CN107226759A - A kind of utilization straw makes the secondary fermentation of fertilizer - Google Patents

A kind of utilization straw makes the secondary fermentation of fertilizer Download PDF

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Publication number
CN107226759A
CN107226759A CN201710295335.4A CN201710295335A CN107226759A CN 107226759 A CN107226759 A CN 107226759A CN 201710295335 A CN201710295335 A CN 201710295335A CN 107226759 A CN107226759 A CN 107226759A
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China
Prior art keywords
mixture
parts
fertilizer
bank
mixed
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CN201710295335.4A
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Chinese (zh)
Inventor
倪龙珠
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NANJING MINGZHU FERTILIZER CO Ltd
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NANJING MINGZHU FERTILIZER CO Ltd
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Priority to CN201710295335.4A priority Critical patent/CN107226759A/en
Publication of CN107226759A publication Critical patent/CN107226759A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C11/00Other nitrogenous fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/50Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Abstract

The present invention relates to the secondary fermentation that a kind of utilization straw makes fertilizer, comprise the following steps that:1)Starch, tryptophan protein kinase, clay powder are mixed;2)By step 1)Mixture piles bank, and is positioned in solar energy fermentation greenhouse;3)Catalyst is uniformly sprayed at step 2)On bank outer surface;4)Material after one time fermentation is placed on by step 3)On bank after processing, and the material after one time fermentation is piled into bank;5)Bank is placed, the oxygen content and moisture content of bank is adjusted, continues to react 13 16 days;6)Bank is turned over into throwing by machinery;After machinery, which is turned over, to be thrown 4 days, then mechanical turning and throwing once;After throwing is turned over for the second time, material is spread out and dried, you can complete to make the secondary fermentation of fertilizer using straw;A kind of utilization straw is made after the secondary fermentation of fertilizer in the present invention, and the yield of fertilizer effectively improves 23.51 24.69%;Antibacterial ability effectively improves 18 22%.

Description

A kind of utilization straw makes the secondary fermentation of fertilizer
Technical field
The invention belongs to the production field of fertilizer fermentation, and in particular to a kind of utilization straw makes the secondary hair of fertilizer Ferment technique.
Background technology
The Fertilizer nutrient element made using straw is complete, being capable of improved soil, the soil that improvement is caused using chemical fertilizer Earth is hardened, improves soil physical and chemical property, enhancing soil water-retaining, fertilizer conservation, the ability of fertilizer.Beneficial microbe in fertilizer enters to bury In earth, harmful bacteria growing can be suppressed and beneficial bacterium is converted into, interact, mutually promote, play the synergy of colony, promote Enter and regulate and control plant growth, effectively the enhancing degeneration-resistant resistance against diseases of crop.
When current China produces to fertilizer in the prior art, mainly sent out using traditional one time fermentation method Ferment, though sponge dough method cycle short rotten degree is not uniform enough, the not high fertilizer efficiency of materials quality is low, and contains nuisance in fertilizer Matter, can cause certain pollution to environment, and the chemical fertilizer produced can not meet the demand of in the market, therefore, how produce one Plant turns into numerous producers problem to be solved with the fertilizer that fertilizer efficiency is high, pollution is small.
The content of the invention
There is provided the secondary hair that a kind of utilization straw makes fertilizer for the deficiencies in the prior art by the present invention Ferment technique, to solve problems of the prior art.
