CN107190528A - The instant accelerant of reactive dye and its application process - Google Patents
The instant accelerant of reactive dye and its application process Download PDFInfo
- Publication number
- CN107190528A CN107190528A CN201710591899.2A CN201710591899A CN107190528A CN 107190528 A CN107190528 A CN 107190528A CN 201710591899 A CN201710591899 A CN 201710591899A CN 107190528 A CN107190528 A CN 107190528A
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- Prior art keywords
- parts
- accelerant
- instant
- reactive dye
- minutes
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/5214—Polymers of unsaturated compounds containing no COOH groups or functional derivatives thereof
- D06P1/5242—Polymers of unsaturated N-containing compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Abstract
The invention belongs to weaving face fabric colouring art, more particularly to a kind of instant accelerant of reactive dye and its application process.Include following effective ingredient according to parts by weight：1 part~5 parts of sodium hydroxide；2-3 parts of soda ash；0.5 part of polyvinylpyrrolidone；1 part~5 parts of potassium carbonate；21 part~5 parts of β bases sodium naphthalene sulfonates；1 part~5 parts of sodium gluconate；4 parts~8 parts of potassium sulfate；25 parts~40 parts of sodium chloride；30 parts~60 parts of sodium sulphate.Compared with prior art, advantages and positive effects of the present invention are, the present invention is by providing a kind of reactive dye instant accelerant, utilize rational formula, make that it effectively instead of glauber salt when in use and soda ash is used, reduce inorganic salts addition, addition is the 68-70% of former consumption, while improving product quality, reduces the production time, cost is saved, the benefit of enterprise has been ensured, dye bath pin water inorganic salt content is reduced, has mitigated post processing washing times, and sewage disposal dynamics, suitable large-scale promotion uses.
Description
Technical field
The invention belongs to weaving face fabric colouring art, more particularly to a kind of instant accelerant of reactive dye and its application side
Method.
Background technology
Dyeing catches color, also referred to as paints, and refers to that with chemistry or other method influence materials it in itself
Color.By dyeing object can be made to show desirable a variety of colors, life is decorateeed with colourful.Textile material
Handled with dye bath, dyestuff and fiber is occurred chemically or physically chemical bond, or generate on fiber insoluble coloring matter
Technical process.
At present, in dyeing, cellulose fibre class (staple in bulk, yarn, fabric) dyeing is occupied with reactive dyeing
Many, it needs addition glauber salt, soda ash as dyeing auxiliaries when dyeing, traditional handicraft usage amount is high, and operator's labor intensity is high, and
Glauber salt and soda ash dissolving are slow, the whole time-consuming power consumption of technical process, meanwhile, in operation, it is necessary to feed in batches, technique
Cumbersome, temperature control is bad and batch processed is bad all there may be dyeing defect, aberration, causes the later stage to need to use substantial amounts of nothing
Machine salt treatment, and then production cost is added, it is unfavorable for the growth and development of enterprise.
The content of the invention
The present invention is directed to the above-mentioned technical problem for using glauber salt, soda ash to exist as dyeing auxiliaries in dyeing course,
Propose that a kind of formula reactive dye that reasonable, easy to process, with low cost and dissolution velocity is fast, Color is good are instant and promote dye
Agent.
In order to achieve the above object, the technical solution adopted by the present invention is that the present invention provides a kind of reactive dye instant rush
Stain, includes following effective ingredient according to parts by weight：
Preferably, including following effective ingredient according to parts by weight：
Preferably, including following effective ingredient according to parts by weight：
Present invention also offers the application process of the instant accelerant of above-mentioned reactive dye, including following effective procedure：
A, according to 1: 15 prepare dye bath, reactive dye are added at room temperature, the cellulose base fiber fabric after scouringing and bleaching is put into, run
20 minutes；
B, after after end of run, add the instant accelerant of reactive dye of above-mentioned preparation；
C, heating and temperature control are incubated 10~60 minutes at 30~90 DEG C；
D, after cooling terminates, cool, soap, dry.
