CN107261718A - A kind of organic solid waste Non-oxygen pyrolytic solid liquid gas three-phase separation device and method - Google Patents

A kind of organic solid waste Non-oxygen pyrolytic solid liquid gas three-phase separation device and method Download PDF

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Publication number
CN107261718A
CN107261718A CN201710560109.4A CN201710560109A CN107261718A CN 107261718 A CN107261718 A CN 107261718A CN 201710560109 A CN201710560109 A CN 201710560109A CN 107261718 A CN107261718 A CN 107261718A
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China
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separator
liquid
oil
solid
gas
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CN201710560109.4A
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Inventor
洪觉慧
戚新军
周光林
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Yancheng Greentown Environmental Protection Technology Co Ltd
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Yancheng Greentown Environmental Protection Technology Co Ltd
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Priority to CN201710560109.4A priority Critical patent/CN107261718A/en
Publication of CN107261718A publication Critical patent/CN107261718A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D50/00Combinations of methods or devices for separating particles from gases or vapours
    • B01D50/40Combinations of devices covered by groups B01D45/00 and B01D47/00
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23GCREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/44Details; Accessories
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23GCREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G7/00Incinerators or other apparatus for consuming industrial waste, e.g. chemicals

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Industrial Gases (AREA)
  • Processing Of Solid Wastes (AREA)
  • Gasification And Melting Of Waste (AREA)

Abstract

The invention discloses a kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase piece-rate system, it is characterised in that:Including gravitational settler, multicyclone dust collector, sprayed tank, multi-level water cooler, three phase separator, oil water separator, liquid packing, multistage solid-liquid separator, dedusting lime-ash return channel, water cooling lime-ash return channel, spray cooler, accumulator tank;With reference to the device, the invention also discloses a kind of solid-liquid-gas three phase separation method.The technical scheme that the present invention is provided has compared with much progress compared with for prior art, is mainly reflected in:Use cost is low, is easy to popularization, good dedusting effect, saves artificial.