To achieve the above object, the technical solution adopted by the present invention is as follows:
A kind of utilization straw makes the secondary fermentation of fertilizer, comprises the following steps that:1)By 3-4 parts of starch, tryptophan 1-2 parts of protein kinase, 40-43 parts of clay powder are mixed evenly;
2)Step 1 will be passed through)Reacted mixture piles a height of 0.5-0.8 meters, a width of 1-2 meters bank, and is positioned over In solar energy fermentation greenhouse;
3)Catalyst is uniformly sprayed at step 2)On bank outer surface;
4)Material after one time fermentation is placed on by step 3)On bank after processing, and will be after one time fermentation Material pile high 2.5-3 meters, wide 4-5 meters bank, by irregular manually being arranged;
5)After bank is placed 5-6 days when temperature reaches 50-53 DEG C, the oxygen content and moisture content of bank are adjusted, makes thing Stockpile is that 6-15%, water content continue reaction 13-16 days under conditions of 43-46% in oxygen content;
6)After by machinery bank is turned over into throwing 4-5 days, daily temperature is recorded;Temperature exists after machinery, which is turned over, to be thrown 4 days At 51-56 DEG C, then mechanical turning and throwing once, and record daily temperature;When it is 71-76 DEG C to turn over the temperature after throwing for the second time, Spread material out progress to dry 13-15 days, and control its water content to be 34-38%, you can complete to make fertilizer using straw Secondary fermentation.
As a modification of the present invention, the step 3)The production technology of middle catalyst is as follows:(1)By warm actinomyces, Filamentous fungi, Trichoderma viride, thermophilic Bacillus are put in a kettle., and seal 3-5 after mixture is stirred at normal temperatures After it, 1-2 parts of glutathione peroxidase, 2-3 parts of whiterot fungi, -6 parts of catalase-3, cellulose are added into mixture 2-4 parts of enzyme and after being mixed, mixture is put into PDA liquid medium, and make mixture react 2.5-3.5 days after mistake Filter;
(2)After 24-27 parts of mushroom slag, 7-9 parts of bagasse, 12-15 parts of manioc waste are pulverized and mixed, and mixture is put into Boiling 20-30 minutes is carried out to 70-75 DEG C;
(3)After golden 8-9 parts of clock rattan, 16-19 parts of clover are pulverized and mixed, ethanol is added into mixture, and make mixture Filtered after carrying out immersion 30-40 minutes, added into filtrate and pass through step(2)Reacted mixture is simultaneously stirred, and will be stirred Mixture afterwards extract 6 times, each 1-1.5 hours, merges extract solution;
(4)Step will be passed through(3)After 4-5 parts of glucose of addition is mixed in filtrate after extraction, 26-28 parts of water is added, And mixture is put into distilling apparatus, and mixture is carried out after distilling 3-4 hours, mixture is passed through to filter It is middle to be filtered;
(5)After nacrite, kaolin, diatomite, gypsum are mixed, mixture is put into reducing mechanism and carries out powder After broken, 35-37 parts of water is added into mixture, and mixture is put into is stirred into agitating device after 49-52 minutes, plus Enter by step(1)Reacted filtered fluid, and stir;
(6)By perlite ore, 22-24 parts are put at 1000-1300 DEG C cooling after progress is calcined 4-5 minutes;
(7)By step(5)The mixture and step of generation(6)After the mixture of generation is mixed, add and add by closing stirring Heat is cooled down to 60-65 DEG C after being further continued for stirring 10-15 minutes;
(8)Step will be passed through(7)Pass through step in reacted mixture(3)Reacted extract solution is well mixed, will Cooled down after mixture water-bath insulation, and mixture is carried out after suction filtration, it is dry for the first time that mixture is put into progress in drying device It is dry;
(9)To step(8)Step is passed through in middle addition(4)Reacted filtered fluid, and will be cooled down after mixture progress water-bath insulation, Suction filtration, mixture is put into drying device and dry for the second time;
(10)Step will be passed through(9)Reacted mixture is put into 510-530 DEG C of high temperature furnace, and carries out roasting 20-24 Minute, mixture is put into and crushed into reducing mechanism, 24-26 parts of glucose is added into the mixture after crushing and is incited somebody to action Mixture is stirred, and the mixture after stirring is put into processor for ultrasonic wave, using 100-130W ultrasonication After 2-4 hours, mixture is passed through into extruder grain, you can obtain catalyst.
As a modification of the present invention, the step(2)Middle mushroom slag is mushroom, mushroom, agaric, the mixing of apricot spore mushroom Thing.
