CN107216551A - A kind of preparation method of novel furniture composite board - Google Patents
A kind of preparation method of novel furniture composite board Download PDFInfo
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- CN107216551A CN107216551A CN201710408323.8A CN201710408323A CN107216551A CN 107216551 A CN107216551 A CN 107216551A CN 201710408323 A CN201710408323 A CN 201710408323A CN 107216551 A CN107216551 A CN 107216551A
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- composite board
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- novel furniture
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/10—Homopolymers or copolymers of propene
- C08L23/12—Polypropene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L25/00—Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
- C08L25/02—Homopolymers or copolymers of hydrocarbons
- C08L25/04—Homopolymers or copolymers of styrene
- C08L25/06—Polystyrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2296—Oxides; Hydroxides of metals of zinc
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Dry Formation Of Fiberboard And The Like (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention discloses a kind of preparation method of novel furniture composite board, including following operating procedure：（1）Will be standby after thermoplastic resin extruding pelletization；（2）After string is crushed, surface activation process is carried out using activating solution, the string after activation is made；（3）String is mixed with the thermoplastic resin after granulation, additive is added thereto, mixture is preheated to 70 80 DEG C, 30min is incubated；（4）Novel furniture composite board is made in mixture heating, compacting after preheating.The preparation method of the novel furniture composite board provided using the present invention, obtained composite board, not only excellent in mechanical performance, and almost odorlessness will not produce harm to the health of consumer.
Description
Technical field
The invention belongs to Furniture panel field, and in particular to a kind of preparation method of furniture composite board.
Background technology
Solid wood board is exactly the wood plank being made of complete timber, and these sheet materials are sturdy and durable, lines is naturally, be finishing
In it is excellent in choosing, but because such sheet material cost is high, construction process requirement is high, and raw material is rareer, is made of solid wood board
Furniture out, costly, with the development of modern technologies, wood-based plate is widely used price in furniture industry.
But commercially available common wood-based plate, generally existing that intensity is not high, and mechanical property is poor, and binding agent used in wood-based plate
Excessively, cause the smell of composite board excessive, the health to user causes harm.
The content of the invention
In order to solve the above problems, the present invention provides a kind of preparation method of novel furniture composite board.
The present invention is achieved by the following technical solutions.
A kind of preparation method of novel furniture composite board, including following operating procedure：
（1）Will be standby after thermoplastic resin extruding pelletization；
（2）After string is crushed, surface activation process is carried out using activating solution, the string after activation is made, wherein
String is made up of the component of following parts by weight：30-40 parts of soybean stalk, 6-9 parts of the banksia rose, 10-15 parts of PERICARPIUM ARECAE, wherein living
Change liquid to be made up of the component of following parts by weight：11-18 parts of methylpropene sodium sulfonate, 9-13 parts of ethylenediamine base propanesulfonate, chloromethane
Sour 11-16 parts of diethylene glycol (DEG) ester, 4-8 parts of pentylcyclohexyl benzoic acid, 7-12 parts of ethylene thiourea, 60-80 parts of absolute ethyl alcohol, water 150-
200 parts；
（3）String is mixed with the thermoplastic resin after granulation, additive is added thereto, mixture is preheated to 70-
80 DEG C, 30min is incubated, wherein additive is made up of the component of following parts by weight：5-8 parts of nano zine oxide, dibutyl sulfide urea 10-15
Part, 11-14 parts of silane coupler NXH-132,13-16 parts of PTPP；
（4）Novel furniture composite board is made in mixture heating, compacting after preheating.
Specifically, above-mentioned thermoplastic resin is times in polyvinyl resin, acrylic resin, polystyrene, makrolon
Meaning is a kind of.
Specifically, above-mentioned steps（3）In, the mass ratio of string and the thermoplastic resin after granulation is 10-17:40.
Specifically, the mass ratio of thermoplastic resin is 1 after the quality of the addition of above-mentioned additive and granulation:80-100.
Specifically, above-mentioned steps（4）In blend heated temperature be 170-200 DEG C, time of insulation is small for 1.5-2
When, the pressure of shaping is 1.3-1.5MPa.
Technical scheme more than, the beneficial effects of the invention are as follows：
The preparation method of novel furniture composite board provided using the present invention, obtained composite board, not only mechanical property
It is excellent, and almost odorlessness, harm will not be produced to the health of consumer.Wherein, the string that the present invention is provided, fiber
Cellulose content is higher, and gray scale is larger, illustrate its not only have preferable mechanical property, and and resin have higher combination
Intensity.Every mechanical property of composite board can effectively be lifted；The activating solution that the present invention is provided, can effectively improve plant fine
The chemical constitution in dimension table face, improves the bonding interface of fiber and matrix resin, promotes fiber dispersed in matrix resin,
The final mechanical property for improving composite, and the activating solution in the present invention, will not be with the active matter of some in string
Matter chemically reacts, and may be such that the banksia rose retains original fragrance, lifts the quality of composite board；The addition that the present invention is provided
After agent, nano zine oxide, dibutyl sulfide urea synergy, the ultraviolet-resistant capacity of string can be lifted, and it can be effective
Lifting composite board water resistance and heat resistance；, can after silane coupler NXH-132, PTPP synergy
The effective cohesive force strengthened between string and resin material, can effectively prevent plate surface from crackle, stomata etc. occur
Phenomenon, greatly improves the quality of composite board.