Description

A kind of organic solid waste Non-oxygen pyrolytic solid liquid gas three-phase separation device and method
Technical field
The present invention relates to a kind of three-phase separating device and method, more particularly to a kind of solid-liquid-gas of organic solid waste pyrolysis art Three-phase separating device and method.
Background technology
The harmful solid waste of China year yield at 15,000,000 tons or so, harmful solid waste can penetrate into soil in soil after weathering Earth, destroys the corrosion capacity of decomposition of soil;The solid waste of long-term outdoor placement can be volatilized substantial amounts of waste gas and dust, and air is caused Severe contamination etc., solid waste pollution problem has caused the attention of society.
The processing to chemical solid waste mainly uses the mode such as landfill, biological treatment after burning at present.Burning process lack On the one hand point is that cost is high, and flying dust (harmful components containing dioxin), the stench on the other hand produced therewith also brings along secondary dirt Dye.China is in the stage of urbanization rate fast lifting, and urban land has been scarce resource, and filling needs large area Secondary pollution problem after soil, landfill is also very serious.
Pyrolytic technique is a kind of dangerous waste treatment technology of novel environment friendly, using widely, but produced after preliminary pyrolysis The separator of solid-liquid-gas three phase mixture is not solved well with method.
The content of the invention
To solve the solid-liquid-gas three phase mixture processing unit and method that are produced after existing current organic solid waste Non-oxygen pyrolytic Deficiency, the invention provides it is a kind of it is simple in construction, be easy to popularization, low use cost, good dedusting effect, save artificial organic Solid waste is pyrolyzed solid liquid gas three-phase separation device, and there is provided a set of corresponding recovery separation method.
The present invention concrete technical scheme be:
A kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase piece-rate system, it is characterised in that:Including gravity settler, multistage Cyclone dust collectors, sprayed tank, multi-level water cooler, three phase separator, oil water separator, liquid packing, multistage solid-liquid separator, dedusting Lime-ash return channel, water cooling lime-ash return channel, spray cooler, accumulator tank;Multistage cyclone is connected to above the gravity settler Deduster, lower section are connected to dedusting lime-ash return channel;The multicyclone dust collector top is connected to sprayed tank, bottom and is connected to Multistage solid-liquid separator;The multistage solid-liquid separator bottom is connected to dedusting lime-ash return channel;The sprayed tank top connection Multi-level water cooler, multistage solid-liquid separator, bottom, which are respectively connecting to, to spray cooler, middle part is connected to the backflow of dedusting lime-ash Device;The multi-level water cooler is connected to three phase separator;The three phase separator top is connected to liquid packing, bottom and connected respectively To oil water separator, spray cooler, accumulator tank;The oil water separator is connected to pans;The accumulator tank is connected to spray Drench cooler;The pans, accumulator tank share a pipeline discharge.
Correspondingly, a kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase separation method, it is characterised in that comprise the following steps:
S1. organic solid waste is after pyrolysis, and water vapour, oil gas and the ash content of generation pass through gravitational settler, pass through nature Gravity and flow slowing down effect is lower removes a part of bulky grain ash content, falls on bottom and returns to pyrolysis by dedusting lime-ash return channel and set It is pyrolyzed again in standby;
S2. the solid-liquid gas mixture after gravitational settling tower enters multicyclone dust collector, respectively the different sizes of dedusting Ash content, the profit of the ash content of generation and cooling enters multistage solid-liquid separator, is automatically separated, periodically discharge lime-ash enters dedusting Dregs of fat return channel, is back in gravitational settler and is pyrolyzed again;
S3. oil gas enters cooling oil sprayed tank after multistage dedusting, passes through spraying cooling using the oil produced in production Device carries out dedusting cooling to its oil gas, and the liquid of generation is mixed by multistage solid-liquid separator and the liquid produced by multi-level water cooler Conjunction enters three phase separator;
S4. last oil gas is condensed into multi-level water cooler, and the condensed fluid and gas of generation enter three phase separator, is separated Fuel-displaced, water, fuel gas, the oil of generation are partly into spray cooler circulated sprinkling, and unnecessary output enters accumulator tank, three-phase The water that separator is produced enters oil water separator, subsequently into production water storage tank, and the oil that oil water separator is produced enters pans, Periodically it is discharged into accumulator tank;
S5. three phase separator comes out the normal temperature oil gas that can not be cooled down and returned after Safety water seal into organic solid waste pyrolysis gas Receipts utilize system.
The technical scheme that the present invention is provided has compared with much progress compared with for prior art, is mainly reflected in:
1. because pyrolysis apparatus is continuous feed dynamic pyrolysis process, causing in pyrolysis gas that ash content ratio is higher, pass through gravity The method that settler, three kinds of dedusting methods of multilevel cyclone dust collection and spray are combined, reaches good dust removing effects;
