CN107200484A - A kind of novel optical fiber corrosion device - Google Patents

A kind of novel optical fiber corrosion device Download PDF

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Publication number
CN107200484A
CN107200484A CN201710411767.7A CN201710411767A CN107200484A CN 107200484 A CN107200484 A CN 107200484A CN 201710411767 A CN201710411767 A CN 201710411767A CN 107200484 A CN107200484 A CN 107200484A
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China
Prior art keywords
support frame
natural rubber
optical fiber
rubber plug
guides pipe
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CN201710411767.7A
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CN107200484B (en
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赵勇
王淑娜
吕日清
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Northeastern University China
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Northeastern University China
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/66Chemical treatment, e.g. leaching, acid or alkali treatment
    • C03C25/68Chemical treatment, e.g. leaching, acid or alkali treatment by etching

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Optical Measuring Cells (AREA)

Abstract

The invention discloses a kind of novel optical fiber corrosion device, including organic glass guide channel, natural rubber plug, reducing fiber guides pipe, support frame, closure and base, lucite groove is fixed on base, both sides notch is blocked with epoxide-resin glue adhesion natural rubber plug, and both sides respectively have a support frame to be fixed on base;The height of support frame is identical with lucite groove, and through hole is provided with support frame, and the hole is overlapped with the natural rubber plug center of circle, and support frame ensures the stability of reducing fiber guides pipe;Natural rubber is inserted with reducing fiber guides pipe beyond the Great Wall, and reducing fiber guides pipe is passed through from support frame through hole, inserts natural rubber plug, and into lucite groove, smooth leads in/out optical fiber.This fiber optical corrosive device overcomes can only threaten the problems such as optical fiber is easily broken after operating personnel's safety, corrosion present in ordinary optic fibre corrosion device from one end corrosion optical fiber, corrosive liquid, simple in construction, easy and safe to operate.

