CN107190522A - 一种用于清粪带的抗菌除臭用涂层布的制备方法 - Google Patents

一种用于清粪带的抗菌除臭用涂层布的制备方法 Download PDF

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CN107190522A
CN107190522A CN201710607043.XA CN201710607043A CN107190522A CN 107190522 A CN107190522 A CN 107190522A CN 201710607043 A CN201710607043 A CN 201710607043A CN 107190522 A CN107190522 A CN 107190522A
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王旭
吴文中
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ANHUI PLATO COATED FABRICS Co Ltd
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Abstract

本发明公开了一种用于清粪带的抗菌除臭用涂层布的制备方法，本发明分别采用底层浆料以及面层浆料分别在机织布表面进行涂刷，得到外表面两层，内表面一层的涂层布，且采用异辛酸铋作为稳定剂的PVC糊树脂作为底层浆料，热稳定性好；采用纯丙乳液作为面层浆料，结实耐磨，同时添加了由生物基材刨花等干馏、冷凝、一定温度下进行蒸馏精制得到的抗菌除臭剂，由于抗菌除臭剂中含有较多的有机酸、酚类以及其他生物活性组分，协同作用抑菌效果显著，能够维持涂层布的抗菌性能，可以用于禽养殖场的清粪带面料，结实耐用，与现有清粪带相比，产品底面为一层涂层，厚度较薄，提高了摩擦系数，有利于传送带的运行。

Description

一种用于清粪带的抗菌除臭用涂层布的制备方法
技术领域
本发明涉及涂层布技术领域，尤其涉及一种用于清粪带的抗菌除臭用涂层布的制备方法。
背景技术
现代养殖企业中多采用传送带式清粪机首要由电机加速设施，链传动，主、自愿辊，承粪带等组成，实用于叠层式笼养禽舍，其中传送式清粪机主要包括清粪带，间接把禽粪保送到笼舍外的清粪车上，缩小环境净化，主动化水平高，升高工人休息强度，运转平安，一直牵引绳，应用寿命长，而且采用清粪带的方式能够保持禽粪的干燥性，容易处理以及再利用。市场上大多数的清粪带采用聚丙烯、聚乙烯等制成，强度、韧性具有一定的劣势，且不具有良好的抗菌除臭性能。机织布具有布面光洁、纹路清晰、质地细密、手感滑爽，纵、横向具有较好的延伸性的特点，且面料透气性好，将此布作为基布，在基布正反面涂覆适量的涂层，尤其是具有抗菌除臭功效的涂层，可以满足清粪带的抗菌除臭需求。
发明内容
本发明目的就是为了弥补已有技术的缺陷，提供一种用于清粪带的抗菌除臭用涂层布的制备方法。
本发明是通过以下技术方案实现的：
一种用于清粪带的抗菌除臭用涂层布的制备方法，包括以下具体步骤：
（1）将一定规格的白色机织布作为基布，将粘度为6000CP左右的底层浆料采用立式涂刷的方式均匀的涂覆在基布的两面，控制涂刷层的厚度为0.38-0.4mm，确保涂层完全盖住布面，然后将其送入立涂烘箱中，升温至140-145℃干燥10-15分钟，再继续升温至155-160℃燥5-7分钟，得到一次干燥涂层布；
（2）将粘度为8000CP左右的面层浆料均匀的涂刷在上述一次烘干涂层布表面，控制涂层厚度为0.46-0.5mm，置于面涂烘箱内进行干燥，升温至170-180℃，控制车速15-17m/min，干燥2-3分钟即得。
一种用于清粪带的抗菌除臭用涂层布的制备方法，步骤（1）中所述的白色机织布的规格为1000D*1000D/20*22。
一种用于清粪带的抗菌除臭用涂层布的制备方法，步骤（1）所述的底层浆料与步骤（2）所述的面层浆料均含有适量的抗菌除臭液，具体制备方法如下：将木材加工残余物刨花等进行粉碎，过200目筛，放入烘箱中以100-110℃完全烘干后放入干馏炉进行干馏，控制炉温500-600℃，反应4-5小时后，得到粗干馏气，然后冷凝回流，将得到的回流废液静置，上层为木醋液，最后将木醋液进行蒸馏精制，控制蒸馏温度97-99℃，得到产率为20-22%的抗菌除臭液。
一种用于清粪带的抗菌除臭用涂层布的制备方法，步骤（1）所述的底层浆料的成分配比为：PVC糊树脂100-110、增塑剂70-75、异辛酸铋3-4，碳酸钙50-55，抗菌除臭剂8-10；步骤（2）所述的面层浆料的成分配比：纯丙乳液100-110，橘红色颜料10-12、增塑剂60-65、抗氧剂2-3、碳酸钙25-28、抗菌除臭剂10-12。
一种用于清粪带的抗菌除臭用涂层布的制备方法，所述的增塑剂是指环氧硬脂酸丁酯、环氧硬脂酸辛酯、邻苯二甲酸二辛酯中的一种或几种；所述的抗氧剂是指二丁基羟基甲苯、没食子酸丙酯中的一种。
本发明的优点是：本发明分别采用底层浆料以及面层浆料分别在机织布表面进行涂刷，得到外表面两层，内表面一层的涂层布，且采用异辛酸铋作为稳定剂的PVC糊树脂作为底层浆料，异辛酸铋通过置换PVC中不稳定的氯原子，维持PVC树脂涂层的热稳定性，同时由于异辛酸铋具有金属原子空轨道，进一步吸收PVC释放出的氯化氢气体达到提高热稳定性的效果；采用纯丙乳液作为面层浆料，结实耐磨，同时添加了由生物基材刨花等干馏、冷凝、一定温度下进行蒸馏精制得到的抗菌除臭剂，由于抗菌除臭剂中含有较多的有机酸、酚类以及其他生物活性组分，协同作用抑菌效果显著，能够维持涂层布的抗菌性能，可以用于禽养殖场的清粪带面料，结实耐用，与现有清粪带相比，产品底面为一层涂层，厚度较薄，提高了摩擦系数，有利于传送带的运行。本发明结实耐用，抗菌除臭，采用废弃生物制造除臭剂，提高了产品附加价值的同时降低了生产成本，适合各种养殖场的清粪带。
具体实施方式
一种用于清粪带的抗菌除臭用涂层布的制备方法，包括以下具体步骤：
（1）将一定规格的白色机织布作为基布，将粘度为6000CP左右的底层浆料采用立式涂刷的方式均匀的涂覆在基布的两面，控制涂刷层的厚度为0.38mm，确保涂层完全盖住布面，然后将其送入立涂烘箱中，升温至140℃干燥10分钟，再继续升温至155℃燥5分钟，得到一次干燥涂层布；
（2）将粘度为8000CP左右的面层浆料均匀的涂刷在上述一次烘干涂层布表面，控制涂层厚度为0.46mm，置于面涂烘箱内进行干燥，升温至170℃，控制车速15m/min，干燥2分钟即得。
一种用于清粪带的抗菌除臭用涂层布的制备方法，步骤（1）中所述的白色机织布的规格为1000D*1000D/20*22。
一种用于清粪带的抗菌除臭用涂层布的制备方法，步骤（1）所述的底层浆料与步骤（2）所述的面层浆料均含有适量的抗菌除臭液，具体制备方法如下：将木材加工残余物刨花等进行粉碎，过200目筛，放入烘箱中以100℃完全烘干后放入干馏炉进行干馏，控制炉温500℃，反应4小时后，得到粗干馏气，然后冷凝回流，将得到的回流废液静置，上层为木醋液，最后将木醋液进行蒸馏精制，控制蒸馏温度97℃，得到产率为20.3%的抗菌除臭液。
一种用于清粪带的抗菌除臭用涂层布的制备方法，步骤（1）所述的底层浆料的成分配比为：PVC糊树脂100、环氧硬脂酸丁酯70、异辛酸铋3，碳酸钙50，抗菌除臭剂8；步骤（2）所述的面层浆料的成分配比：纯丙乳液100，橘红色颜料10、环氧硬脂酸辛酯60、没食子酸丙酯2、碳酸钙25、抗菌除臭剂10。

