CN107189687A - A kind of modulator approach of plant paint tree milk liquid composite coating - Google Patents

A kind of modulator approach of plant paint tree milk liquid composite coating Download PDF

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Publication number
CN107189687A
CN107189687A CN201710444820.3A CN201710444820A CN107189687A CN 107189687 A CN107189687 A CN 107189687A CN 201710444820 A CN201710444820 A CN 201710444820A CN 107189687 A CN107189687 A CN 107189687A
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pretreatment
lacquer
emulsion
tree
parts
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吴昊
洪克俭
王磊
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HUBEI BAOSHIHUA CRAFTWORK CO Ltd
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HUBEI BAOSHIHUA CRAFTWORK CO Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D193/00Coating compositions based on natural resins; Coating compositions based on derivatives thereof
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/005Drying oils
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The present invention relates to a kind of blacking preparation method based on natural raw lacquer.There is provided a kind of plant paint tree milk liquid compound modulator approach.The pretreatment of lacquer tree emulsion:Raw lacquer is filtered into impurity elimination, is 14 20 revs/min of lower stirring at normal temperature in rotating speed in input oxidation polymerization machine, until lacquer tree emulsion moisture is 5 6%, as can be untill the ㎝ newton bodies of wire drawing 6 10;The pretreatment of vegetable oil:The linseed oil of the double drifts of 40 parts of processes is mixed into input with 60 points of tung oil to polymerize in pot, 245 DEG C are heated to, 4 parts of rosin powder of input, which are together stirred, to be boiled, and is discharged fume simultaneously.When rosin melts completely, be warming up to 275 DEG C, kept for 18 25 minutes, detect viscosity, when vegetable oil turn into can the ㎝ newton body of wire drawing 6 10 can take the dish out of the pot, and stir exhausting smoke evacuation and be cooled to normal temperature.Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input kneader than mediating 23 hours.

Description

A kind of modulator approach of plant paint tree milk liquid composite coating
Technical field
The present invention relates to a kind of modulator approach of plant paint tree milk liquid composite coating.
Background technology
Raw lacquer (Raw laequer) refers to the bast scarfing outflow from lacquer tree (Rhus verniciflua Stokes) Milky white emulsion body.Main component include laccol (60-70%), colloid (5-7%), water-insoluble glycoprotein (- 1%), Rhus Laccase (- 0.24%) and moisture content (20-25%) etc..When connect melt air after, its color and luster because of oxidation from the superficial to the deep, in proper order Dark brown is faded to, a kind of hard paint film is eventually become.Raw lacquer paint film is hard bright, wear-resisting, heat-resisting, corrosion-resistant.It is a kind of Natural paint, in China using existing more than 7000 years usage history, there is the appellation of coating " first ancestor ", politics, warp to China Help, culture life once produced material impact, was the great discovery after four inventions.Use for convenience, improve its decoration Performance and other physics and chemistry combination properties, people take all multi-methods to be modified, compound that many raw lacquer coatings have been made.
A kind of natural emulsion of get off is tapped from lacquer tree to be needed to be modified modulation according to technological requirement and could use. Due to the influence of the factors such as seeds, the place of production, the mode of production, storage time, the poor quality opposite sex is fairly obvious.In lacquer tree emulsion Main film forming substance laccol is the mixture that catechol base is constituted with aliphatic chain, includes saturation laccol, monoene laccol, two Alkene laccol, triolefin laccol etc., also, the ratio that these laccols can be shared in laccol total amount due to the difference in seeds and the place of production Example and chemical constitution are also differed, and complicated composition brings certain difficulty to the modulation modification of lacquer tree emulsion..
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of modulator approach of plant paint tree milk liquid composite coating.
The technical scheme is that:A kind of modulator approach of plant paint tree milk liquid composite coating, it is characterised in that plus Work method comprises the following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 13-20 revs/min of lower stirring at normal temperature in rotating speed, directly It is 5-6% to raw lacquer moisture, as can be untill wire drawing 6-10 ㎝ newton bodies;
(b) pretreatment of vegetable oil:
The 40-50 portions of linseed oil by double drifts are polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 3-4 Part rosin powder, which is together stirred, to be boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 points Clock, detect viscosity, when linseed oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input kneader than mediating 2-3 hours As plant paint tree milk liquid composite coating.
