CN107271606A - The method for assessing effect of personal care product - Google Patents
The method for assessing effect of personal care product Download PDFInfo
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- CN107271606A CN107271606A CN201710303324.6A CN201710303324A CN107271606A CN 107271606 A CN107271606 A CN 107271606A CN 201710303324 A CN201710303324 A CN 201710303324A CN 107271606 A CN107271606 A CN 107271606A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0098—Plants or trees
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
- G01N33/025—Fruits or vegetables
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Abstract
A kind of method for assessing personal care product or hydration effect of its composition, methods described includes:Select Part I fresh plant tissue;Part I plant tissue is handled with the personal care product or its composition;And treated Part I plant tissue is heated to 35 to 80 DEG C of drying temperature.
Description
The application is Application No. 201480039428.5, entitled " method for assessing effect of personal care product "
Divisional application.
Technical field
The present invention relates to a kind of method for assessing personal care product or hydration effect of its composition.Especially the present invention is related to
And the method more rapidly and immediately assessed using producing is to the hydration work(of personal care product such as skin or hair care product
The detection of effect.
Background technology
The personal care product for improving the state of skin or hair be often designed to by influence skin or hair absorb and/
Or keep the ability of moisture to play a role.Regrettably, however the benefit of such product will not be felt by user at once,
And can actually expend a few hours, even a couple of days reuses to obtain consumer-realizable benefit.
Internal and external instrument detection to the hydration status of tissue is often laboratory that is complicated and/or being related to costliness
Equipment.In addition, it is such detection often obtain numerical parameter, its for unprofessional person indigestion or at least with desired production
Product effect is connected.
The present inventor thereby determined that so the need for there is provided the method for the hydratability that can prove cosmetics, still
This method does not need particular device and/or easily connected with consumer's interests.
U.S. Patent Publication US4,373,382 (Nicole A.A.Brun) discloses a kind of production for determining to be ready to use in skin
The method of the aquation of product, wherein product to be measured is applied at least a portion of the first vegetable sample such as apple surface,
And at least another untreated sample of first sample and same vegetables under identical reservoir conditions together with store, and
And compare the surface change of these samples.
Although US4,373,382 method is not necessarily to the instrument of complexity, and effective by the state change of vegetables base material
Ground illustrates consumer benefits, but this method still needs consuming a couple of days or a few weeks longer to show obvious effect.Therefore, US4,
373,382 method is not suitable for needing situation that is quick or even showing product efficacy immediately.Such situation is included for example, storehouse
Deposit or point of sale explanation.
The present inventor by providing specific method it has now been discovered that can improve some or all of drawbacks described above.
The content of the invention
In a first aspect, the invention provides a kind of method of the hydration effect for assessing personal care product or its composition,
Methods described includes:
(i) Part I fresh plant tissue is selected;
(ii) Part I plant tissue is handled with the personal care product or its composition;With
(iii) treated Part I plant tissue is heated to 35 to 80 DEG C of drying temperature.
Present invention also offers following technical scheme:
1st, a kind of method for assessing personal care product or hydration effect of its composition, methods described includes:
(i) Part I fresh plant tissue is selected;
(ii) the Part I plant tissue is handled with the personal care product or its composition;With
(iii) treated Part I plant tissue is heated to 35 to 80 DEG C of drying temperature;
The selection Part II fresh plant tissue wherein in step (i);With control agent product treatment in step (ii)
The Part II;Treated Part II is also handled in heating stepses (iii);
And further, wherein then step (iii), methods described includes assessing treated Part I
The step of at least one attribute (iv), planted wherein the evaluated attribute is treated Part I relative to fresh
The change of thing tissue and/or characteristic relative to treated Part II;With
The duration of wherein described heating stepses (iii) is 10s to 1 hours;
Wherein described plant tissue includes petal, leaf or combinations thereof.
2nd, according to the method for the 1st, wherein the control agent is water.
3rd, according to the method for the 1st or 2, wherein the characteristic is outward appearance and/or engineering properties.
4th, the method according to foregoing any one, wherein the plant tissue includes petal.
5th, the method according to foregoing any one, wherein in step (ii), the Part I plant tissue bag
Waterborne liquid processing containing the composition.