As a modification of the present invention, the mushroom, mushroom, agaric, the mass ratio of apricot spore mushroom are 4:3:1:5.
As a modification of the present invention, the step(1)Middle temperature actinomyces, filamentous fungi, Trichoderma viride, thermophilic gemma The mass ratio of bacterium is 3:1:6:1.
As a modification of the present invention, the step(5)Middle nacrite, kaolin, diatomite, the mass ratio of gypsum are 2: 7:2:1。
As a result of above technology, the present invention compared with the prior art, has the advantage that as follows:
After a kind of secondary fermentation of the present invention by making fertilizer to utilization straw, the yield of fertilizer is effectively improved 23.51-24.69%;Antibacterial ability effectively improves 18-22%;The micronutrient levels such as nitrogen, phosphorus, potassium are improved, and can have nitrogen Effect improves 12-17%, and P elements effectively improve 13-15%, and potassium element effectively improves 12-15%;The present invention utilizes plant by one kind Stalk makes the secondary fermentation of fertilizer, can effectively increase the production efficiency of fertilizer, be effectively improved the fertilizer efficiency of soil, fertilizer The plant recovery of nutrient of material is up to 55-58%;A kind of utilization straw makes the secondary fermentation of fertilizer in the present invention, passes through Catalyst is added, the production efficiency for the secondary fermentation that fertilizer is made using straw can be effectively increased, produced Fertilizer advantageously in the absorption of plant.
Embodiment
With reference to embodiment, the present invention is furture elucidated.
Embodiment 1:
A kind of utilization straw makes the secondary fermentation of fertilizer, comprises the following steps that:1)By 3 parts of starch, tryptophan egg White kinases 2,40 parts of clay powder are mixed evenly;
2)Step 1 will be passed through)Reacted mixture piles a height of 0.8 meter, a width of 1 meter of bank, and is positioned over solar energy Ferment in greenhouse;
3)Catalyst is uniformly sprayed at step 2)On bank outer surface;
4)Material after one time fermentation is placed on by step 3)On bank after processing, and will be after one time fermentation Material pile high 3 meters, wide 4 meters of bank, by irregular manually being arranged;
5)After bank is placed 5 days when temperature reaches 53 DEG C, the oxygen content and moisture content of bank are adjusted, bank is existed Oxygen content is that 15%, water content continues reaction 16 days under conditions of 43%;
6)After by machinery bank is turned over into throwing 4 days, daily temperature is recorded;Temperature is 56 after machinery, which is turned over, to be thrown 4 days DEG C when, then mechanical turning and throwing once, and record daily temperature;When it is 71 DEG C to turn over the temperature after throwing for the second time, material is spread out Drive row into dry 15 days, and control its water content to be 34%, you can complete to make the secondary fermentation work of fertilizer using straw Skill.