A kind of modulator approach of plant paint tree milk liquid composite coating of the present invention, it is characterised in that processing method is included such as Lower step:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 13-15 revs/min of lower stirring at normal temperature in rotating speed, directly It is 5-6% to moisture, as can be untill wire drawing 6-10 ㎝ newton bodies;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 4 parts of rosin Powder is together stirred and boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minutes, inspection Viscosimetric, when linseed oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input vacuum kneader than mediating 2-3 Hour is plant paint tree milk liquid composite coating.
It is as follows that a kind of modulator approach of plant paint tree milk liquid composite coating of the present invention is characterized in that processing method includes Step:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 14-20 revs/min of lower stirring at normal temperature in rotating speed, directly It is 5-6% to raw lacquer moisture, raw lacquer liquid turns into can be untill wire drawing 6-10 ㎝ newton bodies;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 40 parts of processes is mixed into input with 60 parts of tung oil to polymerize in pot, 245 DEG C is heated to, puts into 4 parts Rosin powder, which is together stirred, to be boiled, and opens air exhauster smoke evacuation.When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minutes, Detect viscosity, when vegetable oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature.
(c) mediate
Vegetable oil by pretreatment is pressed 50 with lacquer tree emulsion:50 weight in input kneader than mediating 2-3 hours As transparent raw lacquer coating.
A kind of modulator approach of plant paint tree milk liquid composite coating of the present invention, signified natural raw lacquer refers to from lacquer tree The emulsion got off is tapped on (Rhus verniciflur stokes), it includes raw lacquer, Vietnam's raw lacquer, Laos's life Paint, Thailand's raw lacquer, Japanese raw lacquer etc..
A kind of beneficial effect of the modulator approach of plant paint tree milk liquid composite coating of the present invention is due to using new work Skill, wherein without the metal ion drier such as organic solvent and manganese, lead, mercury, zirconium, so that it is high-quality to provide a kind of environmental protection Plant paint tree milk liquid composite coating modulator approach.
The modulator approach for the plant paint tree milk liquid composite coating that the present invention is provided is the special oil for lacquer tree emulsion What bag water-bound was carried out.Main film forming substance laccol in lacquer tree emulsion is that catechol base is constituted from different aliphatic chain bases Mixture, includes saturation laccol, monoene laccol, diene laccol, triolefin laccol etc., also, these laccols can due to seeds and The difference in the place of production and ratio and chemical constitution shared in laccol total amount is also differed.In addition, in lacquer tree emulsion also Containing laccase, moisture, gumminess, oil content etc., these compositions also due to seeds, the place of production, storage, the difference of the mode of production, Their relative scales in system can also change.This technology by control laccol polymerize molecular weight and moisture, The Abietyl modified linseed oil of addition, tung oil, are aided with kneading, obtain plant paint tree milk liquid composite coating and modulator approach.
The plant paint tree milk liquid composite coating provided using the present invention is detected according to national standard;
1st, the reset condition of plant paint tree milk liquid composite coating;
Table 1
2nd, plant paint tree milk liquid composite coating paint film property;
Table 2
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely retouched State, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the present invention In embodiment, the every other implementation that those of ordinary skill in the art are obtained under the premise of creative work is not made Example, belongs to the scope of protection of the invention.
Embodiment 1:A kind of modulator approach of plant paint tree milk liquid composite coating, in the following manner:1st, lacquer tree emulsion Pretreatment:By the manly big wooden lacquer tree emulsion filtering impurity elimination of water content 25%, put into oxidation polymerization machine, be 14- in rotating speed 20 revs/min of lower stirring at normal temperature, until raw lacquer moisture is 5-6%, raw lacquer liquid turns into can be untill wire drawing 6-10 ㎝ newton bodies; 2nd, the pretreatment of vegetable oil:The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C, throwing are heated to Enter 4 parts of rosin powder and together stir to boil, open air exhauster smoke evacuation.When rosin melts completely, 275 DEG C are warming up to, 18- is kept 25 minutes, detect viscosity, when linseed oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to Normal temperature.3rd, the raw lacquer and linseed oil by pretreatment are pressed 50:Mediated in 50 weight ratio input kneader and 2-3 hours be Can.