6th, according to the method for the 5th, wherein concentration by weight of the composition in waterborne liquid be more than it is described into
Divide the concentration by weight in the personal care product.
7th, the method according to foregoing any one, wherein the duration of the heating stepses (iii) is 1 to 20 points
Clock.
8th, the method according to foregoing any one, wherein the heating stepses (iii) are included treated plant group
Knit and contacted with stream of hot air.
9th, the method according to foregoing any one, wherein the drying temperature is less than 70 DEG C.
10th, according to the method for the 9th, wherein the drying temperature is in the range of 40 to 70 DEG C.
11st, the method according to foregoing any one, wherein the product is hair care product.
12nd, the method according to foregoing any one, wherein the composition is selected from polyalcohol, fats material, esters profit
Skin agent, hydro carbons emollient, silicone oil, vitamin, plant extracts or their mixture.
Fresh plant tissue is found to be the base material to moisture-sensitive, and is visually often noticeable.Separately
Outside, by using the drying temperature from 35 to 80 DEG C, plant tissue can cause rapidly and vision-significantly change because drying
Become, and without heat-caused infringement, for example, burn, burn, bubbling, boiling or other cook.
By considering following detailed description and embodiment, every other aspect of the invention will become more readily clear.
Embodiment
The method of the present invention includes step (i) and selects Part I fresh plant tissue.The plant tissue can be whole
Individual plant, flower, leaf, petal, stem, fruit, seed or root, and/or their fragment.More preferably petal, leaf or it
Combination because these are typically relative thin, but with big surface area, and therefore drying is relatively rapid.It is optimal
Plant tissue described in selection of land is petal or its fragment, because petal is generally more crisp for leaf, and therefore for
Drying shows visually more noticeable change.
The plant tissue of " fresh " means that tissue is not dried by water content less than 30% (by weight), and
It generally has the water content of 60-95% scopes.The method of the present invention is preferably used removes tissue (for example from plant living
By harvesting, trimming and/or cut) fresh plant tissue within 24 hours, within more preferably 12 hours, more preferably
For within 6 hours and within most preferably 10 seconds to 3 hours.
Particularly rapidly dried to reach, preferably described Part I is not too big.In particular it is preferred to described first
Part has the quality less than 10g, more preferably less than 2g, more preferably less than 1g, even more preferably less than 0.5g
And more preferably less than 0.2g.
But the Part I should not be too small.Especially, the Part I should be Glassless.Preferably
The Part I has at least 1mg quality, more preferably at least 10mg, and most preferably at least 50mg.
The method of the present invention includes step (ii) and uses personal care product or its composition processing Part I plant tissue.
The personal care product is preferably that intention is applied to hair and/or skin, for the purpose of changing their situation
Personal care product.Especially, the product be preferably be intended to improve hair and/or skin selected from hydration, barrier functionality,
Moisture holding capacity and the situation of combinations thereof.Preferably described product is hair care product, is especially intended to improve scalp condition
Hair care product.
The processing includes at least contacting Part I with the product or composition.The contact can be for example including inciting somebody to action
The product or composition spread at least one surface of the part.10008 additionally or alternatively, the contact can include
The part is immersed in the liquid comprising the product or composition.The processing is additionally may included in and the product or composition
The part is rinsed after contact.If the product is rinse-off products such as skin cleaner, shower cream, shampoo or hair
Conditioner, rinse step is particularly preferred.
In a preferred embodiment, the Part I described in step (ii) is handled with the composition of personal care product.Make
The part is handled with composition rather than whole product to be allowed, for example, the composition is by with the concentration higher than in the product
It is applied to the part and/or with different from applying by way of applying whole product and obtaining.Therefore the water of the composition
Closing effect can be reinforced that hydration effect is presented in a short time.Preferably described Part I plant tissue uses bag
Waterborne liquid processing containing the composition.The concentration (weight) of composition is produced more than personal nursing more preferably described in waterborne liquid
The concentration (weight) of composition described in product.The concentration (weight) of composition can be personal care product for example described in waterborne liquid
Described at least 2 times, more preferably at least 3 times, more preferably at least 5 times of concentration (weight) of composition and most preferably at least
10 times.