The step 3)The production technology of middle catalyst is as follows:(1)By warm actinomyces, filamentous fungi, Trichoderma viride, thermophilic Bacillus is put in a kettle., and gluathione is added into mixture after sealing 5 days after mixture is stirred at normal temperatures 2 parts of peptide peroxidase, 3 parts of whiterot fungi, catalase-3 part, 4 parts of cellulase and after being mixed, mixture is put into Into PDA liquid medium, and mixture is set to be filtered after reacting 2.5 days;The step(1)It is middle temperature actinomyces, filamentous fungi, green Color trichoderma, the mass ratio of thermophilic Bacillus are 3:1:6:1;
(2)After 27 parts of mushroom slag, 7 parts of bagasse, 15 parts of manioc waste are pulverized and mixed, and mixture is put at 70 DEG C Carry out boiling 30 minutes;The step(2)Middle mushroom slag is mushroom, mushroom, agaric, the mixture of apricot spore mushroom;The mushroom, mushroom Mushroom, agaric, the mass ratio of apricot spore mushroom are 4:3:1:5;
(3)After golden 8 parts of clock rattan, 19 parts of clover are pulverized and mixed, ethanol is added into mixture, and soaked mixture Bubble is filtered after 30 minutes, is added into filtrate and is passed through step(2)Reacted mixture is simultaneously stirred, by the mixture after stirring Extract 6 times, 1.5 hours every time, merge extract solution;
(4)Step will be passed through(3)After 4 parts of glucose of addition is mixed in filtrate after extraction, 28 parts of water is added, and will be mixed Compound is put into distilling apparatus, and mixture is carried out after distilling 3 hours, and mixture is passed through into filter and carried out Filter;
(5)After nacrite, kaolin, diatomite, gypsum are mixed, mixture is put into reducing mechanism and carries out powder After broken, 37 parts of water is added into mixture, and mixture is put into is stirred into agitating device after 49 minutes, adds and passes through Step(1)Reacted filtered fluid, and stir;The step(5)Middle nacrite, kaolin, diatomite, the mass ratio of gypsum For 2:7:2:1;
(6)By perlite ore, 24 parts are put at 1000 DEG C cooling after progress is calcined 5 minutes;
(7)By step(5)The mixture and step of generation(6)After the mixture of generation is mixed, add and add by closing stirring Heat is cooled down to 60 DEG C after being further continued for stirring 15 minutes;
(8)Step will be passed through(7)Pass through step in reacted mixture(3)Reacted extract solution is well mixed, will Cooled down after mixture water-bath insulation, and mixture is carried out after suction filtration, it is dry for the first time that mixture is put into progress in drying device It is dry;
(9)To step(8)Step is passed through in middle addition(4)Reacted filtered fluid, and will be cooled down after mixture progress water-bath insulation, Suction filtration, mixture is put into drying device and dry for the second time;
(10)Step will be passed through(9)Reacted mixture is put into 510 DEG C of high temperature furnace, and carries out roasting 24 minutes, will Mixture is put into be crushed into reducing mechanism, and 26 parts of glucose is added into the mixture after crushing and mixture is carried out Stirring, the mixture after stirring is put into processor for ultrasonic wave, after 130W ultrasonication 4 hours, will be mixed Thing passes through extruder grain, you can obtain catalyst.
After a kind of secondary fermentation of the present invention by making fertilizer to utilization straw, the yield of fertilizer is effectively carried High 23.51-24.69%;Antibacterial ability effectively improves 18-22%;The micronutrient levels such as nitrogen, phosphorus, potassium are improved, and can make nitrogen 12-17% is effectively improved, P elements effectively improve 13-15%, and potassium element effectively improves 12-15%;The present invention utilizes plant by one kind Thing stalk makes the secondary fermentation of fertilizer, can effectively increase the production efficiency of fertilizer, be effectively improved the fertilizer efficiency of soil, The plant recovery of nutrient of fertilizer is up to 55-58%.
Embodiment 2:
A kind of utilization straw makes the secondary fermentation of fertilizer, comprises the following steps that:1)By 4 parts of starch, tryptophan egg White 1 part of kinases, 43 parts of clay powder are mixed evenly;
2)Step 1 will be passed through)Reacted mixture piles a height of 0.5 meter, a width of 2 meters of bank, and is positioned over solar energy Ferment in greenhouse;
3)Catalyst is uniformly sprayed at step 2)On bank outer surface;
4)Material after one time fermentation is placed on by step 3)On bank after processing, and will be after one time fermentation Material pile high 3 meters, wide 4 meters of bank, by irregular manually being arranged;
5)After bank is placed 6 days when temperature reaches 50 DEG C, the oxygen content and moisture content of bank are adjusted, bank is existed Oxygen content is that 15%, water content continues reaction 16 days under conditions of 43%;
6)After by machinery bank is turned over into throwing 5 days, daily temperature is recorded;Temperature is 56 after machinery, which is turned over, to be thrown 4 days DEG C when, then mechanical turning and throwing once, and record daily temperature;When it is 71 DEG C to turn over the temperature after throwing for the second time, material is spread out Drive row into dry 13 days, and control its water content to be 38%, you can complete to make the secondary fermentation work of fertilizer using straw Skill.
