CN107267767A - A kind of vulcanization for being used to purify ore body - Google Patents
A kind of vulcanization for being used to purify ore body Download PDFInfo
- Publication number
- CN107267767A CN107267767A CN201710593458.6A CN201710593458A CN107267767A CN 107267767 A CN107267767 A CN 107267767A CN 201710593458 A CN201710593458 A CN 201710593458A CN 107267767 A CN107267767 A CN 107267767A
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- Prior art keywords
- vacuum
- distillation
- condensation chamber
- vacuum distillation
- room
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Acoustics & Sound (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention discloses a kind of vulcanization for being used to purify ore body, including vacuum gland, condensation chamber, room and bottom plate is evaporated in vacuo, the one end on the bottom plate top is provided with vacuum distillation furnace, the bottom of the vacuum distillation furnace is provided with vacuum distillation room, and condensation chamber is installed on vacuum distillation room, the side of the condensation chamber is uniformly provided with observation window, the inside of the vacuum distillation furnace is vertically provided with distillation cascade, and distillation cascade is sequentially passed through in condensation chamber and vacuum distillation room, the top of the distillation cascade is provided with vacuum gland, the other end on the bottom plate top is provided with mechanical pump, the both sides of distillation cascade inside the condensation chamber are mounted on carborundum tube, the top of the graphite crucible is connected by graphite column plate with condenser pipe.The present invention is purified by being provided with vacuum distillation room, condensation chamber and distillation cascade using vacuum distillation mode to foreign metal, improves metal purity, and the use demand for alloing it to meet people improves refining effect.
Description
Technical field
The present invention relates to industrial refining hihg purity metal equipment technical field, specially a kind of vulcanizer for being used to purify ore body
Tool.
Background technology
With the development of society, the fields such as many are both needed to use the basis of the most key part of metal of various high-purities now
Raw material, and the metal purity that traditional smelting technique can reach is general in 4N or so, is followed successively by the element that raw material is made, its property
It can far be not by far up to the mark, therefore be badly in need of a kind of device for refining hihg purity metal, to improve the purity of required metal, therefore
A kind of device of refining hihg purity metal arises at the historic moment, and the such device species on market today is varied, can meet substantially
The use demand of people, but still there are many problems, due to the such device that the foreign metal species in metal is various, traditional
Can not effectively it be handled so that the foreign metal contained in metal can not be effectively totally separated so that miscellaneous in metal
Matter refining effect is not good, it is impossible to meet the use demand of people.
The content of the invention
It is an object of the invention to provide a kind of vulcanization for being used to purify ore body, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical scheme：A kind of vulcanization for being used to purify ore body, including
Vacuum gland, condensation chamber, vacuum distillation room and bottom plate, the one end on the bottom plate top is provided with vacuum distillation furnace, the vacuum
The bottom of retort is provided with vacuum distillation room, and vacuum distillation room and is provided with condensation chamber, and the side of the condensation chamber is uniform
Provided with observation window, the inside of the vacuum distillation furnace is vertically provided with distillation cascade, and distillation cascade is sequentially passed through in condensation chamber and true
Empty distillery, the top of the distillation cascade is provided with vacuum gland, and the other end on the bottom plate top is provided with mechanical pump, and machine
Control cabinet is installed on bottom plate between tool pump and vacuum distillation room, the one end on the control cabinet top is provided with diffusion pump, and
The other end on control cabinet top is provided with vacuum tank, and the top of the vacuum tank is by connecting tube and diffusion pump close to vacuum tank
Side connect, the vacuum tank away from diffusion pump side by the second airway tube and top connect, the top of the vacuum gland
End is connected by the top of the first airway tube and diffusion pump, and the both sides of the distillation cascade of the vacuum distillation chamber interior are mounted on carbon
SiClx pipe, and the inside of distillation cascade of vacuum distillation chamber interior is provided with the distillation cascade inside graphite crucible, the condensation chamber
Uniform be fixed between condenser pipe, and condenser pipe is connected by graphite column plate, the both sides of the distillation cascade inside the condensation chamber
Carborundum tube is mounted on, the top of the graphite crucible is connected by graphite column plate with condenser pipe.