Preferably, in the b step, accelerant run time is 15 minutes.
Preferably, in the b step, the accelerant run time of 1/3rd amounts is first put into for after 15 minutes, then throw
The accelerant for entering remaining 2/3rds amount is run 10 minutes.
Compared with prior art, advantages and positive effects of the present invention are,
1st, the present invention, using rational formula, makes it have when in use by providing a kind of reactive dye instant accelerant
Effect instead of glauber salt and soda ash is used, reduce inorganic salts addition, addition is the 68-70% of former consumption, improves production
While quality, the production time is reduced, labor strength is reduced, cost has been saved, the benefit of enterprise has been ensured, together
When, dye bath pin water inorganic salt content is reduced, mitigates post processing washing times, and sewage disposal dynamics, Environmental Safety, is adapted to big
Scale is promoted the use of.
2nd, the present invention efficiently solves heavy metal ion and water-soluble Central Plains by providing a kind of reactive dye instant accelerant
Consumption of the harmful ion of material to dyestuff itself, meanwhile, using the raw material of different densities, when it is dissolved in water, material is difficult
Produce and condense phenomenon.
3rd, the present invention is by providing a kind of reactive dye instant accelerant, dispersiveness in having solved dyestuff existing, flows
The technical problem of dynamic property and level-dyeing property, meanwhile, reduce residual of the dyestuff in casing wall.
Embodiment
In order to be more clearly understood that the above objects, features and advantages of the present invention, with reference to embodiment to this hair
It is bright to be described further.It should be noted that in the case where not conflicting, the feature in embodiments herein and embodiment can
To be mutually combined.
Many details are elaborated in the following description to facilitate a thorough understanding of the present invention, still, the present invention may be used also
To be implemented using other modes described here are different from, therefore, the present invention is not limited to the specific of specification described below
The limitation of embodiment.
Embodiment 1, the present embodiment provides a kind of instant accelerant of reactive dye
It is first according to parts by weight and weighs 1 part of sodium hydroxide, 1 part of potassium carbonate, 1 part of 2- β bases sodium naphthalene sulfonate, sodium gluconate
1 part, 4 parts of potassium sulfate, 25 parts of sodium chloride, 30 parts of sodium sulphate, 2 parts of soda ash, 0.75 part of polyvinylpyrrolidone, be then added to
In ionized water, completely after reaction, the instant accelerant of reactive dye is obtained.
Then, dye bath is prepared according to 1: 15, levelling agent, superfluous mixture are added at room temperature, and (levelling agent, superfluous mixture can be added
Can be without), stirring is run 10 minutes；Then, reactive dye are added at room temperature, are put into the cellulose fibre after scouringing and bleaching
Fabric, after immersion is run 20 minutes, adds the instant accelerant of reactive dye, the addition of the instant accelerant of reactive dye and work
Property dyestuff addition be 1:1, after after 15 minutes, heating up, simultaneously temperature control, at 60 DEG C, is incubated 20 minutes, after cooling terminates, finally,
Cool, soap, dry, by above-mentioned method, in whole dyeing and printing process, the usage amount of inorganic salts is reduced to original addition
The 68% of amount.
Embodiment 2, the present embodiment provides a kind of instant accelerant of reactive dye
It is first according to parts by weight and weighs 5 parts of sodium hydroxide；5 parts of potassium carbonate；5 parts of 2- β bases sodium naphthalene sulfonate；Sodium gluconate
5 parts；8 parts of potassium sulfate；40 parts of sodium chloride；60 parts of sodium sulphate；2 parts of soda ash；0.75 part of polyvinylpyrrolidone, is then added to
In ionized water, completely after reaction, the instant accelerant of reactive dye is obtained.