Embodiment 2:A kind of modulator approach of plant paint tree milk liquid composite coating, 1, the pretreatment of lacquer tree emulsion:It will contain The Shaanxi clovershrub lacquer tree emulsion of manly big wooden the lacquer tree emulsion and water content 30% of water 25% presses 1:1 weight is than mixing (average moisture content 27.5%) is filtered in impurity elimination, input oxidation polymerization machine, is 14-20 revs/min of lower stirring at normal temperature in rotating speed, directly It is 5-6% to raw lacquer moisture, as can be untill wire drawing 6-10 ㎝ newton bodies;2nd, the pretreatment of vegetable oil:By 40 parts of processes The linseed oil of double drifts polymerize in pot with 60 parts of tung oil inputs, is heated to 245 DEG C, and 4 parts of rosin powder of input, which are together stirred, to be boiled, Open air exhauster smoke evacuation.When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minute, detection viscosity, as can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature.3rd, by the lacquer tree emulsion by pretreatment and plant Oil presses 50:50 weight in input kneader than mediating 2-3 hours.
Embodiment 3:A kind of modulator approach of plant paint tree milk liquid composite coating, in the following manner:1st, raw lacquer is pre- Processing:The early lacquer tree emulsion in Guizhou the west of Guizhou Province of manly big wooden the lacquer tree emulsion and water content 32% of water content 25% is pressed 1:1 weight Amount is put into oxidation polymerization machine than mixing (average moisture content 28.5%) filtering impurity elimination, is 14-20 revs/min of lower normal temperature in rotating speed Stirring, until moisture is 5-6%, as can be untill wire drawing 6-10 ㎝ newton bodies;2nd, the pretreatment of vegetable oil:By 40 parts Linseed oil by double drifts polymerize in pot with 60 parts of tung oil inputs, is heated to 245 DEG C, and 4 parts of rosin powder of input, which are together stirred, to be endured System, opens air exhauster smoke evacuation.When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minutes, viscosity is detected, works as linseed oil As can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature.3rd, by the paint by pretreatment Tree milk liquid and vegetable oil press 50:50 weight in input kneader than mediating 2-3 hours.
Embodiment 4:A kind of modulator approach of plant paint tree milk liquid composite coating, in the following manner:1st, lacquer tree emulsion Pretreatment:By the early lacquer tree emulsion filtering impurity elimination in Guizhou the west of Guizhou Province of water content 32%, put into oxidation polymerization machine, be in rotating speed 13-15 revs/min of lower stirring at normal temperature, until moisture is 5-6%, raw lacquer liquid turns into can be untill wire drawing 6-10 ㎝ newton bodies;2、 The pretreatment of vegetable oil:The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C, input are heated to 4 parts of rosin powder are together stirred and boiled, and open air exhauster smoke evacuation.When rosin melts completely, 275 DEG C are warming up to, 18-25 is kept Minute, detect viscosity, when vegetable oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to often Temperature.3rd, the lacquer tree emulsion and vegetable oil by pretreatment are pressed 50:Mediated in 50 weight ratio input kneader and 2-3 hours be Can.
Embodiment 5:A kind of modulator approach of plant paint tree milk liquid composite coating, in the following manner:1st, lacquer tree emulsion Pretreatment:By the Shaanxi clovershrub lacquer tree emulsion filtering impurity elimination of water content 30%, put into oxidation polymerization machine, be in rotating speed 14-20 revs/min of lower stirring at normal temperature, until moisture is 5-6%, as can be untill wire drawing 6-10 ㎝ newton bodies;2nd, vegetable oil Pretreatment:The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 4 portions of pines Together stirring is boiled at face powder end, opens air exhauster smoke evacuation.When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minutes, Detect viscosity, when vegetable oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature.3、 Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input kneader than mediating 2-3 hours.