Embodiment
Following examples are used for illustrating the present invention, but can not be used for limiting the reality used in the scope of the present invention, embodiment
The condition of applying can be for further adjustments according to the condition of producer, and unaccounted implementation condition is usually conventional laboratory conditions.
Embodiment 1
A kind of preparation method of novel furniture composite board, including following operating procedure：
（1）Will be standby after thermoplastic resin extruding pelletization；
（2）After string is crushed, surface activation process is carried out using activating solution, the string after activation is made, wherein
String is made up of the component of following parts by weight：30 parts of soybean stalk, 6 parts of the banksia rose, 10 parts of PERICARPIUM ARECAE, wherein activating solution by with
The component of lower parts by weight is made：11 parts of methylpropene sodium sulfonate, 9 parts of ethylenediamine base propanesulfonate, 11 parts of chloro-carbonic acid diethylene glycol (DEG) ester,
4 parts of pentylcyclohexyl benzoic acid, 7 parts of ethylene thiourea, 60 parts of absolute ethyl alcohol, 150 parts of water；
（3）String is mixed with the thermoplastic resin after granulation, additive is added thereto, mixture is preheated to 70
DEG C, 30min is incubated, wherein additive is made up of the component of following parts by weight：5 parts of nano zine oxide, 10 parts of dibutyl sulfide urea, silane
11 parts of coupling agent NXH-132,13 parts of PTPP；
（4）Novel furniture composite board is made in mixture heating, compacting after preheating.
Specifically, above-mentioned thermoplastic resin is acrylic resin.
Specifically, above-mentioned steps（3）In, the mass ratio of string and the thermoplastic resin after granulation is 10:40.
Specifically, the mass ratio of thermoplastic resin is 1 after the quality of the addition of above-mentioned additive and granulation:80.
Specifically, above-mentioned steps（4）In blend heated temperature be 170 DEG C, time of insulation is 1.5 hours, shaping
Pressure be 1.3MPa.
Embodiment 2
A kind of preparation method of novel furniture composite board, including following operating procedure：
（1）Will be standby after thermoplastic resin extruding pelletization；
（2）After string is crushed, surface activation process is carried out using activating solution, the string after activation is made, wherein
String is made up of the component of following parts by weight：35 parts of soybean stalk, 7 parts of the banksia rose, 13 parts of PERICARPIUM ARECAE, wherein activating solution by with
The component of lower parts by weight is made：15 parts of methylpropene sodium sulfonate, 11 parts of ethylenediamine base propanesulfonate, chloro-carbonic acid diethylene glycol (DEG) ester 15
Part, 6 parts of pentylcyclohexyl benzoic acid, 10 parts of ethylene thiourea, 70 parts of absolute ethyl alcohol, 170 parts of water；
（3）String is mixed with the thermoplastic resin after granulation, additive is added thereto, mixture is preheated to 75
DEG C, 30min is incubated, wherein additive is made up of the component of following parts by weight：7 parts of nano zine oxide, 13 parts of dibutyl sulfide urea, silane
12 parts of coupling agent NXH-132,15 parts of PTPP；
（4）Novel furniture composite board is made in mixture heating, compacting after preheating.
Specifically, above-mentioned thermoplastic resin is acrylic resin.
Specifically, above-mentioned steps（3）In, the mass ratio of string and the thermoplastic resin after granulation is 13:40.
Specifically, the mass ratio of thermoplastic resin is 1 after the quality of the addition of above-mentioned additive and granulation:90.
Specifically, above-mentioned steps（4）In blend heated temperature be 190 DEG C, time of insulation is 1.7 hours, shaping
Pressure be 1.4MPa.
Embodiment 3
A kind of preparation method of novel furniture composite board, including following operating procedure：
（1）Will be standby after thermoplastic resin extruding pelletization；
（2）After string is crushed, surface activation process is carried out using activating solution, the string after activation is made, wherein
String is made up of the component of following parts by weight：40 parts of soybean stalk, 9 parts of the banksia rose, 15 parts of PERICARPIUM ARECAE, wherein activating solution by with
The component of lower parts by weight is made：18 parts of methylpropene sodium sulfonate, 13 parts of ethylenediamine base propanesulfonate, chloro-carbonic acid diethylene glycol (DEG) ester 16
Part, 8 parts of pentylcyclohexyl benzoic acid, 12 parts of ethylene thiourea, 80 parts of absolute ethyl alcohol, 200 parts of water；
（3）String is mixed with the thermoplastic resin after granulation, additive is added thereto, mixture is preheated to 80
DEG C, 30min is incubated, wherein additive is made up of the component of following parts by weight：8 parts of nano zine oxide, 15 parts of dibutyl sulfide urea, silane
14 parts of coupling agent NXH-132,16 parts of PTPP；
（4）Novel furniture composite board is made in mixture heating, compacting after preheating.