2. by the solid-liquid separator that each deduster is supporting, lime-ash is automatically separated, by two sets of lime-ash return channels certainly Dynamic be discharged in pyrolysis apparatus is pyrolyzed again, and thoroughly solving lime-ash in other techniques needs the shortcoming of manual cleaning.
Brief description of the drawings
Fig. 1 is the structural representation that a kind of organic solid waste that the present invention is provided is pyrolyzed solid liquid gas three-phase separation device
Identified in figure:
1. gravitational settler;2. multicyclone dust collector;3. sprayed tank;4. multi-level water cooler;5. three phase separator;6. oil Separator;7. liquid packing;8. multistage solid-liquid separator;9. dedusting lime-ash return channel;10. water cooling lime-ash return channel;11. spray Cooler;12. accumulator tank;13. pans.
Embodiment
A kind of disclosed organic solid waste pyrolysis solid-liquid-gas three phase separation is filled below in conjunction with drawings and Examples Put and method is further explained.
A kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase piece-rate system as shown in Figure 1, including it is gravity settler 1, many Level cyclone dust collectors 2, sprayed tank 3, multi-level water cooler 4, three phase separator 5, oil water separator 6, liquid packing 7, multistage solid-liquid point From device 8, dedusting lime-ash return channel 9, water cooling lime-ash return channel 10, spray cooler 11, accumulator tank 12;The gravity settler 1 Top is connected to multicyclone dust collector 2, lower section and is connected to dedusting lime-ash return channel 9;The top of multicyclone dust collector 2 connects It is connected to sprayed tank 3, bottom and is connected to multistage solid-liquid separator 8;The bottom of multistage solid-liquid separator 8 is connected to dedusting lime-ash and returned Flow device 9;The top of sprayed tank 3 is connected to spray cooler 11, middle part and is respectively connecting to multi-level water cooler 4, multistage solid-liquid point Dedusting lime-ash return channel 9 is connected to from device 8, bottom;The multi-level water cooler 4 is connected to three phase separator 5;The three phase separation The top of device 5 is connected to liquid packing 7, bottom and is respectively connecting to oil water separator 6, spray cooler 11, accumulator tank 12;The profit Separator 6 is connected to pans 13;The accumulator tank 12 is connected to spray cooler 11;The pans 13, accumulator tank 12 are total to Discharged with a pipeline.
Correspondingly, a kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase separation method, comprises the following steps:
S1. organic solid waste is after pyrolysis, and water vapour, oil gas and the ash content of generation pass through gravitational settler 1, pass through nature Gravity and the lower a part of bulky grain ash content of removal of flow slowing down effect, fall on bottom and return to pyrolysis by dedusting lime-ash return channel 9 It is pyrolyzed again in equipment;
S2. the solid-liquid gas mixture after gravitational settling tower 1 enters multicyclone dust collector 2, respectively the different chis of dedusting Very little ash content, the ash content of generation and the profit of cooling enter multistage solid-liquid separator 8, are automatically separated, and periodically discharge lime-ash enters Dedusting dregs of fat return channel 9, is back in gravitational settler and is pyrolyzed again;
S3. oil gas enters cooling oil sprayed tank 3 after multistage dedusting, passes through spraying cooling using the oil produced in production Device 11 carries out dedusting cooling to its oil gas, and the liquid of generation is by multistage solid-liquid separator 8 and the liquid produced by multi-level water cooler 4 Body is mixed into three phase separator 5;
S4. last oil gas is condensed into multi-level water cooler 4, and the condensed fluid and gas of generation enter three phase separator 5, point Oil, water, fuel gas are separated out, the oil of generation is partly into the circulated sprinkling of spray cooler 11, and unnecessary output enters accumulator tank 12, the water that three phase separator is produced enters oil water separator 6, and subsequently into production water storage tank, the oil that oil water separator is produced enters Enter pans 13, be periodically discharged into accumulator tank 12;
S5. three phase separator 5 comes out the normal temperature oil gas that can not be cooled down and returned after liquid packing 7 into organic solid waste pyrolysis gas Receipts utilize system.
The technical scheme that the present invention is provided has compared with much progress compared with for prior art, is mainly reflected in:
1. because pyrolysis apparatus is continuous feed dynamic pyrolysis process, causing in pyrolysis gas that ash content ratio is higher, pass through gravity The method that settler, three kinds of dedusting methods of multilevel cyclone dust collection and spray are combined, reaches good dust removing effects;
2. by the solid-liquid separator that each deduster is supporting, lime-ash is automatically separated, by two sets of lime-ash return channels certainly Dynamic be discharged in pyrolysis apparatus is pyrolyzed again, and thoroughly solving lime-ash in other techniques needs the shortcoming of manual cleaning.
Above example is the explanation of the embodiment to the present invention, rather than limitation of the present invention, relevant technology The technical staff in field without departing from the spirit and scope of the present invention, can also make various conversion and change and obtain To corresponding equivalent technical scheme, therefore all equivalent technical schemes should be included into the patent protection model of the present invention Enclose.