The composition can be associated with the product in some manner." association " represents that methods described is preferably included really
The fixed composition as the product component the step of.For example, before step (i), methods described can include selection and use
In the composition of the personal care product of assessment.10008 additionally or alternatively, methods described can include (such as literary by mark
Word, video, audio etc.) the step of the composition is associated as into the component of personal care product.
The composition should the composition selected from the hydration effect having had.Such as described composition is preferably or at least included
NMF, emollient, bioactivator or combinations thereof.Most preferably the composition includes or is polyalcohol, fat material
(such as oil, fatty alcohol, aliphatic acid and/or soaps), ester emollients, hydro carbons emollient, silicone oil, vitamin, plant extracts,
Or their mixture.
It is preferred that polyalcohol include PAG and more preferably alkylidene polyol and their derivative,
Including propane diols, DPG, polypropylene glycol, polyethylene glycol and their derivative, sorbierite, hydroxypropyl sorbitol, oneself two
Alcohol, 1,3 butylene glycol, isoprene, 1,2,6- hexanetriols, glycerine, ethoxylated glycerine, propoxylated glycerine and it
Mixture.Most preferably glycerine (also referred to as glycerine).
Silicone oil can be divided into volatility and non-volatile type.Terms used herein " volatility " is referred in environment
There are those materials of measurable vapour pressure at temperature (25 DEG C).Volatile silicone oils are preferably chosen from containing from 3 to 9, preferably
From the ring-type (cyclomethicone) or linear polydimethylsiloxane- of 4 to 5 silicon atoms.
Non-volatile silicone oil as emollient materials includes polyalkylsiloxane, Polyalkylaryl siloxane and polyethers silicon
Siloxane copolymers.Substantial Non-volatile polyalkylsiloxane for this paper includes, such as dimethyl silicone polymer, and it glues
Spend at 25 DEG C about 5 × 10-6To 0.1m2/s.Preferred non-volatile emollients for this composition are poly dimethyl silicon
Oxygen alkane, its viscosity is about 1 × 10 at 25 DEG C-5To about 4 × 10-4m2/s。
Organopolysiloxane cross-linked polymer can be used effectively.It is representative for dimethyl in these materials
Siloxanes/vinyldimethylsiloxane cross-linked polymer and dimethicone crosspolymers, it is from multiple suppliers
Can obtain including Dow Coming (9040,9041,9045,9506 and 9509), General Electric (SFE 839),
Shin Etsu (KSG-15,16 and 18 [dimethyl siloxane/phenyl vinyl dimethicone crosspolymers]), and
Grant Industries (Gransil boards material), and dodecyl dimethyl siloxanes/vinyl that Shin Etsu are provided
Dimethicone crosspolymers (such as KSG-31, KSG-32, KSG-41, KSG-42, KSG-43 and KSG-44).
It is different that the specific embodiment of fat material includes stearyl alcohol, glyceryl monoricinoleate, ermine oil, cetanol, isostearic acid
Propyl ester, stearic acid, isobutyl palmitate, Standamul 7061, oleyl alcohol, isopropyl laurate, lauric acid hexyl ester, the oleic acid last of the ten Heavenly stems
Ester, octadecane -2- alcohol, different cetanol, eicosanol, docosanol, cetin, two-N-butyl of decanedioic acid, myristic acid are different
Propyl ester, isopropyl palmitate, isopropyl stearate, butyl stearate, polyethylene glycol, triethylene glycol, lanolin, cocoa butter, jade
Rice bran oil, cottonseed oil, olive oil, palm-kernel oil, rapeseed oil, safflower seed oil, evening primrose oil, soybean oil, sunflower oil, avocado oil,
Sesame oil, coconut oil, peanut oil, castor oil, acetulan, vaseline, mineral oil, cardamom acid butyl ester, isostearic acid,
Palmitic acid, linoleic acid isopropyl ester, Lauryl lactate, Tetradecyl lactate, decyl oleate, myristic acid cardamom ester and theirs is mixed
Compound.
Have in ester emollients:
A) there is the alkenyl or Arrcostab of the aliphatic acid of 10 to 20 carbon atoms.The example include the different peanut ester of neopentanoic acid,
The oily alkene ester of Dermol 105, isononyl isononanoate, ricinoleic acid cetyl, myristic acid, the oily alkene ester of stearic acid and oleic oil alkene
Ester.
