CN107244692A - It is a kind of to extend the device that yellow lead energy-saving production technology prepares four basic lead sulphates - Google Patents
It is a kind of to extend the device that yellow lead energy-saving production technology prepares four basic lead sulphates Download PDFInfo
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- CN107244692A CN107244692A CN201710363888.9A CN201710363888A CN107244692A CN 107244692 A CN107244692 A CN 107244692A CN 201710363888 A CN201710363888 A CN 201710363888A CN 107244692 A CN107244692 A CN 107244692A
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G21/00—Compounds of lead
- C01G21/20—Sulfates
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
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Abstract
The invention discloses a kind of device for extending yellow lead energy-saving production technology four basic lead sulphates of preparation, including：It is incubated storage vat, automatic metering equipment, circuit orbit, retort, centrifugal device and wastewater collection bucket；The insulation storage vat is arranged on below yellow lead calcining furnace discharging opening, for storing the yellow lead product come out from calcining furnace, the automatic metering equipment is arranged at insulation storage vat feed opening, the circuit orbit is propped by support, form elevated structure, a bit (the initial feeding point) in the center of circle falls in the lower section of insulation storage vat, depending on other positions can be laid out according to workshop；The present invention is simple in construction, practicality is good, fully effectively utilize the product yellow lead of yellow lead production technology, and the temperature after product calcining, not only to realize that energy consumption is low, production efficiency is high, the characteristics of saving production cost, the uniform product appearance equally produced, the waste liquid reusable edible of generation will not bring pollution to environment.
Description
Technical field
The present invention relates to yellow lead deep process technology field, and in particular to one kind extension yellow lead energy-saving production technology prepares four alkali
The device of formula lead sulfate.
Background technology
Current yellow lead production technology is by fusing → powder → calcined oxide → cooling → crushing → packaging processed by lead pig
Into its end product yellow lead (PbO) is directly used in sale, has no the report that production chain directly extends.
The chemical formula of four basic lead sulphates (4BS) is 4PbOPbSO4, equivalent to 4 moles PbO and 1 mole of PbSO4Change
Compound, its primary raw material is PbO and H2SO4.In lead-acid battery industry, 4BS is a kind of anode additive, be in battery just
One of composition of pole active material, appropriate 4BS is added in positive plate production process can promote 4BS in positive plate
Content, is conducive to eliminating capacity of lead acid battery decay, improves cathode performance, improve the service life of lead-acid battery, significantly carry
Rise cost performance, the energy ratio of battery.
4BS preparation method has a variety of in document, such as hydrothermal synthesis method, 3BS thermal decomposition methods, mechanical milling method, Penox
Method, sintering process etc..We have found that the above method has generation 4BS mistakes by the numerous studies to various methods synthesis 4BS processes
The journey time is longer, and is required for heating in addition to expend the energy；And the 4BS purity of synthesis is not enough, particularly 3BS thermal decomposition methods,
The higher defect of production cost.
The content of the invention
The technical problems to be solved by the invention are that offer is a kind of simple in construction, the extension yellow lead production work of energy-conserving and environment-protective
Skill energy-conservation prepares the device of four basic lead sulphates.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of device for extending yellow lead energy-saving production technology four basic lead sulphates of preparation, including：It is incubated storage vat, automatic meter
Measure equipment, circuit orbit, retort, centrifugal device and wastewater collection bucket；
The insulation storage vat is arranged on below yellow lead calcining furnace discharging opening, for storing the yellow lead production come out from calcining furnace
Product, the automatic metering equipment (market-ripe equipment) is arranged at insulation storage vat feed opening, and the circuit orbit is by support
Prop, form elevated structure, a bit (the initial feeding point) in the center of circle falls in the lower section of insulation storage vat, and other positions can basis
Depending on workshop layout；
The retort is provided with three, is divided into the first retort, the second retort and the 3rd retort, three retort
All it is to be made up of base and tank body, four direction pulley is housed below base, can be slided on circuit orbit, pacifies in the middle of base
Equipped with motor, opening two-direction switch can move ahead or retreat, and submounts are tank bodies, and tank body is integrally double-layer oval-shaped shape glass up and down
Glass product, centre is vacuum, and side is inlaid with scale (volume is 200000 cubic centimetres), and liquid is left out in the side against bottom