Description

A kind of novel optical fiber corrosion device
Technical field
The invention belongs to fiber optical corrosive technical field, it is related to a kind of novel optical fiber corrosion device.
Background technology
Lightwave signal in optical fiber is easily influenceed by parameters such as the pressure in external environment, temperature, electric field, magnetic fields, in light Fine sensory field, people make use of the change of these extraneous factors to cause optical property (intensity, the frequency of lightwave signal in optical fiber Rate, wavelength, phase etc.) corresponding change, develop various types of fibre optical sensors.Fibre optical sensor and traditional all kinds of biographies Sensor is compared, as follows with optical fiber and the characteristics of optical measurement:(1) optical fiber has good pliability, and small volume, weight Gently.The sensing element much come in every shape can be made up of simple process according to different detection demands;And can be with calculating Machine is connected with fibre system, realizes remote measurement and control.(2) electromagnetism interference is strong, not perishable etc., available for HTHP, corruption The adverse circumstances such as erosion, and human body is not substantially damaged, be conducive to the application in terms of production and living.(3) measurement sensitivity Height, can distributed measurement, transmission capacity is big, and service life is long, and (Tanghai of document 1. jade is based on optical fiber evanescent field for low manufacture cost Refractive index sensing research [D] University of Anhui, 2015.).Evanscent field and week of the optical fiber evanescent field sensor using fibre core surface Environmental interaction is enclosed, the correlation properties of ambient substance are obtained by the energy attenuation to evanescent wave or wave length shift detection.Light Fiber optic evanescent wave sensor can be used for magnetic field detection, and (document 2. Shen Tao, Feng Yue, for sea otter, wait to be based on optical evanescent wave sensor device Magnetic field detection [J] Acta Opticas, 2015,35 (a01):83-88.), biomass detection (Liu Jinhua of document 3., Liu Tao, Meng Increase, wait a kind of based on biologic sensor for fast travelling waves of optical fibre detect Listeria Monocytogenes method foundation [J] in State's Laboratory Diagnosis, 2014 (7):1045-1047.), volatile organic matter detection (document 4. in celery forever, Li Xuejin, Ou Zhilong, Deng volatile organic compound detection devices of the based on optical fiber evanescent field:CN, CN203443888U [P] .2014.) in terms of.In order to Strengthen the interaction of fibre core surface evanscent field and medium, it is necessary to remove part fiber covering to improve transducer sensitivity.Go Except the method for covering mainly has two kinds:Etch and polishing.Etch is referred mainly to using hydrofluoric acid solution by controlling its dense Degree and etching time are so as to produce the sensor fibre of different-diameter, and this method is less demanding to experiment condition, and has into This low, the advantages of gained optical fiber surface is smooth.
Most of fiber optical corrosive method proposed at present can only corrode optical fiber from side, for example, fix optical fiber vertically Corrode (document 5.A.Iadicicco.S, Campopiano, A.Cutolo, et al.Nonuniform in plastic tube thinned fiber Bragg gratings for simultaneous refractive index and temperature measurements[J],IEEE Photonics Technology Letters,2005,17(7): 1495-1497), or by optical fiber one end level it is put into corrosion device that (history of document 6. is big, Fang Qiang, and Qi Liang one kind realizes optical fiber The device of surface smooth taper corrosion, CN 203938601U [P] .2014.).This forms of corrosion can not be met in some cases Corrode being actually needed for a certain section of optical fiber, another aspect hydrofluoric acid has hypertoxic and volatile, in use probably Operating personnel are damaged, the optical fiber after corroding in addition is more crisp, is easily broken, how to keep optical fiber integrality to be also one has To be solved the problem of.
The content of the invention
The device of the present invention improves the shortcomings of the prior art, and there is provided a kind of simple in construction, operation side Just fiber optical corrosive device.
The technical solution adopted by the present invention is:
A kind of novel optical fiber corrosion device, including organic glass guide channel, natural rubber plug, reducing fiber guides pipe, support frame, Closure and base.Lucite groove is fixed on base, and lucite groove both sides notch is with the natural rubber of epoxide-resin glue adhesion Plug is blocked, and lucite groove both sides respectively have a support frame to be fixed on base;The height of support frame and lucite groove phase Together, diameter 1mm through hole is provided with support frame, the hole is overlapped with the natural rubber plug center of circle, support frame ensures reducing optical fiber The stability of guiding tube, makes both sides reducing fiber guides pipe parallel;Natural rubber is inserted with reducing fiber guides pipe, its diameter beyond the Great Wall 0.45mm is tapered to by 4mm, reducing fiber guides pipe is passed through from support frame through hole, natural rubber plug is inserted, into having Machine glass guide channel, smooth leads in/out optical fiber;Reducing fiber guides pipe enters lucite through support frame and natural rubber Groove, closure is covered ensures sealing on lucite groove.
The device of the present invention, lucite sump volume very little is effectively reduced hydrofluoric acid consumption, and adding can prevent after closure Only hydrofluoric acid volatilizees, and reduces operational danger;Natural rubber plug blocks lucite groove notch, it is ensured that insertion reducing optical fiber Corrosive liquid seepage is not had after guiding tube;The reducing processing of fiber guides pipe is conducive to smooth leading in/out optical fiber;It is fixed on Support frame on base can ensure that left and right sides reducing fiber guides pipe is parallel and stably.
Brief description of the drawings
Fig. 1 is a kind of overall schematic of novel optical fiber corrosion device.
Fig. 2 is Fig. 1 top view.
Fig. 3 is Fig. 1 right view.
Fig. 4 is Fig. 1 front view.
Fig. 5 is etching time and fibre diameter graph of a relation.
Embodiment
Describe the specific embodiment of the present invention in detail with reference to technical scheme and accompanying drawing.
As illustrated, a kind of novel optical fiber corrosion device, including organic glass guide channel 1, lucite groove is cuboid, long 20mm, width 5mm, depth 10mm;Lucite groove both sides are respectively equipped with natural rubber plug 4 (by epoxide-resin glue adhesion), natural rubber Plug is a diameter of 11mm, thickness 1mm cylinder;Natural rubber is inserted with reducing fiber guides pipe 3 beyond the Great Wall, and diameter is gradually become by 4mm 0.45mm is carefully arrived, for leading in/out optical fiber;Support frame 2 is provided with the outside of lucite groove, support frame material is lucite, branch Diameter 1mm through hole, the hole and natural rubber plug center of circle weight are provided with support and lucite groove equal height, support frame Close, reducing fiber guides pipe passes through from support frame through hole, insert natural rubber plug, into lucite groove, support frame can be with Ensure the stability of reducing fiber guides pipe, make both sides reducing fiber guides pipe parallel;Lucite groove is provided with closure 5, close It is lucite to cover material, and corrosion is uneven caused by can preventing hydrofluoric acid volatilization, while providing safety guarantee.
The present apparatus is in use, need the part corroded to peel off coat optical fiber, and being introduced by reducing fiber guides pipe has Machine glass guide channel, treating that corrosion area is placed on lucite groove centre position, adds appropriate hydrofluoric acid, covers closure.By one After the section time, you can the smooth thin diameter optical fiber in surface is obtained, by controlling hydrofluoric acid concentration and etching time to produce The sensor fibre of different-diameter.Corrosion reaction suctions out waste liquid after terminating and dealt carefully with, and into lucite groove, repeatedly injection is gone Ionized water cleans optical fiber, draws optical fiber from reducing fiber guides pipe after cleaning.This mode of operation can be prevented effectively from hydrogen fluorine The harm that acid may be caused to operating personnel.
Try out below in example, the optical fiber used is general single mode fiber, cladding diameter 128um, core diameter 8.2um. Corrosion area length 10mm, used hydrofluoric acid concentration is 40%, and constant temperature corrodes under 25 DEG C of environment.Respectively corrosion 15min, 30min, 45min, 60min, 80min, 85min, 90min, the experimental results are shown inthe following table:
By data fitting a straight line in upper table, referring to Fig. 5, fibre diameter can be obtained and change over time formula:
D=-1.275t+128.6.