The step 3)The production technology of middle catalyst is as follows:(1)By warm actinomyces, filamentous fungi, Trichoderma viride, thermophilic Bacillus is put in a kettle., and gluathione is added into mixture after sealing 5 days after mixture is stirred at normal temperatures 2 parts of peptide peroxidase, 2 parts of whiterot fungi, 6 parts of catalase, 2 parts of cellulase and after being mixed, mixture is put into Into PDA liquid medium, and mixture is set to be filtered after reacting 3.5 days;The step(1)It is middle temperature actinomyces, filamentous fungi, green Color trichoderma, the mass ratio of thermophilic Bacillus are 3:1:6:1;
(2)After 24 parts of mushroom slag, 9 parts of bagasse, 12 parts of manioc waste are pulverized and mixed, and mixture is put at 75 DEG C Carry out boiling 20 minutes;The step(2)Middle mushroom slag is mushroom, mushroom, agaric, the mixture of apricot spore mushroom;The mushroom, mushroom Mushroom, agaric, the mass ratio of apricot spore mushroom are 4:3:1:5;
(3)After golden 9 parts of clock rattan, 16 parts of clover are pulverized and mixed, ethanol is added into mixture, and soaked mixture Bubble is filtered after 40 minutes, is added into filtrate and is passed through step(2)Reacted mixture is simultaneously stirred, by the mixture after stirring Extract 6 times, 1 hour every time, merge extract solution;
(4)Step will be passed through(3)After 5 parts of glucose of addition is mixed in filtrate after extraction, 26 parts of water is added, and will be mixed Compound is put into distilling apparatus, and mixture is carried out after distilling 4 hours, and mixture is passed through into filter and carried out Filter;
(5)After nacrite, kaolin, diatomite, gypsum are mixed, mixture is put into reducing mechanism and carries out powder After broken, 35 parts of water is added into mixture, and mixture is put into is stirred into agitating device after 52 minutes, adds and passes through Step(1)Reacted filtered fluid, and stir;The step(5)Middle nacrite, kaolin, diatomite, the mass ratio of gypsum For 2:7:2:1;
(6)By perlite ore, 24 parts are put at 1000 DEG C cooling after progress is calcined 5 minutes;
(7)By step(5)The mixture and step of generation(6)After the mixture of generation is mixed, add and add by closing stirring Heat is cooled down to 60 DEG C after being further continued for stirring 15 minutes;
(8)Step will be passed through(7)Pass through step in reacted mixture(3)Reacted extract solution is well mixed, will Cooled down after mixture water-bath insulation, and mixture is carried out after suction filtration, it is dry for the first time that mixture is put into progress in drying device It is dry;
(9)To step(8)Step is passed through in middle addition(4)Reacted filtered fluid, and will be cooled down after mixture progress water-bath insulation, Suction filtration, mixture is put into drying device and dry for the second time;
(10)Step will be passed through(9)Reacted mixture is put into 530 DEG C of high temperature furnace, and carries out roasting 24 minutes, will Mixture is put into be crushed into reducing mechanism, and 26 parts of glucose is added into the mixture after crushing and mixture is carried out Stirring, the mixture after stirring is put into processor for ultrasonic wave, after 100W ultrasonication 2 hours, will be mixed Thing passes through extruder grain, you can obtain catalyst.
After a kind of secondary fermentation of the present invention by making fertilizer to utilization straw, the yield of fertilizer is effectively carried High 23.41-24.63%;Antibacterial ability effectively improves 17-21%;The micronutrient levels such as nitrogen, phosphorus, potassium are improved, and can make nitrogen 14-16% is effectively improved, P elements effectively improve 14-15%, and potassium element effectively improves 11-14%;The present invention utilizes plant by one kind Thing stalk makes the secondary fermentation of fertilizer, can effectively increase the production efficiency of fertilizer, be effectively improved the fertilizer efficiency of soil, The plant recovery of nutrient of fertilizer is up to 57-58%.