Then, dye bath is prepared according to 1: 15, reactive dye is added at room temperature, the cellulose fibre after scouringing and bleaching is put into and knits
Thing, after immersion is run 20 minutes, adds the instant accelerant of reactive dye of 1/3rd amounts, after 15 minutes, then puts into remaining
2/3rds amounts accelerant run 10 minutes, the addition of the instant accelerant of reactive dye and the ratio of reactive dye are
10:1, after after 15 minutes, heating up, simultaneously temperature control, at 60 DEG C, is incubated 60 minutes, after cooling terminates, finally, cools, soaps, dries
, by above-mentioned method, in whole dyeing and printing process, the usage amount of inorganic salts is reduced to the 70% of original addition,.
Embodiment 3, the present embodiment provides a kind of instant accelerant of reactive dye
It is first according to parts by weight and weighs 2.5 parts of sodium hydroxide, 3 parts of potassium carbonate, 2 parts of soda ash, polyvinylpyrrolidone
0.75 part, 1 part of 2- β bases sodium naphthalene sulfonate, 2 parts of sodium gluconate, 5 parts of potassium sulfate, 36.5 parts of sodium chloride, 50 parts of sodium sulphate, then
It is added in deionized water, completely after reaction, obtains the instant accelerant of reactive dye.
Then, dye bath is prepared according to 1: 15, levelling agent, superfluous mixture is added at room temperature, stirring is run 10 minutes；Then, exist
Reactive dye are added at room temperature, are put into the cellulose base fiber fabric after scouringing and bleaching, after immersion is run 20 minutes, are added reactive dye
Instant accelerant, the addition of the instant accelerant of reactive dye, the ratio with reactive dye is 5:1, after after 15 minutes, heat up
And temperature control is at 30 DEG C, 60 minutes are incubated, after cooling terminates, finally, cools, soap, dry, by above-mentioned method,
In whole dyeing and printing process, the usage amount of inorganic salts is reduced to the 68% of original addition.
Embodiment 4, the present embodiment provides a kind of instant accelerant of reactive dye
It is first according to parts by weight and weighs 3 parts of sodium hydroxide, 4 parts of potassium carbonate, 2 parts of 2- β bases sodium naphthalene sulfonate, sodium gluconate
3 parts, 5 parts of potassium sulfate, 36.5 parts of sodium chloride, 50 parts of sodium sulphate, be then added in deionized water, completely reaction after, lived
The property instant accelerant of dyestuff.
Then, dye bath is prepared according to 1: 15, levelling agent, superfluous mixture is added at room temperature, stirring is run 10 minutes；Then, exist
Reactive dye are added at room temperature, are put into the cellulose base fiber fabric after scouringing and bleaching, after immersion is run 20 minutes, are added 1/3rd
Measure the instant accelerant of reactive dye to run 15 minutes, reheat remaining 2/3rds instant accelerant of reactive dye, activity
The addition of the instant accelerant of dyestuff and the addition of reactive dye are 16:1, after after 10 minutes, heating up, simultaneously temperature control, at 90 DEG C, is protected
Temperature 10 minutes, after cooling terminates, finally, cools, soaps, dries, by above-mentioned method, in whole dyeing and printing process,
The usage amount of inorganic salts is reduced to the 70% of original addition.
By adding the instant accelerant of reactive dye in batches, be conducive to further reducing the usage amount of inorganic salts,
Substantial amounts of resource has been saved, the performance of enterprises is improved, meanwhile, the use of glauber salt and soda ash that the present invention is avoided reduces ring
Border is polluted, safety and environmental protection.
The above described is only a preferred embodiment of the present invention, being not the limitation for making other forms to the present invention, appoint
What those skilled in the art changed or be modified as possibly also with the technology contents of the disclosure above equivalent variations etc.
Imitate embodiment and be applied to other fields, but every without departing from technical solution of the present invention content, the technical spirit according to the present invention
Any simple modification, equivalent variations and the remodeling made to above example, still fall within the protection domain of technical solution of the present invention.
