实现了成岩过程中孔隙度评价和预测的定量化,在国内外尚未有此研究。(1) Most previous studies on diagenesis were based on petrological testing and analysis methods, qualitatively or semi-quantitatively studying diagenetic sequences and porosity evolution. However, geochemical action plays a huge role in the diagenesis process, especially has a direct impact on reservoir porosity, and can even be said to determine the evolution process of porosity, so it is used to calculate the thermodynamics and dynamics of geochemical action Theory is extremely important. The present invention applies the geochemical numerical simulation technology to the study of the diagenetic process, and combines thermodynamic calculations, laboratory experiments, petrological test analysis and natural analogy to verify each other, not only restores the porosity evolution curve with time, but also combines the regional Geological and diagenetic characteristics within the scope, evaluate and predict the temporal and spatial evolution characteristics of porosity within the regional scope, study the evolution characteristics of porosity during diagenesis from two aspects of time domain and space domain, and thoroughly realize the evaluation and prediction of porosity during diagenesis Quantification of , there is no such research at home and abroad.
(2)成岩过程及其复杂,是由多个阶段、多个子过程共同作用,它们之间相互影响、密切联系,以往关于成岩作用地球化学数值模拟的研究,往往局限于单个成岩作用,如白云石化作用、伊利石化作用等。本技术方案综合考虑所有成岩作用共同影响下的孔隙度演变特征,与实际储层的成岩过程一致,能为油气勘探提供更直接、更有价值的信息。(2) The diagenetic process is extremely complex, and it is composed of multiple stages and multiple sub-processes. They influence each other and are closely related. In the past, the research on the geochemical numerical simulation of diagenesis was often limited to a single diagenesis, such as the Baiyun Petrochemical, Yili petrochemical, etc. This technical solution comprehensively considers the characteristics of porosity evolution under the joint influence of all diagenesis, which is consistent with the diagenetic process of the actual reservoir, and can provide more direct and valuable information for oil and gas exploration.
(3)本发明技术方案是首次运用综合的地球化学理论综合研究多种复杂的成岩作用,与实际成岩一致。(3) The technical solution of the present invention is the first comprehensive study of various complex diagenesis using comprehensive geochemical theories, which is consistent with actual diagenesis.
(4)本发明技术方案,在初步概化(第一个步骤)后,增加了数值模拟工作,也就是在室内实验前通过数值模拟手段反复校正,确定成岩过程、成岩时期和成岩条件,如此再进行室内试验,成功率极高。此步骤非常关键,大大增加了该技术方案的成功率。(4) The technical solution of the present invention, after the preliminary generalization (the first step), increases the numerical simulation work, that is, repeatedly corrects by numerical simulation means before the indoor experiment, and determines the diagenetic process, diagenetic period and diagenetic conditions, so The indoor test is carried out again, and the success rate is extremely high. This step is critical and greatly increases the success rate of this technical solution.
附图说明Description of drawings
图1为实施例1过程流程图;Fig. 1 is the process flowchart of embodiment 1;
图2为实施例1成岩演化过程中水岩作用模型的示意图;Fig. 2 is the schematic diagram of water-rock interaction model in the diagenetic evolution process of embodiment 1;
图3为实施例1模拟结果与实验数据对比;Fig. 3 is the comparison of embodiment 1 simulation result and experimental data;
图4为实施例1孔隙度随地质时间的演变示意图;Fig. 4 is the schematic diagram of the evolution of porosity with geological time in Example 1;
图5为实施例1孔隙度和典型矿物的空间非均质分布示意图。Fig. 5 is a schematic diagram of spatial heterogeneity distribution of porosity and typical minerals in Example 1.
具体实施方式Detailed ways
以下通过具体实施例详细说明本发明的实施过程和产生的有益效果,旨在帮助阅读者更好地理解本发明的实质和特点,不作为对本案可实施范围的限定。The implementation process and beneficial effects of the present invention are described in detail below through specific examples, aiming to help readers better understand the essence and characteristics of the present invention, and not as a limitation to the scope of implementation of this case.