It is preferred that, heat-insulating shield is provided between the vacuum distillation room and condensation chamber.
It is preferred that, heat-insulated packed layer is filled between the vacuum distillation room and condensation chamber and distillation cascade.
It is preferred that, resistive heater is provided with the carborundum tube, and resistive heater is fixed on carborundum in the shape of a spiral
In pipe.
It is preferred that, the longitudinal section of the graphite crucible is trapezoidal.
Compared with prior art, the beneficial effects of the invention are as follows：This is used for the vulcanization for purifying ore body by being provided with
Room, condensation chamber and distillation cascade is evaporated in vacuo, has graphite crucible by the way that indoor location is evaporated in vacuo, and placed in graphite crucible
Foreign metal, carries out heating by the resistance wire in carborundum tube and make it that different types of metal impurities are because itself boils in metal
The difference of point so that metal impurities are vaporized, the steam after vaporizing afterwards carries out effective steam classification by graphite column plate, and leads to
Cross the indoor carborundum tube of condensation and carry out temperature adjustment so that foreign metal recovers solid-state, and falls on graphite column plate, so that real
Showed the classification for metal impurities, improve metal purity, the use demand for alloing it to meet people, and refining effect compared with
It is good.
Brief description of the drawings
Fig. 1 is structural representation of the invention；
Fig. 2 is vacuum distillation furnace diagrammatic cross-section of the invention；
Fig. 3 is column plate schematic diagram of the invention；
In figure：1- vacuum glands；2- vacuum distillation furnaces；3- condensation chambers；4- observation windows；Room is evaporated in vacuo in 5-；6- bottom plates；7- first
Airway tube；8- diffusion pumps；9- vacuum tanks；The airway tubes of 10- second；11- control cabinets；12- mechanical pumps；13- graphite column plates；14- is cold
Solidifying pipe；15- distillation cascades；The heat-insulated packed layers of 16-；17- graphite crucibles；18- carborundum tubes.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
Refer to Fig. 1-3, a kind of embodiment that the present invention is provided：A kind of vulcanization for being used to purify ore body, including it is true
Pneumatics lid 1, condensation chamber 3, vacuum distillation room 5 and bottom plate 6, the one end on the top of bottom plate 6 are provided with vacuum distillation furnace 2, are evaporated in vacuo
The bottom of stove 2, which is provided with vacuum distillation room 5, and vacuum distillation room 5, is provided with condensation chamber 3, vacuum distillation room 5 and condensation chamber 3
Between be provided with heat-insulating shield, heat-insulating shield prevents from producing mixed heat between the two, influences the purification of metal, vacuum distillation room 5 and condensation chamber 3
Heat-insulated packed layer 16 is filled between distillation cascade 15, heat-insulated packed layer 16 prevents that the temperature of vacuum distillation furnace 2 is too high so that
External environment produces thermal pollution, and the side of condensation chamber 3 is uniformly provided with observation window 4, and the inside of vacuum distillation furnace 2 is vertically provided with steaming
Pipe 15 is evaporated, and distillation cascade 15 is sequentially passed through in condensation chamber 3 and vacuum distillation room 5, the top of distillation cascade 15 is provided with vacuum gland
1, the other end on the top of bottom plate 6, which is provided with the bottom plate 6 between mechanical pump 12, and mechanical pump 12 and vacuum distillation room 5, to be provided with
Control cabinet 11, the one end on the top of control cabinet 11 is provided with diffusion pump 8, and the other end on the top of control cabinet 11 is provided with vacuum tank 9,
The top of vacuum tank 9 is connected by connecting tube with diffusion pump 8 close to the side of vacuum tank 9, and vacuum tank 9 is away from the side of diffusion pump 8
It is connected by the second airway tube 10 with 12 top, the top of vacuum gland 1 passes through the top of the first airway tube 7 and diffusion pump 8
The both sides of distillation cascade 15 inside connection, vacuum distillation room 5 are mounted on the steaming inside carborundum tube 18, and vacuum distillation room 5
The inside for evaporating pipe 15 is provided with graphite crucible 17, and the longitudinal section of graphite crucible 17 is trapezoidal, so that graphite crucible 17 is easy to
It is fixed in distillation cascade 15, and easily stored foreign metal, uniformly condenser pipe is fixed with the distillation cascade 15 inside condensation chamber 3
Connected between 14, and condenser pipe 14 by graphite column plate 13, the both sides of the distillation cascade 15 inside condensation chamber 3 are mounted on carbonization
Resistive heater is provided with silicone tube 18, carborundum tube 18, and resistive heater is fixed in carborundum tube 18 in the shape of a spiral, so
So that it is more efficient by Resistant heating, and energy-conservation, while helical form causes Resistant heating evenly, graphite crucible 17
Top is connected by graphite column plate 13 with condenser pipe 14.