Claims (2)

1. a kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase piece-rate system, it is characterised in that:Including gravitational settler, multistage rotation Wind deduster, sprayed tank, multi-level water cooler, three phase separator, oil water separator, liquid packing, multistage solid-liquid separator, dedusting ash Slag return channel, water cooling lime-ash return channel, spray cooler, accumulator tank;Multistage cyclone is connected to above the gravity settler to remove Dirt device, lower section are connected to dedusting lime-ash return channel;The multicyclone dust collector top be connected to sprayed tank, bottom be connected to it is many Level solid-liquid separator;The multistage solid-liquid separator bottom is connected to dedusting lime-ash return channel;The sprayed tank top is connected to Spray cooler, middle part are respectively connecting to multi-level water cooler, multistage solid-liquid separator, bottom and are connected to dedusting lime-ash return channel; The multi-level water cooler is connected to three phase separator;The three phase separator top is connected to liquid packing, bottom and is respectively connecting to Oil water separator, spray cooler, accumulator tank;The oil water separator is connected to pans;The accumulator tank is connected to spray Cooler;The pans, accumulator tank share a pipeline discharge.
2. a kind of organic solid waste Non-oxygen pyrolytic solid-liquid-gas three phase separation method, it is characterised in that comprise the following steps:
S1. organic solid waste is after pyrolysis, and water vapour, oil gas and the ash content of generation pass through gravitational settler, pass through natural gravity And flow slowing down effect is lower removes a part of bulky grain ash content, falls on bottom and return in pyrolysis plant and be pyrolyzed again;S2. through overweight Solid-liquid gas mixture after power sedimentation tower enters multicyclone dust collector, respectively the various sizes of ash content of dedusting, the ash content of generation And the profit of cooling enters multistage solid-liquid separator, is automatically separated, periodically discharge lime-ash enters dedusting dregs of fat return channel, is back to It is pyrolyzed again in gravitational settler;
S3. oil gas enters cooling oil sprayed tank after multistage dedusting, passes through spray cooler pair using the oil produced in production Its oil gas carries out dedusting cooling, and the liquid of generation is mixed into by multistage solid-liquid separator with the liquid produced by multi-level water cooler Enter three phase separator;
S4. last oil gas is condensed into multi-level water cooler, and the condensed fluid and gas of generation enter three phase separator, isolated Oil, water, fuel gas, the oil of generation are partly into spray cooler circulated sprinkling, and unnecessary output enters accumulator tank, three-phase separate The water produced from device enters oil water separator, subsequently into production water storage tank, and the oil that oil water separator is produced enters pans, fixed Phase is discharged into accumulator tank;
S5. three phase separator comes out the normal temperature oil gas that can not be cooled down and reclaims profit into organic solid waste pyrolysis gas after Safety water seal Use system.
CN201710560109.4A 2017-07-11 2017-07-11 A kind of organic solid waste Non-oxygen pyrolytic solid liquid gas three-phase separation device and method Pending CN107261718A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109289225A (en) * 2018-09-12 2019-02-01 中科钢研节能科技有限公司 A kind of device and method of condensing recovery pyrolysis gas and application

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CN103602349A (en) * 2013-11-27 2014-02-26 辽宁留德润滑油有限公司 Pyrolysis gas recovery device and method of distillation apparatus
CN105036507A (en) * 2015-08-07 2015-11-11 中国海洋石油总公司 Pyrolysis oil-gas-water synchronous condensing and oil-water separation recovery system and method
CN206109332U (en) * 2016-09-18 2017-04-19 湖南万容科技股份有限公司 Oil gas purification device
CN106701123A (en) * 2015-08-07 2017-05-24 泰州华瑞电子专用设备有限公司 Subsequent classified collection system for biomass pyrolysis and charring
CN106746419A (en) * 2017-03-07 2017-05-31 盘锦宁泰能源科技有限公司 A kind of oily sludge industrially scalable pyrolysis treatment systems and method

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101845331A (en) * 2010-06-10 2010-09-29 河南省高新技术实业总公司 Method for separating and condensing biomass cracking gases
CN103602349A (en) * 2013-11-27 2014-02-26 辽宁留德润滑油有限公司 Pyrolysis gas recovery device and method of distillation apparatus
CN105036507A (en) * 2015-08-07 2015-11-11 中国海洋石油总公司 Pyrolysis oil-gas-water synchronous condensing and oil-water separation recovery system and method
CN106701123A (en) * 2015-08-07 2017-05-24 泰州华瑞电子专用设备有限公司 Subsequent classified collection system for biomass pyrolysis and charring
CN206109332U (en) * 2016-09-18 2017-04-19 湖南万容科技股份有限公司 Oil gas purification device
CN106746419A (en) * 2017-03-07 2017-05-31 盘锦宁泰能源科技有限公司 A kind of oily sludge industrially scalable pyrolysis treatment systems and method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109289225A (en) * 2018-09-12 2019-02-01 中科钢研节能科技有限公司 A kind of device and method of condensing recovery pyrolysis gas and application
CN109289225B (en) * 2018-09-12 2021-02-19 国宏中晶集团有限公司 Device and method for condensing and recycling pyrolysis gas and application

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