B) fatty acid ester of ether-ester such as ethoxylized fatty alcohol.
C) polyol ester.Butanediol, ethylene glycol list and the single- and di- fatty acid ester of two-fatty acid ester, diethylene glycol, poly- second
It is glycol (200-6000) single- and di- fatty acid ester, the single- and di- fatty acid ester of propane diols, the monoleate of polypropylene glycol 2000, poly-
The monostearate of propane diols 2000, ethoxylated propylene glycol monostearate, the single- and di- fatty acid ester of glyceryl, polyglycereol
Poly- fatty ester, ethoxylated glycerol base list-stearate, 1,3 butylene glycol monostearate, 1,3 butylene glycol distearyl acid
Ester, polyoxyethylene polyol fatty acid esters, sorbitan fatty acid esters and polyoxyethylene sorbitan fatty acid esters
It is gratifying polyol ester.It is especially useful that C1-C30Pentaerythrite, trimethylolpropane and the DOPCP of alcohol.
Exemplary is pentaerythrite tetraethyl capronate.
D) wax ester such as beeswax, spermaceti and tribehenin wax.
E) sterol ester, wherein cholesterol fatty acid ester are the examples.
F) sugar ester of aliphatic acid, the poly- behenate of such as sucrose and the poly- cottonseed acid esters of sucrose.
Useful hydrocarbon includes vaseline, mineral oil, C11-C13Isoparaffin, polyalphaolefin, and special isohexadecane.
The duration of process step (ii), that is, start to apply personal care product or composition and heating step to plant tissue
Suddenly the time between the beginning of (iii) is preferably between 1s and 24 hour.However, this method may be particularly suitable for wherein
Expect at the situation of quick displaying product efficacy, such as stock and/or point of sale.It is therefore preferred to the duration of process step
Less than 2 hours, even more preferably less than 1 hour, even more preferably less than 30 minutes and more preferably less than 10 minutes.
The method of the present invention includes the drying of the heat-treated Part I plant tissue to 35 to 80 DEG C of step (iii)
Temperature.
In order to provide even more rapid drying, preferably drying temperature is at least 40 DEG C, most preferably at least 45 DEG C.
In order to ensure causing rapid and vision-obvious change by drying on plant tissue, without heat-initiation
Infringement, preferably described plant tissue is not kept the long time at too high a temperature.It is therefore preferred to holding for heating stepses
The temperature of continuous time, i.e. plant tissue is in the time of drying temperature for 10s to 1 hours, more preferably 30s to 40 minutes,
More preferably 1 to 20 minutes, and most preferably between 2 to 10 minutes.10008 additionally or alternatively, drying temperature be less than
75 DEG C, more preferably less than 70 DEG C, most preferably less than 60 DEG C.
Heating can be carried out in any convenient manner.Such as heating stepses can include will be treated plant tissue with
Stream of hot air contact for example from hair-dryer.10008 additionally or alternatively, heating stepses can be included treated plant
Tissue is handled in an oven.
Then step (iii), methods described preferably includes at least one that step (iv) assesses treated Part I
Individual attribute.Most preferably, the attribute of assessment is outward appearance, such as size, shape, surface texture, color or combinations thereof.In addition
Ground or alternately, it can be estimated that mechanical property is such as brittleness, fragility.
When for assessing personal care product or composition relative to the hydration effect for compareing agent, method of the invention is special
It is not effective.Therefore in most preferred embodiments, methods described includes middle selection Part II fresh plant in step (i)
Tissue;With control agent product treatment Part II in step (ii);With processing is treated in heating stepses (iii) second
Part.
Part II should be substantially identical with Part I, such as in the species of vegetable material and shape and size side
Face.
It can be any component different from personal care product to be measured or composition to compare agent.But most preferably, control
Agent is water (or comprising at least 99 weight % water, more preferably 99.9-100% in control agent product).
Evaluation attribute in step (iv) is preferably treated Part I relative to fresh plant tissue and/or phase
For the change of the characteristic of treated Part II.Characteristic is preferably outward appearance and/or mechanical property.