Claims (5)

1.一种用于清粪带的抗菌除臭用涂层布的制备方法，其特征在于，包括以下具体步骤：
（1）将一定规格的白色机织布作为基布，将粘度为6000CP左右的底层浆料采用立式涂刷的方式均匀的涂覆在基布的两面，控制涂刷层的厚度为0.38-0.4mm，确保涂层完全盖住布面，然后将其送入立涂烘箱中，升温至140-145℃干燥10-15分钟，再继续升温至155-160℃燥5-7分钟，得到一次干燥涂层布；
（2）将粘度为8000CP左右的面层浆料均匀的涂刷在上述一次烘干涂层布表面，控制涂层厚度为0.46-0.5mm，置于面涂烘箱内进行干燥，升温至170-180℃，控制车速15-17m/min，干燥2-3分钟即得。
2.根据权利要求1所述的一种用于清粪带的抗菌除臭用涂层布的制备方法，其特征在于，步骤（1）中所述的白色机织布的规格为1000D*1000D/20*22。
3.根据权利要求1所述的一种用于清粪带的抗菌除臭用涂层布的制备方法，其特征在于，步骤（1）所述的底层浆料与步骤（2）所述的面层浆料均含有适量的抗菌除臭液，具体制备方法如下：将木材加工残余物刨花等进行粉碎，过200目筛，放入烘箱中以100-110℃完全烘干后放入干馏炉进行干馏，控制炉温500-600℃，反应4-5小时后，得到粗干馏气，然后冷凝回流，将得到的回流废液静置，上层为木醋液，最后将木醋液进行蒸馏精制，控制蒸馏温度97-99℃，得到产率为20-22%的抗菌除臭液。
4.根据权利要求1所述的一种用于清粪带的抗菌除臭用涂层布的制备方法，其特征在于，步骤（1）所述的底层浆料的成分配比为：PVC糊树脂100-110、增塑剂70-75、异辛酸铋3-4，碳酸钙50-55，抗菌除臭剂8-10；步骤（2）所述的面层浆料的成分配比：纯丙乳液100-110，橘红色颜料10-12、增塑剂60-65、抗氧剂2-3、碳酸钙25-28、抗菌除臭剂10-12。
5.根据权利要求4所述的一种用于清粪带的抗菌除臭用涂层布的制备方法，其特征在于，所述的增塑剂是指环氧硬脂酸丁酯、环氧硬脂酸辛酯、邻苯二甲酸二辛酯中的一种或几种；所述的抗氧剂是指二丁基羟基甲苯、没食子酸丙酯中的一种。
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