CN107267287A - The method that hyssop essential oil is extracted from hyssop - Google Patents

The method that hyssop essential oil is extracted from hyssop Download PDF

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Publication number
CN107267287A
CN107267287A CN201710210230.4A CN201710210230A CN107267287A CN 107267287 A CN107267287 A CN 107267287A CN 201710210230 A CN201710210230 A CN 201710210230A CN 107267287 A CN107267287 A CN 107267287A
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Prior art keywords
hyssop
essential oil
broken
temperature
hay cutter
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CN201710210230.4A
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Chinese (zh)
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李先强
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Individual
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/21Amaranthaceae (Amaranth family), e.g. pigweed, rockwort or globe amaranth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/15Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Medical Informatics (AREA)
  • Microbiology (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses the method that hyssop essential oil is extracted from hyssop, pharmaceutical technology field solves the problems, such as the extraction of hyssop essential oil, it is characterized in that being carried out by following step:First, raw material:Fresh root of bidentate achyranthes grass blade, leaf, flower;2nd, instrument:Cut up with a hay cutter broken machine, destilling tower, cooling tower, Packaging Bottle;3rd, fresh hyssop strain body, including stem, leaf, flower are gathered in, cleans up, dries moisture;4th, with bruisher, by Verbena officinalis hand hay cutter, to be broken into diameter≤2cm small broken section;5th, put Verbena officinalis of the hand hay cutter after broken into destilling tower and carry out steam distillation, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, boiler bottom will keep moisture, raw material to touch pot, be charred in order to avoid producing;Six, the mixing gas distilled out is delivered directly to cooling tower, and 0 DEG C of -5 DEG C≤chilling temperature < separates out ice cube, obtains pure hyssop essential oil;7th, by filling bottle closure under hyssop low temperature, 0 DEG C of -5 DEG C≤filling bottle temperature <.

