CN107189101A - A kind of fishing net with good dyeability - Google Patents
A kind of fishing net with good dyeability Download PDFInfo
- Publication number
- CN107189101A CN107189101A CN201710451852.6A CN201710451852A CN107189101A CN 107189101 A CN107189101 A CN 107189101A CN 201710451852 A CN201710451852 A CN 201710451852A CN 107189101 A CN107189101 A CN 107189101A
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- CN
- China
- Prior art keywords
- fishing net
- good dyeability
- nano diatomite
- dyeing
- nylon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/346—Clay
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/90—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/39—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67391—Salts or oxidising-compounds mixtures
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/12—Applications used for fibers
Abstract
The invention discloses a kind of fishing net with good dyeability, the master batch of nylon 6 is mixed and made into fishing net with activation nano diatomite;The present invention can solve fishing net dyeing and easily uneven dyeing occurs, dyeing flower, aberration, the problem of color defect, improve dye utilization rate and dyefastness, reduce dyeing process risk, by adding a certain amount of activation nano diatomite in being prepared in fishing net with adding a certain amount of rare earth oxide in dyestuff when fishing net is dyed, had an effect by rare earth oxide with dye molecule group, the dye groups having an effect occur effectively to be combined with activation nano diatomite again, what dyestuff can be more prone to enters inside fishing net, adhesion is improved significantly, therefore, dyeing rate and dyefastness can be significantly improved.
Description
Technical field
The invention belongs to fishing net staining technique field, and in particular to a kind of fishing net with good dyeability.
Background technology
Fishing net is the net of fishing, and modern fishing net mainly uses polyethylene, and the raw material such as nylon is processed, and has longer make
With nylon 6 it is the more and more of fishing net application prepared by main material in existing fishing net with cycle, and higher catching rate,
And according to the demand in market, the fishing net of nylon 6 is needed to carry out different dyeing processing, its performance is improved, but it is existing
The fishing net of nylon 6 is not good to the affinity of dyestuff, and dye-uptake is general, it is hard to meet the demand in market.
The content of the invention
The purpose of the present invention is that there is provided a kind of fishing net with good dyeability the problem of being directed to existing.
The present invention is achieved by the following technical solutions:
A kind of fishing net with good dyeability, fishing net is mixed and made into by the master batch of nylon 6 with activation nano diatomite.
Further, the activated diatomaceous earth preparation method is:A certain amount of nano diatomite is mixed with deionized water
The nano diatomite water slurry that mass concentration is 3.6-3.8% is configured to, the glycolic of nano diatomite quality 0.2% is added,
Be added in homogenizer under 2000r/min rotating speeds stir 1.5 hours, then use mass fraction for 0.25% hydrochloric acid
The pH of suspension is adjusted to 3.5,78 DEG C are heated to, after 120r/min rotating speeds stirring 30min, then suspension quality is added
0.16% ammonium persulfate, after stirring, 18min is incubated at 60 DEG C, using 350W ultrasonication 3min, is then carried out
Vacuum filtration, is dried using vacuum drying chamber at 100 DEG C, produced.
Further, it is described that the master batch of nylon 6 is mixed and made into fishing net with activation nano diatomite, it is specially that nylon 6 is female
Grain presses 100 with activation nano diatomite:Melting extrusion in an extruder after 3.2-3.5 mass ratio is uniformly mixed, through supercooling
But preliminary draft, drafting forming, winding, line processed, then carry out knitmesh, are made fishing net.
Further, the fishing net with good dyeability is dyed using acid dyes, in dyeing, oxytropism
Acid dyes quality 1.2-1.6% rare earth oxide is added in dyestuff, is stirred, you can.
Further, described when the fishing net with good dyeability is dyed using acid dyes, bath raio is 1:
30, dyeing condition is:50 DEG C enter dye, and 1 DEG C of heating per minute, to 88 DEG C of stoppings, being incubated 15min, is then cooled to 50 DEG C
Fishing net surface loose colour 5min is cleaned, is dried at 80 DEG C to constant weight, you can.
Further, the rare earth oxide is lanthana.