Claims (4)

1. a kind of novel optical fiber corrosion device, including organic glass guide channel (1), natural rubber plug (4), reducing fiber guides pipe (3), Support frame (2), closure (5) and base (6);Characterized in that, lucite groove (1) is fixed on base (6), lucite Groove (1) both sides notch is blocked with epoxide-resin glue adhesion natural rubber plug (4), and respectively there is a support lucite groove (1) both sides Frame (2) is fixed on base (6);The height of support frame (2) is identical with lucite groove (1), and one is provided with support frame (2) directly Footpath 1mm through hole, the hole is overlapped with natural rubber plug (4) center of circle, and support frame (2) ensures the stability of reducing fiber guides pipe, Make both sides reducing fiber guides pipe parallel;Be inserted with reducing fiber guides pipe (3) on natural rubber plug (4), its diameter by 4mm gradually 0.45mm is tapered to, reducing fiber guides pipe (3) is passed through from support frame (2) through hole, insertion natural rubber plug (4), into having Machine glass guide channel (1), smooth leads in/out optical fiber;Reducing fiber guides pipe (3) is through support frame (2) and natural rubber plug (4) Into lucite groove (1), closure (5) is covered ensures sealing on lucite groove (1).
2. a kind of novel optical fiber corrosion device as claimed in claim 1, it is characterised in that lucite groove (1) is cuboid, Long 20mm, width 5mm, depth 10mm, material corrosion resistance.
3. a kind of novel optical fiber corrosion device as claimed in claim 1, it is characterised in that natural rubber plug (4) is a diameter of 11mm, thickness 1mm cylinder, it is ensured that do not have corrosive liquid seepage after insertion reducing fiber guides pipe.
4. a kind of novel optical fiber corrosion device as claimed in claim 1, it is characterised in that support frame (2) and closure (5) Material is lucite, and corrosion is uneven caused by preventing hydrofluoric acid volatilization, while providing safety guarantee.
CN201710411767.7A 2017-06-05 2017-06-05 Optical fiber corrosion device Expired - Fee Related CN107200484B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111087182A (en) * 2020-01-10 2020-05-01 宁波大学 Chemical corrosion preparation method of chalcogenide glass tapered optical fiber
CN111153609A (en) * 2019-07-10 2020-05-15 深圳瑞焱通光子技术有限公司 Optical fiber corrosion device

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040228591A1 (en) * 2000-12-27 2004-11-18 Kenji Ootsu Method of processing end portions of optical fibers and optical fibers having their end portions processed
CN203688839U (en) * 2013-11-07 2014-07-02 北京工业大学 Thermal stripper for sectionally and partially stripping fiber coating and outer cladding, and cladding light detacher
CN104446008A (en) * 2014-12-08 2015-03-25 山东海富光子科技股份有限公司 Device for achieving smooth and tapered corrosion of surfaces of optical fibers

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040228591A1 (en) * 2000-12-27 2004-11-18 Kenji Ootsu Method of processing end portions of optical fibers and optical fibers having their end portions processed
CN203688839U (en) * 2013-11-07 2014-07-02 北京工业大学 Thermal stripper for sectionally and partially stripping fiber coating and outer cladding, and cladding light detacher
CN104446008A (en) * 2014-12-08 2015-03-25 山东海富光子科技股份有限公司 Device for achieving smooth and tapered corrosion of surfaces of optical fibers

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111153609A (en) * 2019-07-10 2020-05-15 深圳瑞焱通光子技术有限公司 Optical fiber corrosion device
CN111087182A (en) * 2020-01-10 2020-05-01 宁波大学 Chemical corrosion preparation method of chalcogenide glass tapered optical fiber

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