CN107166171A - A kind of system that sodium hypochlorite reaction speed is controlled in chlor-alkali production - Google Patents
A kind of system that sodium hypochlorite reaction speed is controlled in chlor-alkali production Download PDFInfo
- Publication number
- CN107166171A CN107166171A CN201710487743.XA CN201710487743A CN107166171A CN 107166171 A CN107166171 A CN 107166171A CN 201710487743 A CN201710487743 A CN 201710487743A CN 107166171 A CN107166171 A CN 107166171A
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- China
- Prior art keywords
- chlorine
- regulating valve
- delivery pipe
- sodium hypochlorite
- chlor
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Classifications
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17D—PIPE-LINE SYSTEMS; PIPE-LINES
- F17D1/00—Pipe-line systems
- F17D1/02—Pipe-line systems for gases or vapours
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/34—Simultaneous production of alkali metal hydroxides and chlorine, oxyacids or salts of chlorine, e.g. by chlor-alkali electrolysis
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17D—PIPE-LINE SYSTEMS; PIPE-LINES
- F17D3/00—Arrangements for supervising or controlling working operations
- F17D3/01—Arrangements for supervising or controlling working operations for controlling, signalling, or supervising the conveyance of a product
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
The present invention relates to the system that sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production, including the first regulating valve being installed in turbo-compressor sealing nitrogen tube, also include delivery pipe, recovery tube, dechlorination vavuum pump and the second regulating valve, one end of the delivery pipe is connected with the first regulating valve port of export pipeline, and chlorine delivery pipe is connected in the other end and chlorine production of the delivery pipe;One end of the recovery tube is connected on the delivery pipe, and the other end of the recovery tube is connected with useless chlorine absorption system;And the dechlorination vavuum pump is connected on the delivery pipe, second regulating valve is installed on the side of the entrance point close to the dechlorination vavuum pump.By the implementation of the present invention, the chlorine that turbo-compressor can be sealed to nitrogen entrainment is changed into chlorine delivery pipe, reduces the logical chlorine dose of useless chlorine absorption system, and then extend the reaction time of sodium hypochlorite.
Description
Technical field
The present invention relates to chlorine turbine type compression set and sodium hypochlorite reaction speed and production in alkali chemical industry enterprises production
The control of amount.
Background technology
The compression of alkali chemical industry enterprises chlorine in the prior art more uses turbo-compressor.The work of turbo-compressor
Process:Enter chlorine gas compressor group by dry chlorine, it rotates produced centrifugal force to chlorine by means of the high speed of impeller
Air-flow work done, is allowed to obtain kinetic energy and static energy, so that cl gas flow pressure rise, 0.150MPa is compressed to by chlorine.Then
Deliver to downstream user.
Wherein, turbo-compressor gland seal device uses labyrinth seal, but only one section great runner of resistance of labyrinth seal.
Effectively to prevent chlorine from leaking, employ and take out, inflate the labyrinth seal form being combined.Therefore turbo-compressor must be used and contained
The wet nitrogen less than 50PPM is sealed, and sealed position is bearing.As shown in Fig. 2 sealing nitrogen by turbo-compressor
Tail chlorine in pipe 1 is directly discharged into useless chlorine absorption system.
The course of work of useless chlorine absorption system is as described below.The waste gas containing chlorine is sent to useless chlorine during chlor-alkali production
Absorption tower.Waste gas containing chlorine includes the sealing nitrogen containing chlorine that turbo-compressor is discharged or leaked.Circulating pump
Absorbing liquid containing 15-20% concentration alkali in retort is squeezed into after cooler cooling, absorbing liquid enters useless chlorine absorption tower simultaneously
Sprayed from absorbing liquid distributor.Waste gas containing chlorine, which is passed through from bottom, enters useless chlorine absorption tower, and filler surface with
Absorbing liquid counter current contacting, reaches the purpose of absorption.Absorbing liquid, which is absorbed in waste gas, forms the inflow of semi-finished product liquid instead after chlorine
Answer and continue circular response in tank, until it becomes stopping reaction after finished product.The tail gas formed after waste gas dechlorination is straight through air-introduced machine
Connect extraction emptying.Useless chlorine absorption system controls negative pressure to be (- 1-- 3kPa).
32.00% liquid caustic soda is made into the absorbing liquid of 15-20% concentration alkali, absorbing liquid in retort with river or chlorine water
The reaction product including sodium hypochlorite is generated with the chlorine reaction in sealing nitrogen.So the chlorine adulterated in sealing nitrogen
The reaction speed of sodium hypochlorite is accelerated, because the amount of chlorine that the sealing nitrogen of turbo-compressor is carried secretly is compressed with turbine type
Machine labyrinth seal leakage rate increases, and is discharged into the amount of chlorine increase of useless chlorine absorption system, so accelerating time of useless chlorine absorption system
Sodium chlorate reaction speed and the yield for adding sodium hypochlorite.So as to passively produce sodium hypochlorite, but sodium hypochlorite is by under
User's restriction is swum, the control of device load is affected.