Mouthful, liquid outlet is connected to centrifugal device by gate valve control using plastic tube, and it is that circle projects upwards about 10mm, protuberance to fill mouth
Exceptionally screw thread is left in side, and sealing plug is that glass is blocked with plastic pipe clip, then blocks filling mouth using sealing gasket rotation, center is left
One aperture, it is straggly above and below the puddler in tank body that stirring prominent outside stirring sheet, aperture is housed up and down equipped with a puddler
Bar is connected to micromachine, and puddler rotation is driven during work；
The centrifugal device is located at the partial below of retort, and the milk containing four basic lead sulphates after reaction completely is beaten
Open a sluice gate after valve, using drop up and down, centrifugal device is flowed into through inlet, the solid-liquor separation after rotation, after liquid is reaction
Waste water, waste water after separation is incorporated into wastewater collection bucket by water pump, solid be moist block four basic lead sulphate (no
Belong to the basic lead sulphate of finished product four)；
The wastewater collection bucket is made up of four cylindrical stainless steels, and yi word pattern is arranged on the one of insulation storage vat
Side, and close to circuit orbit, and erected by support and be higher than 1 meter or so of retort, delivery port, four waste water are left in bottom
The delivery port for collecting bottom of the barrel connects one point of plastic tube respectively, and described point of plastic tube is connected to a main plastic tube, in a point plastic tube
With switching device is housed at main plastics pipe interface, can select to use some collecting vessel, it is convenient to inject water reuse drop
In retort, realization is recycled；Water inlet is directly injected by water pump by water injection pipe from top, and same water injection pipe is also by one
Main plastic tube and four pieces points of plastic tubes, a point plastic tube are connected at wastewater collection bucket, point plastic tube and main plastics pipe interface and are equipped with
Switching device, can select to use some collecting vessel；
The micromachine and agitating device are fixed on base, are arranged on circuit orbit, and can be in circuit orbit
It is upper to slide.
The insulation storage vat is that, by an entirety dimerous up and down, top is cuboid, and bottom four sides is fan
Shape is surrounded, and is double-decker, and centre is vacuum, and heat-preservation cotton is integrally wrapped up outside insulation storage vat.
Also include：Pulverizer, lapping device, baking box and control system；The control system is unified to be arranged on switch board
In, the stirring of retort, the slip of retort are controlled respectively, fed intake and blowing, centrifugal device, the unlatching of water pump, and waste water
Tank switching, baking, crushing, grinding are returned in introducing switching, waste water.
Described baking box, belongs to market-ripe equipment, the solid after will centrifuging, and taking-up is put into baking box drying
.
Described pulverizer, belongs to market-ripe equipment, and its placement location does not have particular requirement, facilitates production to connect in principle
It is continuous to carry out, four basic lead sulphates after drying are put into pulverizer fine particle state is made.
Described lapping device, belongs to market-ripe equipment, and its placement location does not have particular requirement, facilitates production in principle
It is carried out continuously, grinding is to use Gas grinding mode, four basic lead sulphates can be ground into client according to customer demand
The particle diameter needed.
Another object of the present invention is the method that four basic lead sulphates are prepared using said apparatus, and step is as follows：
(1) storage insulation：
Yellow lead drop temperature out of calcining furnace reaches 450 DEG C, therefore sets one to protect below yellow lead calcining furnace discharging opening
Warm storage vat (self-measuring device is housed at storage vat feed opening), is not reduced with the temperature for ensureing yellow lead (lead oxide) product；
(2) first round feeds intake
(1) one-level mixing charging：First retort (reactor, abbreviation A is filled) is moved to below insulation storage vat, first will
30% 125000 cubic centimetres of dilute sulfuric acid prolongs wall injection retort (reactor), and starts agitator, while being protected from storing
Warm bucket discharging opening is dosed to yellow lead product 150kg in retort through automatic metering equipment；
(2) two grades of mixing chargings：In order that the continuity of 4BS productions, while according to the production capacity of yellow lead, there is provided three are big
Small dimension identical retort, and be equidistantly positioned on circular track；After one-level mixing charging is finished, its A tank is moved
Move reaction Accreditation Waiting Area, the second retort abbreviation B tanks are moved to first position (initial position), charging ratio and method and
One-level mixing charging is identical；
(3) three-level mixing charging：3rd retort abbreviation C tanks, are carried out successively；
(4) after the canned material of C are finished, next Accreditation Waiting Area is moved to, now A tanks reach initial point；
(3) second wheels feed intake
(1) second wheel one-level mixing charging：Retort (reactor) abbreviation A is filled, stirring reaction is after 1 hour, now