实施例1Example 1
研究背景Research Background
鄂尔多斯北部气田拥有巨大的油气资源量,石盒子组是主力产气层。经过漫长复杂的地质演化,石盒子组储层经受了一系列强烈的成岩作用,现今的平均孔隙度仅为0.06,平均渗透率仅为1mD,属于低孔低渗的致密砂岩储层,成岩作用的改造使储层具有较强的非均质性,导致致密砂岩气的开采遇到了“低渗、低压、低产、低丰度”的难题。目前,石盒子组致密砂岩储层的形成机制存在争议,储层发生致密的时间和过程尚不确定,也就是孔隙度的演变过程不清楚,导致致密砂岩气的开采效率低。通过本发明技术,能定量评价成岩演化过程中孔隙度随时间和空间的演变,明确储层致密化的机制,从而为致密砂岩气的开采提供指导。其具体过程如下:The northern Ordos gas field has huge oil and gas resources, and the Shihezi Formation is the main gas-producing layer. After a long and complicated geological evolution, the Shihezi Formation reservoir has undergone a series of intense diagenesis. The current average porosity is only 0.06, and the average permeability is only 1mD. It is a tight sandstone reservoir with low porosity and low permeability. The transformation of the reservoir makes the reservoir have strong heterogeneity, which leads to the problem of "low permeability, low pressure, low production and low abundance" in the exploitation of tight sandstone gas. At present, the formation mechanism of tight sandstone reservoirs in the Shihezi Formation is controversial, and the time and process of reservoir compaction are still uncertain, that is, the evolution process of porosity is unclear, resulting in low efficiency of tight sandstone gas recovery. The technique of the invention can quantitatively evaluate the evolution of porosity with time and space in the process of diagenetic evolution, clarify the mechanism of reservoir densification, and provide guidance for the exploitation of tight sandstone gas. The specific process is as follows:
1)通过一系列的室内岩石学测试分析、流体包裹体测试、同位素测试等,明确了石盒子组储层的成岩序列和孔隙度变化趋势,基于矿物转化关系和不同成岩节点的测试数据,推测石盒子组储层的成岩演化过程有4种可能,根据地球化学作用对孔隙度的影响程度,将每种可能的成岩演化过程概化为6个连续的典型时期(如图1所示):1) Through a series of indoor petrological test analysis, fluid inclusion test, isotope test, etc., the diagenetic sequence and porosity change trend of Shihezi Formation reservoirs are clarified. There are four possibilities for the diagenetic evolution process of Shihezi Formation reservoirs. According to the influence degree of geochemical action on porosity, each possible diagenetic evolution process can be generalized into six consecutive typical periods (as shown in Fig. 1):
①压实→早期浅埋藏成岩→异常高温高压→CO2充注→有机酸充注→晚期深埋藏成岩;①Compaction→early shallow burial diagenesis→abnormal high temperature and high pressure→CO 2 charging→organic acid charging→late deep burial diagenesis;
②压实→早期浅埋藏成岩→CO2充注→异常高温高压→有机酸充注→晚期深埋藏成岩;②Compaction→early shallow burial diagenesis→CO 2 charging→abnormal high temperature and high pressure→organic acid charging→late deep burial diagenesis;
③压实→早期浅埋藏成岩→有机酸充注→异常高温高压→CO2充注→晚期深埋藏成岩;③Compaction→early shallow burial diagenesis→organic acid charging→abnormal high temperature and high pressure→CO 2 charging→late deep burial diagenesis;
④压实→早期浅埋藏成岩→异常高温高压→有机酸充注→CO2充注→晚期深埋藏成岩;④Compaction→early shallow burial diagenesis→abnormal high temperature and high pressure→organic acid charging→CO 2 charging→late deep burial diagenesis;
同时,每个成岩时期的成岩条件也有多种可能,如有机酸、CO2充注的充注速率、充注量和充注时长等。At the same time, there are many possibilities for the diagenetic conditions of each diagenetic period, such as organic acids, CO 2 charging rate, charging amount, and charging time.