Although output of the amount of chlorine relative to chlorine during chlor-alkali production of turbo-compressor sealing nitrogen entrainment
Considerably less, but for the industry, the reaction speed for sodium hypochlorite in the chlorine absorption system that gives up is still one and is relatively difficult to resolve
Certainly the problem of.
The content of the invention
The technical problems to be solved by the invention, which are to provide in a kind of chlor-alkali production, controls the sodium hypochlorite reaction speed to be
System, can reduce the reaction speed and the yield according to required control sodium hypochlorite of sodium hypochlorite.
The technical scheme that the present invention solves above-mentioned technical problem is as follows:Sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production
The system of sodium hypochlorite reaction speed is controlled in the system of degree, a kind of chlor-alkali production, including is installed on turbo-compressor sealing
The first regulating valve in nitrogen tube, in addition to delivery pipe, recovery tube, dechlorination vavuum pump and the second regulating valve, the delivery pipe
One end is connected with the first regulating valve port of export pipeline, and chlorine delivery pipe connects in the other end and chlorine production of the delivery pipe
Connect;One end of the recovery tube is connected on the delivery pipe, and the other end of the recovery tube is connected with useless chlorine absorption system;With
And the dechlorination vavuum pump is connected on the delivery pipe, second regulating valve is installed on entering close to the dechlorination vavuum pump
The side at mouth end.
The beneficial effects of the invention are as follows:The chlorine that turbo-compressor can be sealed to nitrogen entrainment is changed into chlorine discharge
Pipe, reduces the logical chlorine dose of useless chlorine absorption system, and then extend the reaction time of sodium hypochlorite.
On the basis of above-mentioned technical proposal, the present invention can also do following improvement.
Further, the system that sodium hypochlorite reaction speed is controlled in the chlor-alkali production, in addition to distance-transmission pressure gauge, it is described
Distance-transmission pressure gauge is connected with second regulating valve.
Further, the system that sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production, in addition to controller, it is described
Second regulating valve and the controller are electrically connected with, and the controller is shown to described the according to the pressure of the distance-transmission pressure gauge
Two regulating valves automatically adjust.
It is that remote pressure gauge is used to show that dechlorination vavuum pump entrance point is nitrogenous using the beneficial effect of above-mentioned further scheme
The pressure of chlorine, so that controller is implemented to automatically adjust to the second regulating valve, so that the nitrogenous chlorine of dechlorination vavuum pump entrance point
Stress control in the range of -1 to -3kPa, to ensure that turbo-compressor seals the stability of flow of nitrogen, so that stable turbine
The operation of formula compressor.
Further, the system that sodium hypochlorite reaction speed is controlled in the chlor-alkali production, in addition to the 3rd regulating valve, it is described
3rd regulating valve is installed on the delivery pipe between the recovery tube and second regulating valve.
It is that the 3rd regulating valve is used to block or open into dechlorination vavuum pump using the beneficial effect of above-mentioned further scheme
The nitrogenous chlorine of entrance point.So as to flexibly control the flow direction of nitrogenous chlorine, and then control the reaction speed of sodium hypochlorite.
Further, the system that sodium hypochlorite reaction speed is controlled in the chlor-alkali production, in addition to the 4th regulating valve, it is described
4th regulating valve is installed on the recovery tube.
It is that the 4th regulating valve is used to block or open into useless chlorine to absorb system using the beneficial effect of above-mentioned further scheme
The nitrogenous chlorine of system.So as to flexibly control the flow direction of nitrogenous chlorine, and then control the reaction speed of sodium hypochlorite.
Further, chlorine is arranged in the system that sodium hypochlorite reaction speed is controlled in the chlor-alkali production, the chlorine production
Put the chlorine output pipe that pipe is electrolytic cell during chlor-alkali production.
Further, the system that sodium hypochlorite reaction speed is controlled in the chlor-alkali production, the output chlorine of the electrolytic cell
Pipe is connected with downstream user end.
Electrolysis is mixed using the nitrogenous chlorine that the beneficial effect of above-mentioned further scheme is the discharge of dechlorination vacuum pump outlet end
The chlorine produced in groove together leads to downstream user end.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention;
Fig. 2 is prior art construction schematic diagram.
In accompanying drawing, the list of parts representated by each label is as follows:
1st, turbo-compressor sealing nitrogen tube, 2, delivery pipe, 3, recovery tube, 4, dechlorination vavuum pump, the 11, first regulation
Valve, the 21, the 3rd regulating valve, the 31, the 4th regulating valve, the 41, second regulating valve, 42, distance-transmission pressure gauge.