The present invention has advantages below compared with prior art:The present invention can solve fishing net dyeing and easily uneven dyeing occurs,
The problem of dyeing flower, aberration, color defect, dye utilization rate and dyefastness are improved, dyeing process risk is reduced, by being prepared in fishing net
Middle a certain amount of activation nano diatomite of addition passes through with adding a certain amount of rare earth oxide in dyestuff when fishing net is dyed
Rare earth oxide is had an effect with dye molecule group, and the dye groups having an effect are carried out with activation nano diatomite again
Effectively combine, what dyestuff can be more prone to enters inside fishing net, and adhesion is improved significantly, therefore, it is possible to significantly carry
High dyeing rate and dyefastness.
Embodiment
Embodiment 1
A kind of fishing net with good dyeability, fishing net is mixed and made into by the master batch of nylon 6 with activation nano diatomite.
The activated diatomaceous earth preparation method is:A certain amount of nano diatomite and deionized water are hybridly prepared into quality
Concentration is 3.6% nano diatomite water slurry, adds the glycolic of nano diatomite quality 0.2%, is added to high-speed stirred
Stirred 1.5 hours under 2000r/min rotating speeds in machine, then use mass fraction to adjust the pH of suspension for 0.25% hydrochloric acid
Section is heated to 78 DEG C to 3.5, after 120r/min rotating speeds stirring 30min, then adds the ammonium persulfate of suspension quality 0.16%,
After stirring, 18min is incubated at 60 DEG C, using 350W ultrasonication 3min, is then filtered by vacuum, at 100 DEG C
Lower use vacuum drying chamber is dried, and produces.
It is described that the master batch of nylon 6 is mixed and made into fishing net with activation nano diatomite, it is specially to receive the master batch of nylon 6 and activation
Rice diatomite presses 100:Melting extrusion in an extruder after 3.2 mass ratio is uniformly mixed, through supercooling preliminary draft, drawing-off is fixed
Type, winding, line processed, then knitmesh is carried out, fishing net is made.
Fishing net with good dyeability is dyed using acid dyes, in dyeing, added in oxytropism dyestuff
The rare earth oxide of Plus acidic dyestuff quality 1.2%, stirs, you can.
Described when the fishing net with good dyeability is dyed using acid dyes, bath raio is 1:30, dyer
Skill condition is:50 DEG C enter dye, and 1 DEG C of heating per minute, to 88 DEG C of stoppings, being incubated 15min, is then cooled to 50 DEG C of cleaning fishing net tables
Face loose colour 5min, is dried at 80 DEG C to constant weight, you can.
The rare earth oxide is lanthana.
Embodiment 2
A kind of fishing net with good dyeability, fishing net is mixed and made into by the master batch of nylon 6 with activation nano diatomite.
The activated diatomaceous earth preparation method is:A certain amount of nano diatomite and deionized water are hybridly prepared into quality
Concentration is 3.8% nano diatomite water slurry, adds the glycolic of nano diatomite quality 0.2%, is added to high-speed stirred
Stirred 1.5 hours under 2000r/min rotating speeds in machine, then use mass fraction to adjust the pH of suspension for 0.25% hydrochloric acid
Section is heated to 78 DEG C to 3.5, after 120r/min rotating speeds stirring 30min, then adds the ammonium persulfate of suspension quality 0.16%,
After stirring, 18min is incubated at 60 DEG C, using 350W ultrasonication 3min, is then filtered by vacuum, at 100 DEG C
Lower use vacuum drying chamber is dried, and produces.
It is described that the master batch of nylon 6 is mixed and made into fishing net with activation nano diatomite, it is specially to receive the master batch of nylon 6 and activation
Rice diatomite presses 100:Melting extrusion in an extruder after 3.5 mass ratio is uniformly mixed, through supercooling preliminary draft, drawing-off is fixed
Type, winding, line processed, then knitmesh is carried out, fishing net is made.
Fishing net with good dyeability is dyed using acid dyes, in dyeing, added in oxytropism dyestuff
The rare earth oxide of Plus acidic dyestuff quality 1.6%, stirs, you can.
Described when the fishing net with good dyeability is dyed using acid dyes, bath raio is 1:30, dyer
Skill condition is:50 DEG C enter dye, and 1 DEG C of heating per minute, to 88 DEG C of stoppings, being incubated 15min, is then cooled to 50 DEG C of cleaning fishing net tables
Face loose colour 5min, is dried at 80 DEG C to constant weight, you can.
The rare earth oxide is lanthana.
Embodiment 3
A kind of fishing net with good dyeability, fishing net is mixed and made into by the master batch of nylon 6 with activation nano diatomite.