Description

The method that hyssop essential oil is extracted from hyssop
Technical field
The present invention relates to the method that Verbena officinalis essential oil is extracted from hyssop, belong to pharmaceutical technology field.
Background technology
Hyssop essential oil is from hyssop plant(Hyssopus officinalis)Middle extraction, belong to Amaranthaceae, also known as For hyssop.This fairly expensive essential oil can effectively auxiliary treatment women deficiency disorder and lunar periodicity oedema.Helping In terms for the treatment of respiratory system, mucus can be effectively removed, alleviates bronchial spasm.It can be utilized to treat bronchus Inflammation, asthma, influenza and flu, it helps the bruise in wound healing and dissipation skin.
Hyssop kenel:Perennial herb, stem is straight and hard, and high about 30 centimeters~50 centimeters branches of plant are opened below stem Begin to separate upright or expand, leaf stockless, line style or drape over one's shoulders needle-like full edge, two ends are carefully blunt nosed, slightly meat, and two sides majority oil droplets, wheel dissipates Inflorescence difference piece side axillary, branch and leaf crinosity, there is noon taste.6~15 flowers are opened, corolla is usually purple, also have pink or white Color, lip, base portion tubbiness, and long 1.3 centimetres, sepal triangle strip wool.
Hyssop is distributed this shrub and is sporadically distributed in Mediterranean Region, and height about 60cm has very strong suction to honeybee Gravitation.Hyssop was once name doctor's Hippcrates of Greece(About B.C. 460~about B.C. 370, Hippocrates, doctor The father of medicine)Used name, is to develop to come from Hebrew " ezob ", means " sacred plant ".It is in ancient book (《Old Testament》)In be often mentioned, at that time, people make the symbol of soul purification of it, however, this saying is signified Plant is it could also be possible that origanum.
Stem lignifying, the crinosity of hyssop, blade is small, green, long hairy, and flower purple blue is the plant of famous in ancient. Its eustipes part is as root of bidentate achyranthes lid.It is also mentioned in the Holy Bible.It has effects that purification, can with repellent pestilence, leprosy, Treat the disease in thoracic cavity.It also be used to purify religious site, is taken as one kind to intersperse plant in Middle Ages, carrys out repellent louse. In 10th century, it as the making raw material of ligueur, is incorporated into Europe by Benedictine people.
Hyssop essential oil effect:1. hyssop essential oil can give people a kind of sensation of warning, help to alleviate anxious and fatigue. Therefore, in the rehabilitation stage, it can be used as invigorant.2. when treating flu caused by respiratory disease and virus, it It is also effective, such as treatment flu, cough, throat pain, influenza, bronchitis, asthma, catarrh and tonsillitis.3. it has Help treatment gastric colic, ventosity and indigestion, regulation circulation.4. in intermenstrual period, the problem of oedema is individual regular, Hyssop essential oil plays the role of balance.Generally, this essential oil contributes to eumenorrhea, for amenorrhea and leukorrhea Exception has mitigation.5. it can also be reduced blood pressure by reducing heart rate and expansion peripheral arterial.6. it has had for bruise Treat characteristic.
Hyssop essential oil does not have excitant, without sensitiveness, but to use appropriateness.Pregnant woman and epilepsy sufferers should avoid making With.Hyssop essential oil is the powerful oil of kind of effect, can alleviate respiratory disease, and regulation digestive system is not normal, treats uropoiesis System infections, and skin problem, including bruise, eczema, infection and dermatitis.Hyssop essential oil makees compound massage oil or is diluted in Used in bathtub, anxiety, neural fatigue, respiratory disease, viral infection, problem of menstruation, stomach angina, stomach can be alleviated Flatulence, indigestion and promotion skin rehabilitation.
The content of the invention
In order to extract the hyssop essential oil of one stream to meet demand of the field of medicaments to hyssop essential oil, my invention A kind of method that hyssop essential oil is extracted from hyssop, this method extracts simple, and processing is simple, and small investment brings notable results, and carries Take rate high, the hyssop essential oil of extraction is the extracting method that small-sized manufacturer can be carried out.
The method solution problem that hyssop essential oil is extracted from hyssop is adopted the technical scheme that by following step Carry out:First, raw material used:Fresh root of bidentate achyranthes grass blade, leaf, flower;2nd, instrument used:Broken machine, destilling tower, cooling tower are cut up with a hay cutter, is wrapped Bottling;3rd, fresh hyssop strain body, including stem, leaf, flower are gathered in, cleans up, dries moisture;4th, with bruisher by horsewhip It is small broken section that grass hand hay cutter is broken into diameter≤2cm;5th, put Verbena officinalis of the hand hay cutter after broken into destilling tower and carry out steam distillation, 120 DEG C >=steam Temperature >=100 DEG C are evaporated, boiler bottom will keep moisture, raw material to touch pot, be charred in order to avoid producing;Six, the mixed steam distilled out Body is delivered directly to cooling tower, and 0 DEG C of -5 DEG C≤chilling temperature < separates out ice cube, obtains pure hyssop essential oil;7th, by hyssop Filling bottle closure under low temperature, 0 DEG C of -5 DEG C≤filling bottle temperature <.
The beneficial effect of hyssop essential oil is extracted from hyssop is:Extracting hyssop essential oil from hyssop can be by whole strain Hyssop is as raw material is made, and only simply cutting up with a hay cutter broken processing just can throw into destilling tower progress heating distillation production;From hyssop The middle method for extracting hyssop essential oil make use of the characteristics of derived essential oil contained by hyssop is easy to volatilization, and high temperature hyssop is thin Cell wall, discharges hyssop derived essential oil, is evaporated together with water vapour and is transported to cooling tower;Hyssop is extracted from hyssop The method of essential oil make use of the difference of hyssop essential oil and water cooling adiabatic condensation temperature, by the moisture in mixed vapour in cooling tower All separate out, obtain the hyssop essential oil of high-purity.
Embodiment
Embodiment.The method solution problem that hyssop essential oil is extracted from hyssop is adopted the technical scheme that by following The step of carry out:First, raw material used:Fresh root of bidentate achyranthes grass blade, leaf, flower;2nd, instrument used:Cut up with a hay cutter broken machine, it is destilling tower, cold But tower, Packaging Bottle;3rd, fresh hyssop strain body, including stem, leaf, flower are gathered in, cleans up, dries moisture;4th, with smashing to pieces It is small broken section that Verbena officinalis hand hay cutter is broken into diameter≤2cm by machine;5th, put Verbena officinalis of the hand hay cutter after broken into destilling tower and carry out steam distillation, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, boiler bottom will keep moisture, raw material to touch pot, be charred in order to avoid producing;Six, distill out Mixing gas be delivered directly to cooling tower, 0 DEG C of -5 DEG C≤chilling temperature < separates out ice cube, obtains pure hyssop essential oil;7th, By filling bottle closure under hyssop low temperature, 0 DEG C of -5 DEG C≤filling bottle temperature <.

Claims (1)

1. the method for hyssop essential oil is extracted from hyssop, it is characterized in that being carried out by following step:First, raw material used: Fresh root of bidentate achyranthes grass blade, leaf, flower;2nd, instrument used:Cut up with a hay cutter broken machine, destilling tower, cooling tower, Packaging Bottle;3rd, gather in fresh Hyssop strain body, including stem, leaf, flower, clean up, dry moisture;4th, Verbena officinalis hand hay cutter is broken into diameter≤2cm with bruisher It is small broken section;5th, put Verbena officinalis of the hand hay cutter after broken into destilling tower and carry out steam distillation, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, steam Evaporating the bottom of a pan will keep moisture, raw material to touch pot, be charred in order to avoid producing;Six, the mixing gas distilled out is delivered directly to cooling Tower, 0 DEG C of -5 DEG C≤chilling temperature < separates out ice cube, obtains pure hyssop essential oil;7th, filling bottle under hyssop low temperature is sealed Lid, 0 DEG C of -5 DEG C≤filling bottle temperature <.
CN201710210230.4A 2017-03-31 2017-03-31 The method that hyssop essential oil is extracted from hyssop Withdrawn CN107267287A (en)

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CN201710210230.4A CN107267287A (en) 2017-03-31 2017-03-31 The method that hyssop essential oil is extracted from hyssop

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106336951A (en) * 2016-10-27 2017-01-18 张文艳 Method for extracting verbena essence oil from verbena

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106336951A (en) * 2016-10-27 2017-01-18 张文艳 Method for extracting verbena essence oil from verbena

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MATHEW ATTOKARAN等: "《天然食用香料与色素》", 30 September 2014 *

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Application publication date: 20171020