Specifically used mode：In use, foreign metal is placed in graphite crucible 17, and graphite crucible 17 is placed in distillation
The bottom of pipe 15, controls the carborundum tube 18 in vacuum distillation room 5 to be heated so that metal impurities by control cabinet 11
Melt to being in gaseous state, steam classified metallic vapour by the effect of graphite column plate 13, it is logical afterwards into condenser pipe 14
The regulation temperature of carborundum tube 18 crossed in the control condensation chamber 3 of control cabinet 11 so that metal gaseous state recovers to be in solid-state, and falls in graphite
On column plate 18, complete the classification for different metal impurity and handle, substantially increase the refining effect of metal.With prior art phase
Than, the beneficial effects of the invention are as follows：This be used to purifying the vulcanization of ore body by be provided with vacuum distillation room, condensation chamber and
Distillation cascade, has graphite crucible by the way that indoor location is evaporated in vacuo, and places foreign metal in graphite crucible, passes through carborundum tube
Interior resistance wire carries out heating and make it that different types of metal impurities are due to the difference of itself boiling point in metal so that metal impurities
Vaporization, the steam after vaporizing afterwards carries out effective steam classification by graphite column plate, and passes through the carborundum tube in condensation chamber
Temperature adjustment is carried out so that foreign metal recovers solid-state, and falls on graphite column plate, it is achieved thereby that for point of metal impurities
Class, improves metal purity, the use demand for alloing it to meet people, and refining effect is preferable.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as to the claim involved by limitation.
Claims (6)
1. a kind of vulcanization for being used to purify ore body, including vacuum gland（1）, condensation chamber（3）, vacuum distillation room（5）And bottom
Plate（6）, it is characterised in that：The bottom plate（6）The one end on top is provided with vacuum distillation furnace（2）, the vacuum distillation furnace（2）'s
Bottom is provided with vacuum distillation room（5）, and vacuum distillation room（5）On condensation chamber is installed（3）, the condensation chamber（3）Side
It is uniformly provided with observation window（4）, the vacuum distillation furnace（2）Inside distillation cascade is vertically installed（15）, and distillation cascade（15）According to
It is secondary through condensation chamber（3）With vacuum distillation room（5）, the distillation cascade（15）Top vacuum gland is installed（1）, the bottom
Plate（6）The other end on top is provided with mechanical pump（12）, and mechanical pump（12）With vacuum distillation room（5）Between bottom plate（6）On
Control cabinet is installed（11）, the control cabinet（11）The one end on top is provided with diffusion pump（8）, and control cabinet（11）Top it is another
One end is provided with vacuum tank（9）, the vacuum tank（9）Top pass through connecting tube and diffusion pump（8）Close to vacuum tank（9）One
Side is connected, the vacuum tank（9）Away from diffusion pump（8）Side passes through the second airway tube（10）With（12）Top connection, it is described
Vacuum gland（1）Top pass through the first airway tube（7）With diffusion pump（8）Top connection, the vacuum distillation room（5）It is internal
Distillation cascade（15）Both sides be mounted on carborundum tube（18）, and vacuum distillation room（5）Internal distillation cascade（15）Inside
Graphite crucible is installed（17）, the condensation chamber（3）Internal distillation cascade（15）It is interior to be uniformly fixed with condenser pipe（14）, and condensation
Pipe（14）Between pass through graphite column plate（13）Connection, the condensation chamber（3）Internal distillation cascade（15）Both sides be mounted on
Carborundum tube（18）, the graphite crucible（17）Top pass through graphite column plate（13）With condenser pipe（14）Connection.