The activated diatomaceous earth preparation method is:A certain amount of nano diatomite and deionized water are hybridly prepared into quality
Concentration is 3.7% nano diatomite water slurry, adds the glycolic of nano diatomite quality 0.2%, is added to high-speed stirred
Stirred 1.5 hours under 2000r/min rotating speeds in machine, then use mass fraction to adjust the pH of suspension for 0.25% hydrochloric acid
Section is heated to 78 DEG C to 3.5, after 120r/min rotating speeds stirring 30min, then adds the ammonium persulfate of suspension quality 0.16%,
After stirring, 18min is incubated at 60 DEG C, using 350W ultrasonication 3min, is then filtered by vacuum, at 100 DEG C
Lower use vacuum drying chamber is dried, and produces.
It is described that the master batch of nylon 6 is mixed and made into fishing net with activation nano diatomite, it is specially to receive the master batch of nylon 6 and activation
Rice diatomite presses 100:Melting extrusion in an extruder after 3.3 mass ratio is uniformly mixed, through supercooling preliminary draft, drawing-off is fixed
Type, winding, line processed, then knitmesh is carried out, fishing net is made.
Fishing net with good dyeability is dyed using acid dyes, in dyeing, added in oxytropism dyestuff
The rare earth oxide of Plus acidic dyestuff quality 1.4%, stirs, you can.
Described when the fishing net with good dyeability is dyed using acid dyes, bath raio is 1:30, dyer
Skill condition is:50 DEG C enter dye, and 1 DEG C of heating per minute, to 88 DEG C of stoppings, being incubated 15min, is then cooled to 50 DEG C of cleaning fishing net tables
Face loose colour 5min, is dried at 80 DEG C to constant weight, you can.
The rare earth oxide is lanthana.
Comparative example 1:Differed only in embodiment 1 without activation nano diatomite.
Comparative example 2:Differed only in embodiment 1 without common untreated nano diatomite.
Comparative example 3:Rare earth oxide is not added in acid dyes when differing only in dyeing with embodiment 1.
Experiment:Using infrared high-temperature overflow dyeing machine, dyestuff is Acid Red G RS, respectively by embodiment and comparative example method system
Into fishing net and dyed, using ultraviolet specrophotometer test dyeing stoste optical density, record dye liquor raffinate absorbance, meter
Calculate dye-uptake:
Table 1
Dye-uptake % | |
Embodiment 1 | 98.36 |
Embodiment 2 | 98.30 |
Embodiment 3 | 98.32 |
Comparative example 1 | 82.17 |
Comparative example 2 | 85.26 |
Comparative example 3 | 89.22 |
As can be seen from Table 1, can substantially it be carried using nano diatomite of the present invention after activation process in fishing net preparation
The dye-uptake for the fishing net that height is made, the fishing net dye-uptake being made of common nano diatomite is substantially reduced, and is added in dyestuff
Rare earth oxide can cooperate with the Dye up-take for improving fishing net with activation nano diatomite;
Washing fastness test is carried out to the fishing net after above-mentioned dyeing, graded using standard grey scale, as a result such as table 2:
Table 2
Colour fading fastness/level | Staining fastness/level | |
Embodiment 1 | 5 | 4 |
Embodiment 2 | 5 | 4 |
Embodiment 3 | 5 | 4 |
Comparative example 1 | 3 | 2 |
Comparative example 2 | 3 | 2 |
Comparative example 3 | 4 | 3 |
As can be seen from Table 2, can substantially it be carried using nano diatomite of the present invention after activation process in fishing net preparation
The dyestuff fastness for the fishing net that height is made, the fishing net dyefastness being made of common nano diatomite is substantially reduced, in dyestuff
Addition rare earth oxide can cooperate with the dyefastness for improving fishing net with activation nano diatomite.
Claims (6)
1. a kind of fishing net with good dyeability, it is characterised in that the master batch of nylon 6 is mixed into system with activation nano diatomite
Into fishing net.
2. a kind of fishing net with good dyeability according to claim 1, it is characterised in that the activated diatomaceous earth
Preparation method is:A certain amount of nano diatomite and deionized water are hybridly prepared into the nano-silicon that mass concentration is 3.6-3.8%
Diatomaceous earth water slurry, adds the glycolic of nano diatomite quality 0.2%, is added in homogenizer in 2000r/min rotating speeds
Lower stirring 1.5 hours, then uses mass fraction to adjust the pH of suspension to 3.5 for 0.25% hydrochloric acid, is heated to 78 DEG C,
After 120r/min rotating speeds stirring 30min, then the ammonium persulfate of suspension quality 0.16% is added, after stirring, at 60 DEG C
18min is incubated, using 350W ultrasonication 3min, is then filtered by vacuum, is carried out at 100 DEG C using vacuum drying chamber
Dry, produce.