Insulation storage vat below, from storing heat-preserving container discharging opening be dosed to retort through automatic metering equipment in yellow lead product
100kg；
(2) with the first round (2), (3), (4) step；
(4) third round feeds intake
(1) third round one-level mixing charging：Retort (reactor) abbreviation A is filled, after stirring reaction half an hour, now
Insulation storage vat below, from storing heat-preserving container discharging opening be dosed to retort through automatic metering equipment in yellow lead product
50kg；Yellow lead product and dilute sulfuric acid are with weight ratio 5 in principle：1.001 ratio mixing, makes dilute sulfuric acid slightly excessive, it is ensured that yellow
The all thoroughly reactions, and then lift and ensure the quality of generated finished product of red product；
(2) with the first round second and third, four steps；
(5) separate：I.e. above-mentioned 4th step C tanks third time feeds intake and stops at original place after end, and A tanks are by two small
When course of reaction after, yellow lead product thoroughly reacts completely, in slightly yellow milk, opens the discharge valve of retort, makes it
Centrifugal device is injected, makes its solid-liquor separation, liquid is really reacted waste water, and solid is then four basic lead sulphates；
(6) collect：Waste water after separation is incorporated into wastewater collection bucket by water pump, to be recycled to use；The alkali formula of solid four
Lead sulfate is now in moist block white solid.
(7) dry：The above-mentioned basic lead sulphate of blocks of solid four is inserted in drying baker and dried；
(8) grind：Four basic lead sulphates after above-mentioned drying are inserted in pulverizer, crushing is ground, are made
Four basic lead sulphates.
The beneficial effects of the invention are as follows：The present invention is simple in construction, and practicality is good, fully effectively utilizes yellow lead (PbO) production
Temperature after the product yellow lead (PbO) of technique, and product calcining, not only to realize that energy consumption is low, production efficiency is high, saves production
The characteristics of cost, the uniform product appearance equally produced, the waste liquid reusable edible of generation will not bring pollution to environment.
Brief description of the drawings
Fig. 1 is structural side view of the present invention；
The XRD that Fig. 2 is 4BS prepared by apparatus of the present invention (in figure, top is sample drawing, and bottom is 4BS standard cards)；
Fig. 3 is the prismatic figure of 4BS samples prepared by apparatus of the present invention；
Fig. 4 is graininess figure after 4BS ball millings prepared by apparatus of the present invention.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Conjunction is specifically illustrating, and the present invention is expanded on further.
As shown in Figure 1-2, a kind of device for extending yellow lead energy-saving production technology four basic lead sulphates of preparation, including：Insulation
Storage vat 1, automatic metering equipment 2, circuit orbit 3, retort 4, centrifugal device 5 and wastewater collection bucket 6；
Insulation storage vat 1 is arranged on yellow lead calcining furnace and (not indicated in figure) below discharging opening, goes out for storing from calcining furnace
The yellow lead product come, automatic metering equipment 2 (market-ripe equipment) is arranged at the insulation feed opening of storage vat 1, the quilt of circuit orbit 3
Support 7 is propped, and forms elevated structure, and a bit (the initial feeding point) in the center of circle falls in the lower section of insulation storage vat 1, and other positions can
Depending on being laid out according to workshop；Insulation storage vat 1 is that top is cuboid by an entirety dimerous up and down,
Bottom four sides surrounds for sector, and is double-decker, and centre is vacuum, in the overall parcel heat-preservation cotton in the outside of insulation storage vat 1.
Retort 4 is provided with three, is divided into the first retort, the second retort and the 3rd retort, three retort are all
It is to be made up of base 401 and tank body 402, base 401 is equipped with four direction pulley 403 below, direction pulley 403 is arranged on circle
It on shape track 3, can be slided on circuit orbit 3, motor (not indicated in figure) is installed in the middle of base 401, open suitable open
Pass can move ahead or retreat, and base 401 is tank body 402 above, and it is double-layer oval-shaped shape glassware that tank body is overall about 402, in
Between be vacuum, side is inlaid with scale (volume is 200000 cubic centimetres), and liquid outlet is left against the side of bottom (in figure not
Sign), liquid outlet is connected to centrifugal device 5 by gate valve control using plastic tube, and it is that circle projects upwards about 10mm to fill mouth, dashes forward
Go out portion outboard and leave screw thread, sealing plug is that glass is blocked with plastic pipe clip, then block filling mouth, center using sealing gasket rotation
An aperture is left, up and down equipped with a puddler 404, the puddler in tank body 402 is straggly equipped with stirring sheet 405 about 404, small
Prominent puddler 404 is connected to micromachine 406 outside hole, drives puddler 404 to rotate during work, the He of micromachine 406
Agitating device is fixed on base 401, is arranged on circuit orbit 3, and can be slided on circuit orbit 3.