Claims (6)
1. a kind of instant accelerant of reactive dye, it is characterised in that include following effective ingredient according to parts by weight：
2. the instant accelerant of reactive dye according to claim 1, it is characterised in that have according to parts by weight including following
Imitate composition：
3. the instant accelerant of reactive dye according to claim 2, it is characterised in that have according to parts by weight including following
Imitate composition：
4. the application process of the instant accelerant of reactive dye described in aforesaid right 1~3, it is characterised in that including following effective
Step：
A, according to 1: 5~15 prepare dye baths, reactive dye are added at room temperature, the cellulose base fiber fabric after scouringing and bleaching is put into, run
20 minutes；
B, after after end of run, add the instant accelerant of reactive dye prepared by any one of claims 1 to 3；
C, heating and temperature control are incubated 10~60 minutes at 30~90 DEG C；
D, after cooling terminates, cool, soap, dry.
5. the application process of the instant accelerant of reactive dye according to claim 4, it is characterised in that in the b step,
Accelerant run time is 15 minutes.
6. the application process of the instant accelerant of reactive dye according to claim 4, it is characterised in that in the b step,
First input 1/3rd amounts accelerant run time be 15 minutes after, then put into remaining 2/3rds amount accelerant run
10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710591899.2A CN107190528A (en) | 2017-07-19 | 2017-07-19 | The instant accelerant of reactive dye and its application process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710591899.2A CN107190528A (en) | 2017-07-19 | 2017-07-19 | The instant accelerant of reactive dye and its application process |
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| Publication Number | Publication Date |
|---|---|
| CN107190528A true CN107190528A (en) | 2017-09-22 |
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| CN201710591899.2A Pending CN107190528A (en) | 2017-07-19 | 2017-07-19 | The instant accelerant of reactive dye and its application process |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110644267A (en) * | 2019-09-18 | 2020-01-03 | 五邑大学 | Non-phosphorus liquid substitute alkali and preparation method thereof |
| CN114573999A (en) * | 2022-04-06 | 2022-06-03 | 浙江亿得新材料股份有限公司 | Compounding method of reactive dye red suitable for dyeing composite cellulose fibers, and product and application thereof |
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| CN101974819A (en) * | 2010-09-30 | 2011-02-16 | 福建众和股份有限公司 | Pretreatment, dyeing and finishing process of pepper fiber woven fabric |
| CN102899929A (en) * | 2012-10-30 | 2013-01-30 | 东华大学 | Processing method of salt-free dyeing through activated dye |
| CN102926235A (en) * | 2012-11-08 | 2013-02-13 | 绍兴文理学院 | Liquid mixed base for activated dye high temperature dyeing and preparation method and application thereof |
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2017
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Patent Citations (5)
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| CN101806002A (en) * | 2010-03-03 | 2010-08-18 | 广东德美精细化工股份有限公司 | Accelerating agent for reactive dyeing, and preparation method and applications thereof |
| CN101974819A (en) * | 2010-09-30 | 2011-02-16 | 福建众和股份有限公司 | Pretreatment, dyeing and finishing process of pepper fiber woven fabric |
| CN102899929A (en) * | 2012-10-30 | 2013-01-30 | 东华大学 | Processing method of salt-free dyeing through activated dye |
| CN102926234A (en) * | 2012-11-05 | 2013-02-13 | 绍兴文理学院 | Activated dye accelerating agent and dyeing method |
| CN102926235A (en) * | 2012-11-08 | 2013-02-13 | 绍兴文理学院 | Liquid mixed base for activated dye high temperature dyeing and preparation method and application thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110644267A (en) * | 2019-09-18 | 2020-01-03 | 五邑大学 | Non-phosphorus liquid substitute alkali and preparation method thereof |
| CN114573999A (en) * | 2022-04-06 | 2022-06-03 | 浙江亿得新材料股份有限公司 | Compounding method of reactive dye red suitable for dyeing composite cellulose fibers, and product and application thereof |
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