Embodiment 3:
A kind of utilization straw makes the secondary fermentation of fertilizer, comprises the following steps that:1)By 4 parts of starch, tryptophan egg White 1 part of kinases, 42 parts of clay powder are mixed evenly;
2)Step 1 will be passed through)Reacted mixture piles a height of 0.5 meter, a width of 2 meters of bank, and is positioned over solar energy Ferment in greenhouse;
3)Catalyst is uniformly sprayed at step 2)On bank outer surface;
4)Material after one time fermentation is placed on by step 3)On bank after processing, and will be after one time fermentation Material pile high 3 meters, wide 4 meters of bank, by irregular manually being arranged;
5)After bank is placed 6 days when temperature reaches 52 DEG C, the oxygen content and moisture content of bank are adjusted, bank is existed Oxygen content is that 13%, water content continues reaction 15 days under conditions of 45%;
6)After by machinery bank is turned over into throwing 4 days, daily temperature is recorded;Temperature is 56 after machinery, which is turned over, to be thrown 4 days DEG C when, then mechanical turning and throwing once, and record daily temperature;When it is 73 DEG C to turn over the temperature after throwing for the second time, material is spread out Drive row into dry 13 days, and control its water content to be 38%, you can complete to make the secondary fermentation work of fertilizer using straw Skill.
The step 3)The production technology of middle catalyst is as follows:(1)By warm actinomyces, filamentous fungi, Trichoderma viride, thermophilic Bacillus is put in a kettle., and gluathione is added into mixture after sealing 4 days after mixture is stirred at normal temperatures 1 part of peptide peroxidase, 3 parts of whiterot fungi, catalase-3 part, 4 parts of cellulase and after being mixed, mixture is put into Into PDA liquid medium, and mixture is set to be filtered after reacting 3.5 days;The step(1)It is middle temperature actinomyces, filamentous fungi, green Color trichoderma, the mass ratio of thermophilic Bacillus are 3:1:6:1;
(2)After 27 parts of mushroom slag, 9 parts of bagasse, 12 parts of manioc waste are pulverized and mixed, and mixture is put at 75 DEG C Carry out boiling 28 minutes;The step(2)Middle mushroom slag is mushroom, mushroom, agaric, the mixture of apricot spore mushroom;The mushroom, mushroom Mushroom, agaric, the mass ratio of apricot spore mushroom are 4:3:1:5;
(3)After golden 9 parts of clock rattan, 19 parts of clover are pulverized and mixed, ethanol is added into mixture, and soaked mixture Bubble is filtered after 30 minutes, is added into filtrate and is passed through step(2)Reacted mixture is simultaneously stirred, by the mixture after stirring Extract 6 times, 1.5 hours every time, merge extract solution;
(4)Step will be passed through(3)After 5 parts of glucose of addition is mixed in filtrate after extraction, 27 parts of water is added, and will be mixed Compound is put into distilling apparatus, and mixture is carried out after distilling 4 hours, and mixture is passed through into filter and carried out Filter;
(5)After nacrite, kaolin, diatomite, gypsum are mixed, mixture is put into reducing mechanism and carries out powder After broken, 35 parts of water is added into mixture, and mixture is put into is stirred into agitating device after 52 minutes, adds and passes through Step(1)Reacted filtered fluid, and stir;The step(5)Middle nacrite, kaolin, diatomite, the mass ratio of gypsum For 2:7:2:1;
(6)By perlite ore, 23 parts are put at 1000 DEG C cooling after progress is calcined 5 minutes;
(7)By step(5)The mixture and step of generation(6)After the mixture of generation is mixed, add and add by closing stirring Heat is cooled down to 60 DEG C after being further continued for stirring 15 minutes;
(8)Step will be passed through(7)Pass through step in reacted mixture(3)Reacted extract solution is well mixed, will Cooled down after mixture water-bath insulation, and mixture is carried out after suction filtration, it is dry for the first time that mixture is put into progress in drying device It is dry;
(9)To step(8)Step is passed through in middle addition(4)Reacted filtered fluid, and will be cooled down after mixture progress water-bath insulation, Suction filtration, mixture is put into drying device and dry for the second time;
(10)Step will be passed through(9)Reacted mixture is put into 530 DEG C of high temperature furnace, and carries out roasting 20 minutes, will Mixture is put into be crushed into reducing mechanism, and 26 parts of glucose is added into the mixture after crushing and mixture is carried out Stirring, the mixture after stirring is put into processor for ultrasonic wave, after 130W ultrasonication 4 hours, will be mixed Thing passes through extruder grain, you can obtain catalyst.