Centrifugal device 5 is located at the partial below of retort 4, and the milk containing four basic lead sulphates after reaction completely is opened
After gate valve, using drop up and down, centrifugal device 5 is flowed into through inlet, the solid-liquor separation after rotation, liquid is reacted
Waste water, waste water after separation is incorporated into wastewater collection bucket 6 by water pump, solid be moist block four basic lead sulphate (no
Belong to the basic lead sulphate of finished product four)；
Wastewater collection bucket 6 is made up of four cylindrical stainless steels, and yi word pattern is arranged on the side of insulation storage vat 1,
And erected and higher than 4 one meters or so of retort close to circuit orbit 3, and by stake body, delivery port is left in bottom, and four waste water are received
The delivery port of collection bucket 6 bottom connects one point of plastic tube 601 respectively, and a point plastic tube 601 is connected to a main plastic tube 602, in a point modeling
Expects pipe 601 and the interface of main plastic tube 602 are equipped with switching device 603, can select to use some collecting vessel, convenient by waste water
Using in drop injection retort 4, realization is recycled；Water inlet is directly injected by water pump 604 by water injection pipe from top, equally
Water injection pipe is also that, by a main plastic tube and four pieces points of plastic tubes, a point plastic tube is connected to wastewater collection bucket 6, point plastic tube and master
Switching device is housed at plastics pipe interface, can select to use some collecting vessel.
In order to improve the continuity of work, the device also includes：Pulverizer 8, lapping device 9, baking box 10 and control system
System 11；Control system system 11 1 is arranged in switch board, and the stirring of retort, the slip of retort are controlled respectively, feeds intake and puts
Tank switching, baking, crushing, grinding are returned in material, centrifugal device, the unlatching of water pump, and waste water introducing switching, waste water.Baking box 10
Belong to market-ripe equipment, the solid after will centrifuging, taking-up is put into the drying of baking box 10.Pulverizer 8 belongs to city
Field mature equipment, its placement location does not have particular requirement, facilitates production to be carried out continuously in principle, by four alkali formulas after drying
Fine particle state is made in lead sulfate input pulverizer 8.Lapping device 9 belongs to market-ripe equipment, and its placement location does not have
Particular requirement, facilitates production to be carried out continuously in principle, grinding be use Gas grinding mode, can according to customer demand,
Four basic lead sulphates are ground to the particle diameter of client's needs.
The method that four basic lead sulphates are prepared using said apparatus, step is as follows：
(1) storage insulation：
Yellow lead drop temperature out of calcining furnace reaches 450 DEG C, therefore sets one to protect below yellow lead calcining furnace discharging opening
Self-measuring device is housed at warm storage vat, storage vat feed opening, not reduced with the temperature for ensureing yellow lead (lead oxide) product；
(2) first round feeds intake
(1) one-level mixing charging：By the first retort (reactor) be moved to insulation storage vat below, first by 30% it is dilute
125000 cubic centimetres of sulfuric acid prolongs wall injection retort (reactor), and starts agitator, while being discharged from storing heat-preserving container
Mouth is dosed to yellow lead product 150kg in retort through automatic metering equipment；
(2) two grades of mixing chargings：In order that the continuity of 4BS productions, while according to the production capacity of yellow lead, there is provided three are big
Small dimension identical retort, and be equidistantly positioned on circular track；After one-level mixing charging is finished, by the first reaction
Tank is moved to reaction Accreditation Waiting Area, and the second retort is moved to first position (initial position), charging ratio and method and one-level
Mixing charging is identical；
(3) three-level mixing charging：After two grades of mixing chargings are finished, the second retort is moved to reaction Accreditation Waiting Area, the
