CN107167429A - A kind of reactor observation sampling apparatus for being used to produce TBP tributyl phosphates - Google Patents
A kind of reactor observation sampling apparatus for being used to produce TBP tributyl phosphates Download PDFInfo
- Publication number
- CN107167429A CN107167429A CN201710626653.4A CN201710626653A CN107167429A CN 107167429 A CN107167429 A CN 107167429A CN 201710626653 A CN201710626653 A CN 201710626653A CN 107167429 A CN107167429 A CN 107167429A
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- Prior art keywords
- observation
- tank
- tracheae
- pipe
- sampling apparatus
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N2001/1031—Sampling from special places
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
Abstract
A kind of reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, is related to a kind of observation sampling apparatus, tracheae（7）One end and observation tank（20）Upper end connection, tracheae（7）Load is in " L " shape support bar（6）The other end passes through perforation after upper（12）End is located at cavity A（18）Top, observation tank（20）Lower end and charging aperture（3）Between be connected with liquid pipe（19）, observe tank（20）And sleeve A（8）Connection, in observation tank（20）Side wall be provided with sampling pipe（5）；The present invention connects the tracheae of tank inner chamber body by being set in observation tank top, in observation pot bottom, the liquid pipe of reaction solution in connection tank body is set, move up and down observation tank, the reaction solution for making observation tank inject in tank body, realizes the situation of reaction solution and the beneficial effect sampled in time in observation tank body in time.
Description
【Technical field】
Sampling apparatus is observed the present invention relates to one kind, is used more particularly, to a kind of reactor for being used to produce TBP tributyl phosphates
Observe sampling apparatus.
【Background technology】
The agent of TBP calcium phosphate+ forages is used as solvent, also frequently as NC Nitroncellulose, cellulose acetate, chlorinated rubber and polychlorostyrene
The plasticizer of ethene, the extractant of rare metal etc., heat exchange medium.Due to its low surface tension, the physical property of water is insoluble in,
The film of established foam can be effectively set to be in an unsure state and rapid froth breaking as industrial defoamer.In production
General raw material is oxygen phosphorus and butanol during TBP tributyl phosphates, is generally required when oxygen phosphorus and butanol are reacted and uses reaction
Kettle, when reactor is reacted oxygen phosphorus and butanol, the agitating device in reactor, which is served, is sufficiently mixed two kinds of solution
Effect, prepare TBP calcium phosphate+ forage agent during, due to it is technologic requirement, it is necessary to which reaction solution is passed through
Different filling bodies are repeatedly replaced, but how long need to change the time for filling and typically all calculating according to technological process, are also had
The time rule of thumb drawn, is due to circumstance of temperature difference and reactor though due technique effect can be played by so doing
The influence of the factors such as aging, calculates from manufacture craft level is improved, the raising of Product Precision still has against the theoretic time
A certain distance, traditional reactor is general to be both provided with observation window at top, but observation window can only see at the top of liquid level
Situation, it is impossible to know the situation of liquid level bottom, more the solution in tank can not be sampled in time.
【The content of the invention】
In order to overcome the shortcomings of in background technology, the present invention discloses a kind of reactor for being used to produce TBP tributyl phosphates and seen
Sampling apparatus is examined, the tracheae of tank inner chamber body is connected by being set in observation tank top, connection tank body is set in observation pot bottom
The liquid pipe of interior reaction solution, moves up and down observation tank, the reaction solution for making observation tank inject in tank body, realizes observation tank in time
The situation of internal reaction solution and the beneficial effect sampled in time.
In order to realize the goal of the invention, the present invention is adopted the following technical scheme that：
A kind of reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, including tank body, tracheae, column and observation
Tank, cavity A is provided with the inside of tank body, and the centre position at the top of tank body is provided with motor, and the rotating shaft of motor is stretched into cavity A simultaneously
Stirring-head is provided with the end of rotating shaft, charging aperture is additionally provided with the top of tank body, discharging opening is provided with the bottom of tank body, in discharging
Mouth is provided with bearing in the lower end of column, is respectively sleeved on sleeve pipe B and sleeve A, sleeve pipe from top to bottom on column provided with perforation
B and sleeve A can be slided on column, and " L " shape support bar is provided with sleeve pipe B, and cavity B is provided with observation tank, tracheae
One end and the upper end connection of observation tank, tracheae load rear other end on " L " shape support bar are located at cavity A top through perforated tip
Portion, liquid pipe, observation tank and sleeve A connection are connected between the lower end of observation tank and charging aperture, is set on the side wall of observation tank
There is sampling pipe.
The described reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, between observation tank and sleeve A
Provided with connecting rod.