Embodiment 6:A kind of modulator approach of plant paint tree milk liquid composite coating, in the following manner:1st, lacquer tree emulsion Pretreatment:By the manly big wooden lacquer tree emulsion of water content 25%, 30%, 32%, 22%, Shaanxi clovershrub lacquer tree emulsion, expensive State the west of Guizhou Province morning lacquer tree emulsion, Vietnam's lacquer tree emulsion press 1:1:1:1 weight filters impurity elimination than mixing (average moisture content 27.3%), Put into oxidation polymerization machine, be 14-20 revs/min of lower stirring at normal temperature in rotating speed, until moisture is 5-6%, as can wire drawing Untill 6-10 ㎝ newton bodies;2nd, the pretreatment of vegetable oil:The linseed oil of the double drifts of 40 parts of processes is polymerize pot with 60 parts of tung oil inputs It is interior, 245 DEG C are heated to, 4 parts of rosin powder of input, which are together stirred, to be boiled, and opens air exhauster smoke evacuation.When rosin melts completely, rise Temperature to 275 DEG C, keep 18-25 minute, detect viscosity, when vegetable oil as can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and Stirring exhausting smoke evacuation is cooled to normal temperature.3rd, the lacquer tree emulsion and vegetable oil by pretreatment are pressed 50:50 weight is pinched than input Mediated 2-3 hours in conjunction machine.
Embodiment 7:A kind of modulator approach of plant paint tree milk liquid composite coating, by foregoing six with institute in example The plant paint tree milk liquid composite coating of acquisition is detected according to national standard to its reset condition respectively, then again will It is coated on woodenware and pottery object according to coating application operational procedure, and its testing result is as follows:
Plant paint tree milk liquid composite coating reset condition testing result:Table 3
Plant paint tree milk liquid composite coating paint film property testing result:Table 4
Show that indices are substantially close from above-mentioned 6 with the Indexs measure result of example, this technology has fine Repeatability.
Embodiment 8:A kind of modulator approach of plant paint tree milk liquid composite coating, processing method comprises the following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 13 revs/min of lower stirring at normal temperature in rotating speed, until raw It is 5% to paint moisture, as can be untill the ㎝ newton bodies of wire drawing 6;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 3 parts of rosin Powder is together stirred and boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 18 minutes, detection is viscous Degree, when linseed oil turn into can the ㎝ newton body of wire drawing 6 can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input kneader than mediating 2 hours i.e. For plant paint tree milk liquid composite coating.
Embodiment 9:A kind of modulator approach of plant paint tree milk liquid composite coating, processing method comprises the following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 20 revs/min of lower stirring at normal temperature in rotating speed, until raw It is 6% to paint moisture, as can be untill the ㎝ newton bodies of wire drawing 10;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 50 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 4 parts of rosin Powder is together stirred and boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 25 minutes, detection is viscous Degree, when linseed oil turn into can the ㎝ newton body of wire drawing 10 can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input kneader than mediating 3 hours i.e. For plant paint tree milk liquid composite coating.
Embodiment 10:A kind of modulator approach of plant paint tree milk liquid composite coating, processing method comprises the following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 17 revs/min of lower stirring at normal temperature in rotating speed, until raw It is 5.5% to paint moisture, as can be untill the ㎝ newton bodies of wire drawing 8;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 45 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 3.5 portions of pines Together stirring is boiled at face powder end, opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 22 minutes, detection Viscosity, when linseed oil turn into can the ㎝ newton body of wire drawing 8 can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input kneader than mediating 2.5 hours As plant paint tree milk liquid composite coating.