Three retort are moved to first position (initial position), and charging ratio is identical with one-level mixing charging with method；
After the charging of (4) the 3rd retort is finished, next Accreditation Waiting Area is moved to, now the first retort reaches initial bit
Put；
(3) second wheels feed intake
(1) second wheel one-level mixing charging：After the first retort (reactor) stirring reaction 1 hour, now protecting
Below warm storage vat, from storing heat-preserving container discharging opening be dosed to retort through automatic metering equipment in yellow lead product 100kg；
(2) second two grades of wheel mixing chargings：After the mixing charging of the second wheel one-level is finished, the first retort is moved to instead
Accreditation Waiting Area is answered, the second retort is moved to first position (initial position), charging ratio and method and the second wheel one-level mixing
Charging is identical；
(3) second wheel three-level mixing chargings：After the two grades of mixing chargings of the second wheel are finished, the second retort is moved to instead
Accreditation Waiting Area is answered, the 3rd retort is moved to first position (initial position), charging ratio and method and the second wheel one-level mixing
Charging is identical；
After the charging of (4) the 3rd retort is finished, next Accreditation Waiting Area is moved to, now the first retort reaches initial bit
Put；
(4) third round feeds intake
(1) third round one-level mixing charging：After the first retort (reactor) stirring reaction half an hour, now exist
Be incubated storage vat below, from storing heat-preserving container discharging opening be dosed to retort through automatic metering equipment in yellow lead product
50kg；Yellow lead product and dilute sulfuric acid are with weight ratio 5 in principle：1.001 ratio mixing, makes dilute sulfuric acid slightly excessive, it is ensured that yellow
The all thoroughly reactions, and then lift and ensure the quality of generated finished product of red product；
(2) two grades of mixing chargings of third round：After the mixing charging of third round one-level is finished, the first retort is moved to instead
Accreditation Waiting Area is answered, the second retort is moved to first position (initial position), charging ratio and method and the mixing of third round one-level
Charging is identical；
(3) third round three-level mixing charging：After two grades of mixing chargings of third round are finished, the second retort is moved to instead
Accreditation Waiting Area is answered, the 3rd retort is moved to first position (initial position), charging ratio and method and the mixing of third round one-level
Charging is identical；
The charging of (4) the 3rd retort is finished, stop motion；
(5) separate：Above-mentioned (four) step, that is, the 3rd retort third time feed intake after terminating and stop at original place, and first
Retort is after the course of reaction of two hours, and yellow lead product thoroughly reacts completely, in slightly yellow milk, opens retort
Discharge valve, make its inject centrifugal device, make its solid-liquor separation, liquid is really reacted waste water, and solid is then four alkali
Formula lead sulfate；
(6) collect：Waste water after separation is incorporated into wastewater collection bucket by water pump, to be recycled to use, the alkali formula of solid four
Lead sulfate is now in moist block white solid.
(7) dry：The above-mentioned basic lead sulphate of blocks of solid four is inserted in drying baker and dried；
(8) grind：Four basic lead sulphates after above-mentioned drying are inserted in pulverizer, crushing is ground, are made
Four basic lead sulphates.
The 4BS products of this technique productions and the standard of production technology are as follows：
(1) raw materials for production are yellow lead (PbO) and H2SO4, process do not produce the three wastes；
(2) sample is tested through XRD, wherein not containing other impurity (Fig. 2)；
(3) in SEM photograph, the particle diameter of most particles is between 1~3 micron.
During actual judgement, the diffraction maximum of synthetic sample and 4BS standard PDF cards 23-333 diffraction maximum position complete one
Cause, but relative intensity can be different.Reach that this is required, that is, judge sample as pure 4BS.If gained sample has unnecessary peak,
Then it is determined as with the presence of impurity.