Embodiment
The principle and feature of the present invention are described below in conjunction with accompanying drawing, the given examples are served only to explain the present invention, and
It is non-to be used to limit the scope of the present invention.
In the description of the invention, it is to be understood that the orientation or position of the instruction such as term " on ", " under ", " interior ", " outer "
It is, based on orientation shown in the drawings or position relationship, to be for only for ease of the description present invention and simplify description to put relation, rather than
Indicate or imply that the device or element of meaning there must be specific orientation, with specific azimuth configuration and operation, therefore can not
It is interpreted as limitation of the present invention.In the description of the invention, " multiple " are meant that two or more, are limited unless otherwise clearly tool
It is fixed.
In the description of the invention, it is necessary to illustrate, unless otherwise clearly defined and limited, term " installation ", " phase
Even ", " connection " should be interpreted broadly, for example, it may be being fixedly connected or being detachably connected, or be integrally connected;Can
To be to be directly connected to, can also be indirectly connected with by intermediary, can be two element internals connection or two elements
Interaction relationship.For the ordinary skill in the art, above-mentioned term can be understood in the present invention with concrete condition
Concrete meaning.
As shown in figure 1, the present invention provides the system that sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production, including install
The first regulating valve 11 in nitrogen tube 1 is sealed in turbo-compressor.Also include delivery pipe 2, recovery tube 3, the and of dechlorination vavuum pump 4
Second regulating valve 41.One end of delivery pipe 2 is connected with the port of export pipeline of the first regulating valve 11.The other end and chlorine of delivery pipe 2
Chlorine delivery pipe is connected in production.One end of recovery tube 3 is connected on delivery pipe 2.The other end of recovery tube 3 absorbs with useless chlorine
System connection.Dechlorination vavuum pump 4 is connected on delivery pipe 2.Second regulating valve 41 is installed on the entrance point close to dechlorination vavuum pump 4
Side.
By the implementation of the present invention, the first regulating valve 11 is used to be turned on and off in turbo-compressor sealing nitrogen tube 1
Whether nitrogenous chlorine discharges.Delivery pipe 2 is used to nitrogenous chlorine leading to chlorine delivery pipe.Because nitrogenous chlorine is from turbine type pressure
Contracting secret envelope nitrogen tube 1 in pressure be negative pressure, be specially -1 to -3kPa and in chlorine delivery pipe chlorine pressure be 30kPa.
So needing the device of the connection regulation pressure on delivery pipe 2, such as the second regulating valve 41 and dechlorination vavuum pump 4.Second regulating valve
41 be used for from turbo-compressor seal nitrogen tube 1 discharge nitrogenous chlorine carry out pressure adjustment, make its control -1 to -
In the range of 3kPa, to ensure that turbo-compressor seals the stability of flow of nitrogen, so that the operation of stable turbo-compressor.It is de-
Chlorine vavuum pump 4 is used to pressurize to nitrogenous chlorine, makes its pressure identical with chlorine gas pressure in chlorine delivery pipe, is specially
30kPa.When user terminal needs sodium hypochlorite, the second regulating valve 41 is closed, nitrogenous chlorine is led to recovery tube 3 and then is passed through useless
Chlorine absorption system is so as to manufacture sodium hypochlorite.The chlorine that the present invention can seal turbo-compressor nitrogen entrainment is changed into chlorine
Delivery pipe, reduces the logical chlorine dose of useless chlorine absorption system, and then extends the reaction time of sodium hypochlorite.
In one embodiment, in addition to distance-transmission pressure gauge 42.Distance-transmission pressure gauge 42 is connected with the second regulating valve 41.Teletransmission pressure
Power table 42 is applied to the pressure that measurement does not play the media such as the liquid, steam and gas of corrosiveness to steel and copper alloy.Because
One slide wire resistance formula transmitter is set inside electric resistance long distance sensing pressure meter, therefore measured value can be reached away from the secondary of measurement with electricity
In instrument, to realize centralized detecting and far distance controlled.In addition, distance-transmission pressure gauge and pressure can be indicated on the spot, in order to scene
Performance review.Specifically, the gas access end of distance-transmission pressure gauge 42 is connected with the port of export of the second regulating valve 41.Distance-transmission pressure gauge
42 be equipment in the prior art, and its specific attachment structure with the second regulating valve 41 is not existed herein with being present in the prior art
Repeat.
Further, in addition to controller (not shown).Second regulating valve 41 is electrically connected with controller.Controller
Shown according to the pressure of distance-transmission pressure gauge 42 and second regulating valve 41 is automatically adjusted.