2. a kind of vulcanization for being used to purify ore body according to claim 1, it is characterised in that：The vacuum distillation room
（5）With condensation chamber（3）Between be provided with heat-insulating shield.
3. a kind of vulcanization for being used to purify ore body according to claim 1, it is characterised in that：The vacuum distillation room
（5）And condensation chamber（3）With distillation cascade（15）Between be filled with heat-insulated packed layer（16）.
4. a kind of vulcanization for being used to purify ore body according to claim 1, it is characterised in that：The carborundum tube
（18）It is interior to be provided with resistive heater, and resistive heater is fixed on carborundum tube in the shape of a spiral（18）It is interior.
5. a kind of vulcanization for being used to purify ore body according to claim 1, it is characterised in that：The graphite crucible
（17）Longitudinal section it is trapezoidal.
6. a kind of vulcanization for being used to purify ore body according to claim 1, it is characterised in that：The vacuum gland
（1）Top pass through the first airway tube（7）With diffusion pump（8）Top connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710593458.6A CN107267767A (en) | 2017-07-20 | 2017-07-20 | A kind of vulcanization for being used to purify ore body |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710593458.6A CN107267767A (en) | 2017-07-20 | 2017-07-20 | A kind of vulcanization for being used to purify ore body |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107267767A true CN107267767A (en) | 2017-10-20 |
Family
ID=60079331
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710593458.6A Pending CN107267767A (en) | 2017-07-20 | 2017-07-20 | A kind of vulcanization for being used to purify ore body |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107267767A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2690414Y (en) * | 2003-11-27 | 2005-04-06 | 四川鑫炬矿业资源开发股份有限公司 | Vacuum distilling device for refining high purity metal |
| CN201109792Y (en) * | 2007-07-17 | 2008-09-03 | 董晋 | Vacuum multilevel distillation parting furnace |
| CN105506309A (en) * | 2015-12-04 | 2016-04-20 | 兰州空间技术物理研究所 | Three-stage distillation device for purifying alkali metal and method of purifying alkali metal |
| CN205710865U (en) * | 2016-05-16 | 2016-11-23 | 青海大学 | The tower multi-stage evaporator of the recoverable band of vinasse and condenser vacuum retort |
| CN206521508U (en) * | 2017-01-06 | 2017-09-26 | 上饶市致远环保科技有限公司 | A kind of vacuum distillation plant of refining hihg purity metal |
-
2017
- 2017-07-20 CN CN201710593458.6A patent/CN107267767A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2690414Y (en) * | 2003-11-27 | 2005-04-06 | 四川鑫炬矿业资源开发股份有限公司 | Vacuum distilling device for refining high purity metal |
| CN201109792Y (en) * | 2007-07-17 | 2008-09-03 | 董晋 | Vacuum multilevel distillation parting furnace |
| CN105506309A (en) * | 2015-12-04 | 2016-04-20 | 兰州空间技术物理研究所 | Three-stage distillation device for purifying alkali metal and method of purifying alkali metal |
| CN205710865U (en) * | 2016-05-16 | 2016-11-23 | 青海大学 | The tower multi-stage evaporator of the recoverable band of vinasse and condenser vacuum retort |
| CN206521508U (en) * | 2017-01-06 | 2017-09-26 | 上饶市致远环保科技有限公司 | A kind of vacuum distillation plant of refining hihg purity metal |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20171020 |
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| WD01 | Invention patent application deemed withdrawn after publication |