2)运用多相流反应溶质运移模拟软件TOUGHREACT,模拟以上推测的4种成岩演化过程,每种成岩演化过程分为6个时期模拟,且每个时期对应多种成岩条件(有机酸、CO2充注的充注速率、充注量和充注时长)。将各种模拟结果与储层的成岩序列和孔隙度变化趋势进行对比,确定石盒子组储层所经历的主要地球化学反应,矿物转化关系如式(1)-(4)所示。石盒子组储层经历了最初的压实和早成岩埋藏后,伴随油气充注,经历了大量CO2的入侵,对孔隙度的改变较大,随后地层发生了高温高压条件的突变,然后伴随着油气的第二次充注,有机酸注入,最后经历了晚期深埋藏成岩演化过程。总之,通过此步的数值模拟工作,得知石盒子组储层所经历的成岩演化过程与步骤1)中推测的第②种可能一致,而其他3种可能的成岩演化过程模拟结果均与步骤1)中实测数据所表现的趋势不一致。同时,通过数值模拟工作,确定了每个成岩阶段的温度、压力等成岩条件。2) Using the multiphase flow reaction solute migration simulation software TOUGHREACT to simulate the four diagenetic evolution processes speculated above, each diagenetic evolution process is divided into 6 periods of simulation, and each period corresponds to a variety of diagenetic conditions (organic acid, CO 2 charging rate, charging amount and charging time). Comparing various simulation results with the diagenetic sequence and porosity change trend of the reservoir, the main geochemical reactions experienced by the Shihezi Formation reservoir are determined, and the mineral transformation relationship is shown in equations (1)-(4). After the Shihezi Formation reservoir experienced initial compaction and early diagenetic burial, accompanied by oil and gas charging, it experienced a large amount of CO 2 intrusion, which greatly changed the porosity. The second charging of oil and gas, the injection of organic acids, and finally experienced the late deep burial diagenetic evolution process. In short, through the numerical simulation work in this step, it is known that the diagenetic evolution process experienced by the Shihezi Formation reservoir is consistent with the second possibility speculated in step 1), while the simulation results of the other three possible diagenetic evolution processes are all consistent with the diagenetic evolution process in step 1). 1) The trends shown in the measured data are inconsistent. At the same time, through numerical simulation work, the diagenetic conditions such as temperature and pressure of each diagenetic stage are determined.
CaCO3(方解石)+H+→Ca2++HCO3 - CaCO 3 (calcite)+H + →Ca 2+ +HCO 3 -
长石类矿物+H2O+H+→(K+,Na+,Ca2+)+SiO2+高岭石Feldspar minerals+H 2 O+H + →(K + ,Na + ,Ca 2+ )+SiO 2 +kaolinite
高岭石+K+→伊利石+H2O+H+ Kaolinite+K + → illite+H 2 O+H +
蒙皂石+K++Al3+→伊利石+Na++Ca2++Fe3++Mg2++Si4+ Smectite + K + +Al 3+ → illite + Na + +Ca 2+ +Fe 3+ +Mg 2+ +Si 4+
3)在实验室,用成岩模拟系统实验装置进行了这6个成岩时期的高温高压反应实验,第一个时期8天,其他时期均6天。其中,初始岩样成分和流体浓度是根据步骤1中的研究区岩石学测试结果进行反推的,表1和表2分别是初始岩样成分和成岩演化过程的流体浓度。实验中各个阶段的温度、压力等主要参数均取自于步骤2,如表3所示。3) In the laboratory, the high-temperature and high-pressure reaction experiments of the six diagenetic periods were carried out with the experimental device of the diagenetic simulation system. The first period was 8 days, and the other periods were 6 days. Among them, the initial rock sample composition and fluid concentration are inversely deduced based on the petrological test results in the study area in step 1. Table 1 and Table 2 are the initial rock sample composition and fluid concentration during diagenetic evolution, respectively. The main parameters such as temperature and pressure in each stage of the experiment are taken from Step 2, as shown in Table 3.
表1初始岩样配制中各矿物的相对含量Table 1 The relative content of each mineral in the initial rock sample preparation
表2实验中各流体的浓度(mg/L)The concentration of each fluid in the experiment of table 2 (mg/L)
表3成岩演化过程中各阶段的实验条件Table 3 Experimental conditions in each stage of diagenetic evolution
收集各个成岩时期反应后的岩样和水样,水样冷却至常温,过滤,测量pH值及溶液中典型离子(K+、Ca2+、Na+、Mg2+、Al3+、Fe、Cl-、Si和SO4 2-)的浓度;对岩样进行了以下测试:①X射线衍射(XRD)和光谱分析(XRF),测试岩样中矿物和元素含量。②扫描电镜(SEM)和薄片鉴定,观察岩石表面矿物的溶蚀或沉淀特征。③铸体薄片,测量并计算岩样的面孔率。④X射线微米CT,扫描岩样的孔隙结构和面孔特征。Collect rock samples and water samples after the reaction of each diagenetic period, cool the water samples to room temperature, filter, measure the pH value and typical ions in the solution (K + , Ca 2+ , Na + , Mg 2+ , Al 3+ , Fe, Cl - , Si and SO 4 2- ); the following tests were carried out on the rock samples: ① X-ray diffraction (XRD) and spectroscopic analysis (XRF) to test the mineral and element contents in the rock samples. ② Scanning electron microscope (SEM) and thin section identification to observe the dissolution or precipitation characteristics of minerals on the rock surface. ③Cast thin section, measure and calculate the surface porosity of the rock sample. ④ X-ray micro-CT scans the pore structure and face features of rock samples.