The described reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, is provided with valve on sampling pipe
A, is provided with valve B in liquid pipe, and valve C is provided with the lower end of discharging opening, and valve D is provided with tracheae.
The described reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, the material of observation tank is transparent
Glass.
The described reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, tracheae and liquid pipe are respectively soft
Pipe.
By adopting the above-described technical solution, the present invention has the advantages that：
The reactor observation sampling apparatus of the present invention for being used to produce TBP tributyl phosphates, by observation tank top
The tracheae of connection tank inner chamber body is set, the liquid pipe of reaction solution in connection tank body is set in observation pot bottom, sight is moved up and down
Examine tank, make observation tank inject tank body in reaction solution, realize in time observation tank body in reaction solution situation and adopt in time
The beneficial effect of sample；Unique structure of the present invention, reasonable in design, practical, wide market.
【Brief description of the drawings】
Fig. 1 is structural representation of the invention；
In figure：1st, tank body；2nd, motor；3rd, charging aperture；4th, valve A；5th, sampling pipe；6th, " L " shape support bar；7th, tracheae；8th, sleeve pipe
A；9th, sleeve pipe B；10th, column；11st, discharging opening；12nd, perforate；13rd, valve B；14th, valve C；15th, valve D；16th, stirring-head；17、
Reaction solution；18th, cavity A；19th, liquid pipe；20th, tank is observed；21st, cavity B；22nd, connecting rod；23rd, bearing.
【Embodiment】
The present invention can be explained in more detail by the following examples, it is open the invention is not limited in the following examples
The purpose of the present invention is intended to protect all changes and improvements in the scope of the invention；
Being used for reference to described in accompanying drawing 1 produces the reactor observation sampling apparatus of TBP tributyl phosphates, including tank body 1, tracheae
7th, column 10 and observation tank 20, cavity A18 is provided with the inside of tank body 1, and motor 2, electricity are provided with the centre position at the top of tank body 1
The rotating shaft of machine 2 is stretched into cavity A18 and is provided with stirring-head 16 in the end of rotating shaft, and charging aperture 3 is additionally provided with the top of tank body 1,
Discharging opening 11 is provided with the bottom of tank body 1, provided with perforation 12 on discharging opening 11, bearing 23 is provided with the lower end of column 10,
Sleeve pipe B9 and sleeve A 8 are respectively sleeved on column 10 from top to bottom, sleeve pipe B9 and sleeve A 8 can be slided on column 10,
Sleeve pipe B9 is provided with " L " shape support bar 6, and the material of observation tank 20 is clear glass, and cavity B21, gas are provided with observation tank 20
One end of pipe 7 and the upper end connection of observation tank 20, the other end passes through 12 ends of perforation position after tracheae 7 is carried on a shoulder pole on " L " shape support bar 6
In cavity A18 top, liquid pipe 19 is connected between the lower end of observation tank 20 and charging aperture 3, observation tank 20 and sleeve A 8 connect
Connect, connecting rod 22 is provided between observation tank 20 and sleeve A 8, sampling pipe 5 is provided with the side wall of observation tank 20, in sampling pipe 5
Valve A4 is provided with, valve B13 is provided with liquid pipe 19, valve C14 is provided with the lower end of discharging opening 11, is provided with tracheae 7
Valve D15, tracheae 7 and liquid pipe 19 are respectively flexible pipe.
Implement the reactor observation sampling apparatus of the present invention for being used to produce TBP tributyl phosphates, needing to obtain
When reporting situations of reaction solution 17 in tank body 1 is taken, valve A4 and valve C14, Open valve B13 and valve D15 is closed, downwards
Mobile sleeve pipe A8, the level height for observing tank 20 is placed in below the liquid level of reaction solution 17, at this moment, the air in observation tank 20
Flowed into along tracheae 7 in cavity A18, reaction solution 17 is flowed into observation tank 20 along liquid pipe 19, because observation tank 20 is transparent, institute
Can intuitively see the situation of reaction solution 17, it is necessary to which when obtaining the situation of reaction solution 17 in tank body 1 again, elder generation is upwards
Mobile sleeve pipe A8, the level height for observing tank 20 is placed in more than the liquid level of reaction solution 17, at this moment, the reaction in observation tank 20
Solution 17 is flowed back in tank body 1 along liquid pipe 19, the air in cavity A18 along tracheae 7 flow into observation tank 20 along, again by sleeve A 8 to
Lower movement, you can obtain the latest data of reaction solution 17 in tank body 1 again, it is desirable to when being sampled to reaction solution 17, open
Valve A4 is opened, the reaction solution 17 for needing to sample is picked out from sampling pipe 5, after sampling is finished, valve A4 is closed, when need not pass through
When observing the reaction solution 17 in the observation tank body 1 of tank 20, sleeve A 8 is moved up, the level height for observing tank 20 is placed in reaction
More than the liquid level of solution 17, the reaction solution 17 observed in tank 20 is emptied, close valve B13 and valve D15.