After a kind of secondary fermentation of the present invention by making fertilizer to utilization straw, the yield of fertilizer is effectively carried High 23.51-24.57%;Antibacterial ability effectively improves 18-21%;The micronutrient levels such as nitrogen, phosphorus, potassium are improved, and can make nitrogen 12-16% is effectively improved, P elements effectively improve 13-14%, and potassium element effectively improves 12-14%;The present invention utilizes plant by one kind Thing stalk makes the secondary fermentation of fertilizer, can effectively increase the production efficiency of fertilizer, be effectively improved the fertilizer efficiency of soil, The plant recovery of nutrient of fertilizer is up to 55-57%.
Above-described embodiment is only the preferred technical solution of the present invention, and is not construed as the limitation for the present invention, the present invention The technical scheme that should be recorded with claim of protection domain, including in the technical scheme recorded of claim technical characteristic etc. It is protection domain with alternative, i.e., equivalent substitution within this range is improved, also within protection scope of the present invention.

Claims (6)

1. a kind of utilization straw makes the secondary fermentation of fertilizer, it is characterised in that comprise the following steps that:1)By starch 3-4 parts, 1-2 parts of tryptophan protein kinase, 40-43 parts of clay powder be mixed evenly;
2)Step 1 will be passed through)Reacted mixture piles a height of 0.5-0.8 meters, a width of 1-2 meters bank, and is positioned over In solar energy fermentation greenhouse;
3)Catalyst is uniformly sprayed at step 2)On bank outer surface;
4)Material after one time fermentation is placed on by step 3)On bank after processing, and will be after one time fermentation Material pile high 2.5-3 meters, wide 4-5 meters bank, by irregular manually being arranged;
5)After bank is placed 5-6 days when temperature reaches 50-53 DEG C, the oxygen content and moisture content of bank are adjusted, makes thing Stockpile is that 6-15%, water content continue reaction 13-16 days under conditions of 43-46% in oxygen content;
6)After by machinery bank is turned over into throwing 4-5 days, daily temperature is recorded;Temperature exists after machinery, which is turned over, to be thrown 4 days At 51-56 DEG C, then mechanical turning and throwing once, and record daily temperature;When it is 71-76 DEG C to turn over the temperature after throwing for the second time, Spread material out progress to dry 13-15 days, and control its water content to be 34-38%, you can complete to make fertilizer using straw Secondary fermentation.