4)基于室内实验的条件,进行成岩演化过程(包括不同成岩时期)的数值模拟,模型示意图如图2所示,将模拟结果与实验结果进行对比,如图3所示,校正模拟矿物动力学计算参数和比表面积。4) Based on the conditions of the laboratory experiment, the numerical simulation of the diagenetic evolution process (including different diagenetic periods) is carried out. The schematic diagram of the model is shown in Figure 2. The simulation results are compared with the experimental results, as shown in Figure 3, and the simulated mineral dynamics is corrected. Calculate parameters and specific surface area.
5)延长每个成岩时期的模拟时间,进行储层实际成岩时间尺度的成岩演化过程模拟,共280百万年。将模拟结果与实测数据进行对比,校正模型参数,建立了孔隙度随时间演变的定量模拟系统。孔隙度的演变曲线如图4所示,孔隙度经过压实作用,由初期的30%降至15%,早成岩时期孔隙度基本保持不变,随着CO2气体的充注,矿物溶蚀,孔隙度增加,但停止注入之后,且温度和压力增加,导致大量碳酸盐岩沉淀,孔隙度急剧降至10%以下,储层发生致密,也就是说,伴随油气的第一次充注,CO2气体的侵入对储层的致密化起到了关键作用,后期的有机酸充注和成藏对孔隙度的影响不大。5) Extend the simulation time of each diagenetic period, and simulate the diagenetic evolution process of the actual diagenetic time scale of the reservoir, a total of 280 million years. The simulation results were compared with the measured data, the model parameters were corrected, and a quantitative simulation system of porosity evolution with time was established. The evolution curve of porosity is shown in Fig. 4. After compaction, the porosity decreased from 30% at the initial stage to 15%. The porosity remained basically unchanged during the early diagenetic period. With the charging of CO2 gas, minerals were dissolved, The porosity increases, but after the injection is stopped, and the temperature and pressure increase, a large amount of carbonate rocks are precipitated, the porosity drops sharply below 10%, and the reservoir becomes tight, that is, with the first oil and gas charging, The intrusion of CO 2 gas played a key role in the densification of the reservoir, and the late organic acid charging and accumulation had little effect on the porosity.
6)基于研究区区域范围内的物源和成岩数据,构建三维模型,模拟区域范围上储层的成岩演化过程,模拟结果如图5所示。结果表明,模拟结果与区域实测数据一致,均表现为整体以长石类矿物的溶解为主,转化为伊利石,并生成铁白云石和片钠铝石沉淀。但是,初始矿物和孔隙度、渗透率的非均质导致成岩作用在区域上表现为非均质,最终孔隙度呈现非均质状态,储层发生了不同程度的致密化。根据模拟的孔隙度在空间上的分布,能够评价有利储层。6) Based on the provenance and diagenetic data in the study area, a three-dimensional model was constructed to simulate the diagenetic evolution process of the reservoir on the regional scale. The simulation results are shown in Figure 5. The results show that the simulated results are consistent with the measured data in the area, and they all show that the overall dissolution of feldspar minerals is dominated by the transformation into illite, and the formation of anodolomite and dawsonite precipitation. However, the heterogeneity of initial minerals, porosity and permeability lead to regional heterogeneity of diagenesis, resulting in heterogeneity of final porosity, and different degrees of densification of the reservoir. From the simulated spatial distribution of porosity, favorable reservoirs can be evaluated.
本发明技术方案通过系列实验与模拟相结合,提出了一套完整的、科学的、系统的评价孔隙度的方法,能够建立孔隙度随时空演变的定量模拟系统,不仅恢复漫长成岩演化过程中孔隙度的演变曲线,而且能够实现孔隙度在空间上的定量评价和预测,既查明了储层的致密化机理,又能为油气等资源的勘探指明方向,提高开采效率。The technical scheme of the present invention combines a series of experiments and simulations, and proposes a complete, scientific, and systematic method for evaluating porosity, which can establish a quantitative simulation system for porosity evolution over time and space, and not only restores porosity in the long process of diagenetic evolution The evolution curve of porosity can be realized, and the quantitative evaluation and prediction of porosity in space can be realized, which can not only find out the densification mechanism of the reservoir, but also point out the direction for the exploration of oil and gas and other resources, and improve the production efficiency.
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