Embodiment 11:A kind of modulator approach of plant paint tree milk liquid composite coating, processing method comprises the following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 13-15 revs/min of lower stirring at normal temperature in rotating speed, directly It is 5.5% to moisture, as can be untill the ㎝ newton bodies of wire drawing 7;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 4 parts of rosin Powder is together stirred and boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 21 minutes, detection is viscous Degree, when linseed oil turn into can the ㎝ newton body of wire drawing 7 can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight is smaller than mediating 3 in input vacuum kneader When be plant paint tree milk liquid composite coating.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (2)

1. a kind of modulator approach of plant paint tree milk liquid composite coating, it is characterised in that processing method comprises the following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 13-20 revs/min of lower stirring at normal temperature in rotating speed, until raw lacquer Moisture is 5-6%, as can be untill wire drawing 6-10 ㎝ newton bodies;
(b) pretreatment of vegetable oil:
The 40-50 portions of linseed oil by double drifts are polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 3-4 parts of rosin Powder is together stirred and boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minutes, detection Viscosity, when linseed oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:Mediated in 50 weight ratio input kneader and 2-3 hours be Plant paint tree milk liquid composite coating.
2. according to a kind of modulator approach of plant paint tree milk liquid composite coating of claim 1, it is characterised in that processing method bag Include following steps:
(a) pretreatment of lacquer tree emulsion:
Lacquer tree emulsion is filtered in impurity elimination, input oxidation polymerization machine, is 13-15 revs/min of lower stirring at normal temperature in rotating speed, until moisture Content is 5-6%, as can be untill wire drawing 6-10 ㎝ newton bodies;
(b) pretreatment of vegetable oil:
The linseed oil of the double drifts of 40 parts of processes is polymerize in pot with 60 parts of tung oil inputs, 245 DEG C is heated to, puts into 4 parts of rosin powder Together stirring is boiled, and opens air exhauster smoke evacuation;When rosin melts completely, 275 DEG C are warming up to, is kept for 18-25 minutes, detection is viscous Degree, when linseed oil turn into can wire drawing 6-10 ㎝ newton bodies can take the dish out of the pot, and stir exhausting smoke evacuation be cooled to normal temperature;
(c) mediate:
Lacquer tree emulsion and vegetable oil by pretreatment is pressed 50:50 weight in input vacuum kneader than mediating 2-3 hours As plant paint tree milk liquid composite coating.
CN201710444820.3A 2017-06-14 2017-06-14 A kind of modulator approach of plant paint tree milk liquid composite coating Pending CN107189687A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005078031A1 (en) * 2004-02-17 2005-08-25 Meiji University Legal Person Urushi lacquer containing colloidal metal and article coated with the urushi lacquer
CN102286249A (en) * 2010-06-17 2011-12-21 葛义谦 Biological pain and manufacturing method
CN102585701A (en) * 2012-03-16 2012-07-18 惠州市长润发涂料有限公司 Vegetable oil paint
CN104387971A (en) * 2014-11-07 2015-03-04 湖南眸安土漆有限公司 Method for preparing transparent raw lacquer coating
CN105219267A (en) * 2015-10-28 2016-01-06 湖北宝石花工艺品有限公司 A kind of modulator approach of transparent raw lacquer coating
CN106221576A (en) * 2016-08-24 2016-12-14 哈尔滨漆艺之星科技发展有限公司 A kind of kermesinus paint for lacquer painting making and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005078031A1 (en) * 2004-02-17 2005-08-25 Meiji University Legal Person Urushi lacquer containing colloidal metal and article coated with the urushi lacquer
CN102286249A (en) * 2010-06-17 2011-12-21 葛义谦 Biological pain and manufacturing method
CN102585701A (en) * 2012-03-16 2012-07-18 惠州市长润发涂料有限公司 Vegetable oil paint
CN104387971A (en) * 2014-11-07 2015-03-04 湖南眸安土漆有限公司 Method for preparing transparent raw lacquer coating
CN105219267A (en) * 2015-10-28 2016-01-06 湖北宝石花工艺品有限公司 A kind of modulator approach of transparent raw lacquer coating
CN106221576A (en) * 2016-08-24 2016-12-14 哈尔滨漆艺之星科技发展有限公司 A kind of kermesinus paint for lacquer painting making and preparation method thereof

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Application publication date: 20170922