2. a kind of utilization straw according to claim 1 makes the secondary fermentation of fertilizer, it is characterised in that institute State step 3)The production technology of middle catalyst is as follows:(1)Warm actinomyces, filamentous fungi, Trichoderma viride, thermophilic Bacillus are placed on In reactor, and after mixture is stirred at normal temperatures after sealing 3-5 days, the addition glutathione peroxidating into mixture 1-2 parts of thing enzyme, 2-3 parts of whiterot fungi, -6 parts of catalase-3,2-4 parts of cellulase and after being mixed, mixture is put into Into PDA liquid medium, and mixture is set to be filtered after reacting 2.5-3.5 days;
(2)After 24-27 parts of mushroom slag, 7-9 parts of bagasse, 12-15 parts of manioc waste are pulverized and mixed, and mixture is put into Boiling 20-30 minutes is carried out to 70-75 DEG C;
(3)After golden 8-9 parts of clock rattan, 16-19 parts of clover are pulverized and mixed, ethanol is added into mixture, and make mixture Filtered after carrying out immersion 30-40 minutes, added into filtrate and pass through step(2)Reacted mixture is simultaneously stirred, and will be stirred Mixture afterwards extract 6 times, each 1-1.5 hours, merges extract solution;
(4)Step will be passed through(3)After 4-5 parts of glucose of addition is mixed in filtrate after extraction, 26-28 parts of water is added, And mixture is put into distilling apparatus, and mixture is carried out after distilling 3-4 hours, mixture is passed through to filter It is middle to be filtered;
(5)After nacrite, kaolin, diatomite, gypsum are mixed, mixture is put into reducing mechanism and carries out powder After broken, 35-37 parts of water is added into mixture, and mixture is put into is stirred into agitating device after 49-52 minutes, plus Enter by step(1)Reacted filtered fluid, and stir;
(6)By perlite ore, 22-24 parts are put at 1000-1300 DEG C cooling after progress is calcined 4-5 minutes;
(7)By step(5)The mixture and step of generation(6)After the mixture of generation is mixed, add and add by closing stirring Heat is cooled down to 60-65 DEG C after being further continued for stirring 10-15 minutes;
(8)Step will be passed through(7)Pass through step in reacted mixture(3)Reacted extract solution is well mixed, will Cooled down after mixture water-bath insulation, and mixture is carried out after suction filtration, it is dry for the first time that mixture is put into progress in drying device It is dry;
(9)To step(8)Step is passed through in middle addition(4)Reacted filtered fluid, and will be cooled down after mixture progress water-bath insulation, Suction filtration, mixture is put into drying device and dry for the second time;
(10)Step will be passed through(9)Reacted mixture is put into 510-530 DEG C of high temperature furnace, and carries out roasting 20-24 Minute, mixture is put into and crushed into reducing mechanism, 24-26 parts of glucose is added into the mixture after crushing and is incited somebody to action Mixture is stirred, and the mixture after stirring is put into processor for ultrasonic wave, using 100-130W ultrasonication After 2-4 hours, mixture is passed through into extruder grain, you can obtain catalyst.
3. a kind of utilization straw according to claim 2 makes the secondary fermentation of fertilizer, it is characterised in that:Institute State step(2)Middle mushroom slag is mushroom, mushroom, agaric, the mixture of apricot spore mushroom.
4. a kind of utilization straw according to claim 3 makes the secondary fermentation of fertilizer, it is characterised in that:Institute It is 4 to state mushroom, mushroom, agaric, the mass ratio of apricot spore mushroom:3:1:5.
5. a kind of utilization straw according to claim 2 makes the secondary fermentation of fertilizer, it is characterised in that:Institute State step(1)Middle temperature actinomyces, filamentous fungi, Trichoderma viride, the mass ratio of thermophilic Bacillus are 3:1:6:1.
6. a kind of utilization straw according to claim 2 makes the secondary fermentation of fertilizer, it is characterised in that:Institute State step(5)Middle nacrite, kaolin, diatomite, the mass ratio of gypsum are 2:7:2:1.
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CN109942322A (en) * 2017-12-21 2019-06-28 兴业县众旺种植专业合作社 A kind of passion fruit organic fertilizer
CN112159284A (en) * 2020-09-15 2021-01-01 南京明珠肥料有限责任公司 Process for producing biological organic fertilizer by plant straws and traditional Chinese medicine residues
CN112159285A (en) * 2020-09-15 2021-01-01 南京明珠肥料有限责任公司 Preparation process for producing organic fertilizer by plant straws and traditional Chinese medicine residues
CN114230412A (en) * 2021-12-23 2022-03-25 嘉兴上柒寸生物科技有限公司 Preparation method and equipment for secondary fermentation of straw protein by using rhizopus oligosporus

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Application publication date: 20171003