Specifically, above-mentioned thermoplastic resin is polystyrene.
Specifically, above-mentioned steps（3）In, the mass ratio of string and the thermoplastic resin after granulation is 17:40.
Specifically, the mass ratio of thermoplastic resin is 1 after the quality of the addition of above-mentioned additive and granulation:100.
Specifically, above-mentioned steps（4）In blend heated temperature be 200 DEG C, time of insulation is 2 hours, shaping
Pressure is 1.5MPa.
Comparative example 1
Step（2）In activating solution be sodium hydroxide solution that volume fraction is 3%, remaining step is identical with embodiment 1.
Comparative example 2
Step（3）In additive do not contain silane coupler NXH-132, tripolyphosphate potassium composition, remaining step and embodiment 2
It is identical.
Composite board is made with the method for embodiment and comparative example respectively, every Mechanics Performance Testing then is carried out to it,
Test result is as shown in table 1：
Table 1
| Project | Tensile strength（MPa） | Elongation at break（%） | Impact flexibility（KJ/m2） | Have no irritating odor |
| Embodiment 1 | 18.5 | 1.7 | 15.8 | Nothing |
| Comparative example 1 | 14.1 | 1.1 | 12.2 | Slight plastics taste |
| Embodiment 2 | 18.9 | 1.8 | 16.1 | Nothing |
| Comparative example 2 | 9.2 | 0.7 | 10.4 | Nothing |
| Embodiment 3 | 19.1 | 1.8 | 16.2 | Nothing |
As shown in Table 1, novel furniture composite board produced by the present invention, excellent in mechanical performance, and nonirritant smell,
Quality is preferable.
Certainly, described above is not limitation of the present invention, and the present invention is also not limited to the example above, the art
Those of ordinary skill, in the essential scope of the present invention, the change made, changes, addition or replace, should all belong to of the invention
Protection domain.
Claims (5)
1. a kind of preparation method of novel furniture composite board, it is characterised in that including following operating procedure：
（1）Will be standby after thermoplastic resin extruding pelletization；
（2）After string is crushed, surface activation process is carried out using activating solution, the string after activation is made, wherein
String is made up of the component of following parts by weight：30-40 parts of soybean stalk, 6-9 parts of the banksia rose, 10-15 parts of PERICARPIUM ARECAE, wherein living
Change liquid to be made up of the component of following parts by weight：11-18 parts of methylpropene sodium sulfonate, 9-13 parts of ethylenediamine base propanesulfonate, chloromethane
Sour 11-16 parts of diethylene glycol (DEG) ester, 4-8 parts of pentylcyclohexyl benzoic acid, 7-12 parts of ethylene thiourea, 60-80 parts of absolute ethyl alcohol, water 150-
200 parts；
（3）String is mixed with the thermoplastic resin after granulation, additive is added thereto, mixture is preheated to 70-
80 DEG C, 30min is incubated, wherein additive is made up of the component of following parts by weight：5-8 parts of nano zine oxide, dibutyl sulfide urea 10-15
Part, 11-14 parts of silane coupler NXH-132,13-16 parts of PTPP；
（4）Novel furniture composite board is made in mixture heating, compacting after preheating.
2. a kind of preparation method of novel furniture composite board according to claim 1, it is characterised in that above-mentioned heat
Plastic resin is any one in polyvinyl resin, acrylic resin, polystyrene, makrolon.
3. a kind of preparation method of novel furniture composite board according to claim 1, it is characterised in that above-mentioned step
Suddenly（3）In, the mass ratio of string and the thermoplastic resin after granulation is 10-17:40.
4. a kind of preparation method of novel furniture composite board according to claim 1, it is characterised in that additive
The quality of addition and the mass ratio of thermoplastic resin after granulation be 1:80-100.
5. a kind of preparation method of novel furniture composite board according to claim 1, it is characterised in that step
（4）In blend heated temperature be 170-200 DEG C, time of insulation is 1.5-2 hour, and the pressure of shaping is 1.3-
1.5MPa。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710408323.8A CN107216551A (en) | 2017-06-02 | 2017-06-02 | A kind of preparation method of novel furniture composite board |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710408323.8A CN107216551A (en) | 2017-06-02 | 2017-06-02 | A kind of preparation method of novel furniture composite board |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107216551A true CN107216551A (en) | 2017-09-29 |
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ID=59947221
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710408323.8A Pending CN107216551A (en) | 2017-06-02 | 2017-06-02 | A kind of preparation method of novel furniture composite board |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102942797A (en) * | 2012-10-17 | 2013-02-27 | 广西大学 | Plant fiber wood-plastic composite material and preparation method thereof |
-
2017
- 2017-06-02 CN CN201710408323.8A patent/CN107216551A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102942797A (en) * | 2012-10-17 | 2013-02-27 | 广西大学 | Plant fiber wood-plastic composite material and preparation method thereof |
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Application publication date: 20170929 |