In one embodiment, methods described include capture one or more vegetable material image and store and/or
The step of transmitting one or more image.One or more image can be stored for example on the recordable medium for example
CD, flash memory or other computer-readable memories.One or more image can be sent for for example at one or many
Shown on individual visible display device.Suitable visible display device includes such as monitor, TV screens and/or mobile device screen
Curtain.
Except in embodiment, or other places for being explicitly indicated, the amount or reaction condition, material of material are represented in this specification
The physical characteristic of material and/or all numerals used can optionally be interpreted as being modified by word " about ".
All contents are in terms of the weight of product, unless otherwise prescribed.
It should be noted that in specific any number range, any specific higher limit can be with any certain lower limit value
It is associated.
In order to avoid producing doubt, word " comprising " means "comprising" but is not necessarily " being made up of what " or " by what
Composition ".In other words, listed step or option are not exhaustive.
The content of the invention disclosed herein, which is considered as covering, is present in owning in multinomial dependent claims each other
Embodiment, no matter not the fact that claim does not have multinomial subordinate or redundancy.
Following examples are provided to help to understand the present invention.Embodiment is not intended to limit the scope of claim.
Embodiment
Embodiment 1
Test sample is by by 7.5gShampoo, 7.5gHair conditioner is mixed with 35g water
Close to prepare.Shampoo includes 0.05%w/w glycerine and 0.01%w/w Radix et Caulis Opuntiae Dillenii extracts.Hair conditioner is sweet comprising 0.1%
Oil and 0.01%w/w Radix et Caulis Opuntiae Dillenii extracts.
Control agent is 50g water.
Four petals are derived from oenothera biennis (pink blossom oenothera biennis (oenothera rosea)) plant.Two panels is positioned over test specimens
In product and two panels be positioned over control agent in.Removed in petal after submerging 5 minutes from test sample and control agent, and
5s is each rinsed in circulating water.
Rinsed petal, which is spread, to be opened onboard, and is placed in baking oven and is pre-heated to 50 DEG C.Petal after 15 minutes
Removed from baking oven, and carry out visual inspection.
It was observed that the petal treated with test sample still appears as fresh petal, and show seldom take off
Water mark as.On the contrary, obvious dehydration sign is shown with the treated petal of control agent, including shrinkage, surface wrinkling and face
Discoloration is deep.
Embodiment 2
For effect of some compositions for confirming the hair care product described in embodiment 1, test sample passes through will
7.5g glycerine, 1.5g Radix et Caulis Opuntiae Dillenii extracts and 41g water mix to prepare.
Control agent is 50g water.
Four petals are derived from oenothera biennis (pink blossom oenothera biennis) plant.Two panels is positioned in test sample and two panels is positioned over
Compare in agent.Removed in petal after submerging 5 minutes from test sample and control agent.Petal is allowed to carry out several seconds of draining
Clock does not still implement rinse step.
Treated petal, which is spread, to be opened onboard, and is placed in baking oven and is pre-heated to 50 DEG C.Petal after 15 minutes
Removed from baking oven, and carry out visual inspection.
It was observed that the petal treated with test sample still appears as fresh petal, and show seldom take off
Water mark as.On the contrary, showing visible dehydration sign, including shrinkage, surface wrinkling and face with the treated petal of control agent
Discoloration is deep.
Claims (15)
1. a kind of method for being used to show the result for assessing hydration effect of personal care product or its composition, methods described bag
Include:
(i) Part I fresh plant tissue is selected;
(ii) the Part I plant tissue is handled with the personal care product or its composition;With
(iii) treated Part I plant tissue is heated to 35 to 80 DEG C of drying temperature;Wherein selected in step (i)
Select Part II fresh plant tissue;With Part II described in control agent product treatment in step (ii);In heating stepses
(iii) treated Part II is also handled in;
And further, wherein then step (iii), methods described includes assessing treated Part I at least
The step of one attribute (iv), wherein the evaluated attribute be treated Part I relative to fresh plant group
Knit and/or characteristic relative to treated Part II change;The assessment result to user is shown (v);
The duration of wherein described heating stepses (iii) is 10s to 1 hours;
Wherein described plant tissue includes petal, leaf or combinations thereof.