Part not in the detailed description of the invention is prior art.
Claims (5)
1. a kind of reactor observation sampling apparatus for being used to produce TBP tributyl phosphates, including tank body（1）, tracheae（7）, it is vertical
Post（10）With observation tank（20）, it is characterized in that：In tank body（1）Inside be provided with cavity A（18）, in tank body（1）The centre at top
Position is provided with motor（2）, motor（2）Rotating shaft stretch into cavity A（18）It is interior and the end of rotating shaft be provided with stirring-head（16）, in tank
Body（1）Top be additionally provided with charging aperture（3）, in tank body（1）Bottom be provided with discharging opening（11）, in discharging opening（11）It is provided with and wears
Hole（12）, in column（10）Lower end be provided with bearing（23）, in column（10）On be respectively sleeved on sleeve pipe B from top to bottom（9）With
Sleeve A（8）, sleeve pipe B（9）And sleeve A（8）Can be in column（10）It is upper to slide, in sleeve pipe B（9）It is provided with " L " shape support bar
（6）, in observation tank（20）It is interior to be provided with cavity B（21）, tracheae（7）One end and observation tank（20）Upper end connection, tracheae（7）Load
In " L " shape support bar（6）The other end passes through perforation after upper（12）End is located at cavity A（18）Top, observation tank（20）'s
Lower end and charging aperture（3）Between be connected with liquid pipe（19）, observe tank（20）And sleeve A（8）Connection, in observation tank（20）Side wall
It is provided with sampling pipe（5）.
2. the reactor observation sampling apparatus according to claim 1 for being used to produce TBP tributyl phosphates, its feature
It is：In observation tank（20）And sleeve A（8）Between be provided with connecting rod（22）.
3. the reactor observation sampling apparatus according to claim 1 for being used to produce TBP tributyl phosphates, its feature
It is：In sampling pipe（5）It is provided with valve A（4）, in liquid pipe（19）It is provided with valve B（13）, in discharging opening（11）Lower end be provided with
Valve C（14）, in tracheae（7）It is provided with valve D（15）.
4. the reactor observation sampling apparatus according to claim 1 for being used to produce TBP tributyl phosphates, its feature
It is：Observe tank（20）Material be clear glass.
5. the reactor observation sampling apparatus according to claim 1 for being used to produce TBP tributyl phosphates, its feature
It is：Tracheae（7）And liquid pipe（19）Respectively flexible pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710626653.4A CN107167429B (en) | 2017-07-28 | 2017-07-28 | A reation kettle is with observing sampling device for producing TBP tributyl phosphate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710626653.4A CN107167429B (en) | 2017-07-28 | 2017-07-28 | A reation kettle is with observing sampling device for producing TBP tributyl phosphate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107167429A true CN107167429A (en) | 2017-09-15 |
| CN107167429B CN107167429B (en) | 2023-03-17 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710626653.4A Active CN107167429B (en) | 2017-07-28 | 2017-07-28 | A reation kettle is with observing sampling device for producing TBP tributyl phosphate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107167429B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3001437U (en) * | 1994-02-25 | 1994-08-30 | 三共株式会社 | Sampling device |
| CN201997328U (en) * | 2010-11-29 | 2011-10-05 | 广东紫金正天药业有限公司 | Chemical reaction tank |
| CN202045111U (en) * | 2011-03-10 | 2011-11-23 | 宝山钢铁股份有限公司 | Portable sampling pipe degreasing purging device |
| CN205748991U (en) * | 2016-06-03 | 2016-11-30 | 王勇 | A kind of oil product detection Composite sample sampler |
-
2017
- 2017-07-28 CN CN201710626653.4A patent/CN107167429B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3001437U (en) * | 1994-02-25 | 1994-08-30 | 三共株式会社 | Sampling device |
| CN201997328U (en) * | 2010-11-29 | 2011-10-05 | 广东紫金正天药业有限公司 | Chemical reaction tank |
| CN202045111U (en) * | 2011-03-10 | 2011-11-23 | 宝山钢铁股份有限公司 | Portable sampling pipe degreasing purging device |
| CN205748991U (en) * | 2016-06-03 | 2016-11-30 | 王勇 | A kind of oil product detection Composite sample sampler |
Non-Patent Citations (1)
| Title |
|---|
| 张敏,周斌: "原油罐下采样设施的应用和改进" * |
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| Publication number | Publication date |
|---|---|
| CN107167429B (en) | 2023-03-17 |
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