The particle diameter of the sample of synthesis can be determined from scanning electron microscope (SEM) photograph, laser particle analyzer can also be used to determine.This technique
The 4BS samples of synthesis are prismatic (such as Fig. 3), and sample length is 8~20 μm or so, and width is 1 μm or so.After ball milling
Sample is graininess, and particle diameter is less than 1 micron (such as Fig. 4)：Because as crystal seed, particle is the smaller the better.Therefore, every particle diameter is less than
It is qualified that 1~3 μm of person is considered as.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (4)
1. a kind of extend the device that yellow lead energy-saving production technology prepares four basic lead sulphates, it is characterised in that including：It is incubated storing
Bucket, automatic metering equipment, circuit orbit, retort, centrifugal device and wastewater collection bucket；
The insulation storage vat is arranged on below yellow lead calcining furnace discharging opening, for storing the yellow lead product come out from calcining furnace,
The automatic metering equipment is arranged at insulation storage vat feed opening, and the circuit orbit is propped by support；
The retort is provided with three, is divided into the first retort, the second retort and the 3rd retort, three retort are all
It is made up of base and tank body, four direction pulley is housed below base, can slide, be provided with the middle of base on circuit orbit
Motor, opening two-direction switch can move ahead or retreat, and submounts are tank bodies, and tank body is integrally double-layer oval-shaped shape glass system up and down
Product, centre is vacuum, and side is inlaid with scale, and liquid outlet is left against the side of bottom, and liquid outlet uses modeling by gate valve control
Expects pipe is connected to centrifugal device, and it is that circle projects upwards about 10mm to fill mouth, and screw thread is left in ledge outside, and sealing plug is with modeling
Expects pipe card blocks glass, then blocks filling mouth using sealing gasket rotation, an aperture is left at center, up and down equipped with a puddler,
The puddler straggly that protruded outside stirring sheet, aperture that is equipped with is connected to micromachine above and below puddler in tank body, band during work
Dynamic puddler rotation；
The centrifugal device is located at the partial below of retort, and the milk containing four basic lead sulphates after reaction completely opens lock
After valve, using drop up and down, centrifugal device is flowed into through inlet, the solid-liquor separation after rotation, liquid is reacted useless
Water, the waste water after separation is incorporated into wastewater collection bucket by water pump, and solid is moist block four basic lead sulphate；
The wastewater collection bucket is made up of four cylindrical stainless steels, and yi word pattern is arranged on the side of insulation storage vat, and
Close to circuit orbit, and erected by support and be higher than 1 meter or so of retort, delivery port, four wastewater collections are left in bottom
The delivery port of bottom of the barrel connects one point of plastic tube respectively, and described point of plastic tube is connected to a main plastic tube, in point plastic tube and a master
Switching device is housed at plastics pipe interface, can select to use some collecting vessel, convenient inject water reuse drop is reacted
In tank, realization is recycled；Water inlet is directly injected by water pump by water injection pipe from top, and same water injection pipe is also by a main modeling
Expects pipe and four pieces points of plastic tubes, a point plastic tube are connected at wastewater collection bucket, point plastic tube and main plastics pipe interface equipped with switching
Device, can select to use some collecting vessel.
2. a kind of device for extending yellow lead energy-saving production technology four basic lead sulphates of preparation according to claim 1, it is special
Levy and be, the micromachine and agitating device are fixed on base, are arranged on circuit orbit, and can be on circuit orbit
Slide.
3. a kind of device for extending yellow lead energy-saving production technology four basic lead sulphates of preparation according to claim 1, it is special
Levy and be, the insulation storage vat is that, by an entirety dimerous up and down, top is cuboid, and bottom four sides is sector
Surround, and be double-decker, centre is vacuum, heat-preservation cotton is integrally wrapped up outside insulation storage vat.
4. a kind of device for extending yellow lead energy-saving production technology four basic lead sulphates of preparation according to claim 1, it is special
Levy and be, in addition to：Pulverizer, lapping device, baking box and control system；The control system is unified to be arranged on switch board
In, the stirring of retort, the slip of retort are controlled respectively, fed intake and blowing, centrifugal device, the unlatching of water pump, and waste water
Tank switching, baking, crushing, grinding are returned in introducing switching, waste water.
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| CN201710363888.9A CN107244692B (en) | 2017-05-22 | 2017-05-22 | A kind of device for extending yellow lead energy-saving production technology and preparing four basic lead sulphates |
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| CN201710363888.9A CN107244692B (en) | 2017-05-22 | 2017-05-22 | A kind of device for extending yellow lead energy-saving production technology and preparing four basic lead sulphates |
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| CN107244692B CN107244692B (en) | 2018-09-18 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107834065A (en) * | 2017-10-27 | 2018-03-23 | 超威电源有限公司 | The adding set and adding method of liquid additive during a kind of lead-acid accumulator and cream |
| CN109709306A (en) * | 2019-01-03 | 2019-05-03 | 河南大学 | A kind of soil acidification soil improvement experimental provision |
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| CN107244692B (en) | 2018-09-18 |
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