2. method according to claim 1, wherein the control agent is water.
3. according to the method for claim 1 or 2, wherein the characteristic is outward appearance and/or engineering properties.
4. the method according to any one of preceding claims, wherein the plant tissue includes petal.
5. the method according to any one of preceding claims, wherein in step (ii), the Part I plant tissue
Handled with the waterborne liquid comprising the composition.
6. method according to claim 5, wherein concentration by weight of the composition in waterborne liquid be more than it is described into
Divide the concentration by weight in the personal care product.
7. the method according to any one of preceding claims, wherein the duration of the heating stepses (iii) is 1 to 20
Minute.
8. the method according to any one of preceding claims, wherein the heating stepses (iii) are included treated plant
Thing tissue is contacted with stream of hot air.
9. the method according to any one of preceding claims, wherein the drying temperature is less than 70 DEG C.
10. method according to claim 9, wherein the drying temperature is in the range of 40 to 70 DEG C.
11. the method according to any one of preceding claims, wherein the product is hair care product.
12. the method according to any one of preceding claims, wherein the composition is selected from polyalcohol, fats material, ester
Class emollient, hydro carbons emollient, silicone oil, vitamin, plant extracts or their mixture.
13. the method according to any one of preceding claims, wherein methods described also include one or more plant of capture
The image of material and the step of store and/or transmit a kind of described or multiple images;One or more image can be passed
Send for being shown on one or more visible display devices.
14. a kind of side for the recording medium for preparing the result for showing the hydration effect for assessing personal care product or its composition
Method, methods described includes:
(i) Part I fresh plant tissue is selected;
(ii) the Part I plant tissue is handled with the personal care product or its composition;With
(iii) treated Part I plant tissue is heated to 35 to 80 DEG C of drying temperature;Wherein selected in step (i)
Select Part II fresh plant tissue;With Part II described in control agent product treatment in step (ii);In heating stepses
(iii) treated Part II is also handled in;
And further, wherein then step (iii), methods described includes assessing treated Part I at least
The step of one attribute (iv), wherein the evaluated attribute be treated Part I relative to fresh plant group
Knit and/or characteristic relative to treated Part II change;
The duration of wherein described heating stepses (iii) is 10s to 1 hours;
Wherein described plant tissue includes petal, leaf or combinations thereof, and
The image of the vegetable material of one or more above method acquisition is captured, and is stored it on recordable media.
15. a kind of show vegetable material image to show the water of assessment personal care product or its composition on visible display device
The method for closing the result of effect, wherein described image are captured and stored during following:
(i) Part I fresh plant tissue is selected;
(ii) the Part I plant tissue is handled with the personal care product or its composition;With
(iii) treated Part I plant tissue is heated to 35 to 80 DEG C of drying temperature;Wherein selected in step (i)
Select Part II fresh plant tissue;With Part II described in control agent product treatment in step (ii);In heating stepses
(iii) treated Part II is also handled in;
And further, wherein then step (iii), methods described includes assessing treated Part I at least
The step of one attribute (iv), wherein the evaluated attribute be treated Part I relative to fresh plant group
Knit and/or characteristic relative to treated Part II change;
The duration of wherein described heating stepses (iii) is 10s to 1 hours;
Wherein described plant tissue includes petal, leaf or combinations thereof.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
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CNPCT/CN2013/079730 | 2013-07-19 | ||
CN2013079730 | 2013-07-19 | ||
EP13183501.9 | 2013-09-09 | ||
EP13183501 | 2013-09-09 | ||
CN201480039428.5A CN105378473A (en) | 2013-07-19 | 2014-06-27 | Method for evaluating efficacy of personal care product |
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CN201480039428.5A Division CN105378473A (en) | 2013-07-19 | 2014-06-27 | Method for evaluating efficacy of personal care product |
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CN107271606A true CN107271606A (en) | 2017-10-20 |
CN107271606B CN107271606B (en) | 2020-07-03 |
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CN201480039428.5A Pending CN105378473A (en) | 2013-07-19 | 2014-06-27 | Method for evaluating efficacy of personal care product |
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- 2014-06-27 CN CN201710303324.6A patent/CN107271606B/en active Active
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CN105378473A (en) | 2016-03-02 |
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