3. a kind of fishing net with good dyeability according to claim 1, it is characterised in that described that nylon 6 is female
Grain is mixed and made into fishing net with activation nano diatomite, is specially that the master batch of nylon 6 and activation nano diatomite are pressed into 100:3.2-3.5
Mass ratio uniformly melting extrusion in an extruder after mixing, through supercooling preliminary draft, drafting forming, winding, line processed, then enter
Row knitmesh, is made fishing net.
4. the colouring method of a kind of fishing net with good dyeability according to claim 1, it is characterised in that will have
The fishing net for having good dyeability is dyed using acid dyes, in dyeing, and acid dyes matter is added in oxytropism dyestuff
1.2-1.6% rare earth oxide is measured, is stirred, you can.
5. the colouring method of a kind of fishing net with good dyeability according to claim 4, it is characterised in that described
When fishing net with good dyeability is dyed using acid dyes, bath raio is 1:30, dyeing condition is:50℃
Enter dye, 1 DEG C of heating per minute, to 88 DEG C of stoppings, being incubated 15min, is then cooled to 50 DEG C of cleaning fishing net surface loose colour 5min,
Dried at 80 DEG C to constant weight, you can.
6. the colouring method of a kind of fishing net with good dyeability according to claim 4, it is characterised in that described
Rare earth oxide is lanthana.
Priority Applications (1)
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CN201710451852.6A CN107189101A (en) | 2017-06-15 | 2017-06-15 | A kind of fishing net with good dyeability |
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CN201710451852.6A CN107189101A (en) | 2017-06-15 | 2017-06-15 | A kind of fishing net with good dyeability |
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CN201710451852.6A Pending CN107189101A (en) | 2017-06-15 | 2017-06-15 | A kind of fishing net with good dyeability |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109024001A (en) * | 2018-08-03 | 2018-12-18 | 巢湖市渔郎渔具有限公司 | A method of improving fishing net dyeing efficiency |
CN109281200A (en) * | 2018-09-26 | 2019-01-29 | 深圳市裕农科技股份有限公司 | A kind of dyeing assistant and preparation method thereof |
CN110093790A (en) * | 2019-04-30 | 2019-08-06 | 巢湖市翔宇渔具有限公司 | A kind of method of fishing net natural pigment dyeing |
CN110106727A (en) * | 2019-04-26 | 2019-08-09 | 巢湖市翔宇渔具有限公司 | A kind of fishing net colouring method reducing sewage yield |
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CN104562249A (en) * | 2014-06-30 | 2015-04-29 | 巢湖市翔宇渔具有限公司 | Fishing net wire molding process |
CN104963219A (en) * | 2015-07-09 | 2015-10-07 | 上海工程技术大学 | Method for improving dyeing rate and fixation rate of reactive dye on kawo kawo fibers |
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CN104562249A (en) * | 2014-06-30 | 2015-04-29 | 巢湖市翔宇渔具有限公司 | Fishing net wire molding process |
CN104963219A (en) * | 2015-07-09 | 2015-10-07 | 上海工程技术大学 | Method for improving dyeing rate and fixation rate of reactive dye on kawo kawo fibers |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109024001A (en) * | 2018-08-03 | 2018-12-18 | 巢湖市渔郎渔具有限公司 | A method of improving fishing net dyeing efficiency |
CN109281200A (en) * | 2018-09-26 | 2019-01-29 | 深圳市裕农科技股份有限公司 | A kind of dyeing assistant and preparation method thereof |
CN109281200B (en) * | 2018-09-26 | 2020-11-13 | 深圳市裕农科技股份有限公司 | Dyeing auxiliary and preparation method thereof |
CN110106727A (en) * | 2019-04-26 | 2019-08-09 | 巢湖市翔宇渔具有限公司 | A kind of fishing net colouring method reducing sewage yield |
CN110093790A (en) * | 2019-04-30 | 2019-08-06 | 巢湖市翔宇渔具有限公司 | A kind of method of fishing net natural pigment dyeing |
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