By the implementation of the present embodiment, remote pressure gauge 42 is used for the pressure for showing the nitrogenous chlorine of the entrance point of dechlorination vavuum pump 4
Power, so that controller is implemented to automatically adjust to the second regulating valve 41, so that the pressure of the nitrogenous chlorine of the entrance point of dechlorination vavuum pump 4
Control is in the range of -1 to -3kPa, to ensure that turbo-compressor seals the stability of flow of nitrogen, so that stable turbine type compression
The operation of machine.
In one embodiment, in addition to the 3rd regulating valve 21.3rd regulating valve 21 is installed on the regulating valve of recovery tube 3 and second
On delivery pipe 2 between 41.The mounting means that 3rd regulating valve 21 is installed on delivery pipe 2 uses installation side of the prior art
Formula, press and open holes point is used at the entry and exit two ends of the 3rd regulating valve 21 and the junction of delivery pipe 2.
By the implementation of the present embodiment, the 3rd regulating valve 21 is used to block or open into the entrance point of dechlorination vavuum pump 4
Nitrogenous chlorine.So as to flexibly control the flow direction of nitrogenous chlorine, and then control the reaction speed of sodium hypochlorite.When there is user's request
When, the 3rd regulating valve 21 is closed, nitrogenous chlorine leads to useless chlorine absorption system and is used to produce sodium hypochlorite.When no user demand,
The 3rd regulating valve 21 is opened, nitrogenous chlorine leads to chlorine delivery pipe.
In one embodiment, in addition to the 4th regulating valve 31.4th regulating valve 31 is installed on recovery tube 3.4th regulation
The mounting means that valve 31 is installed on recovery tube 3 uses mounting means of the prior art, in the entry and exit of the 4th regulating valve 31
Two ends and the junction of recovery tube 3 use press and open holes point.
By the implementation of the present embodiment, the 4th regulating valve 31 is used to blocking or opening the nitrogenous chlorine into useless chlorine absorption system
Gas.So as to flexibly control the flow direction of nitrogenous chlorine, and then control the reaction speed of sodium hypochlorite.When there is user's request, open
4th regulating valve 31, recovery tube 3 is connected with useless chlorine absorption system;The second regulating valve 41 is closed, delivery pipe 2 hinders with chlorine delivery pipe
It is disconnected;Nitrogenous chlorine leads to useless chlorine absorption system, for producing sodium hypochlorite.When no user demand, the 4th regulating valve 31 is closed,
Recovery tube 3 is blocked with useless chlorine absorption system;The second regulating valve 41 is opened, delivery pipe 2 is connected with chlorine delivery pipe;Nitrogenous chlorine row
It is put into chlorine delivery pipe.
In one embodiment, chlorine delivery pipe is the chlorine output pipe of electrolytic cell during chlor-alkali production in chlorine production.
Specifically, the port of export of dechlorination vavuum pump 4 is connected by the chlorine output pipe of pipeline and electrolytic cell.
Further, the chlorine output pipe of electrolytic cell is connected with downstream user end.
By the implementation of the present embodiment, produced in the nitrogenous chlorine mixing electrolytic cell of the port of export of dechlorination vavuum pump 4 discharge
Chlorine together leads to downstream user end.In mixed gas, because nitrogenous amount of chlorine is relative to the amount of chlorine produced in electrolytic cell
Very few, the nitrogen content in nitrogenous chlorine is also considerably less in addition, so having no effect on usability of the downstream user to chlorine.
Specifically, the content of nitrogenous chlorine is 30 cubes, the amount of chlorine produced in electrolytic cell is 5500 to 6000 cubes.
The foregoing is only presently preferred embodiments of the present invention, be not intended to limit the invention, it is all the present invention spirit and
Within principle, any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (7)
1. controlling the system of sodium hypochlorite reaction speed in a kind of chlor-alkali production, including it is installed on turbo-compressor sealing nitrogen
Manage (1) on the first regulating valve (11), it is characterised in that also including delivery pipe (2), recovery tube (3), dechlorination vavuum pump (4) and
Second regulating valve (41),
One end of the delivery pipe (2) is connected with the first regulating valve (11) port of export pipeline, the delivery pipe (2) it is another
End is connected with chlorine delivery pipe in chlorine production;
One end of the recovery tube (3) is connected on the delivery pipe (2), and the other end and the useless chlorine of the recovery tube (3) absorb
System is connected;
And the dechlorination vavuum pump (4) is connected on the delivery pipe (2), second regulating valve (41) is installed on close to institute
State the side of the entrance point of dechlorination vavuum pump (4).
2. the system of sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production according to claim 1, it is characterised in that also
Including distance-transmission pressure gauge (42), the distance-transmission pressure gauge (42) is connected with second regulating valve (41).
3. the system of sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production according to claim 2, in addition to controller,
Second regulating valve (41) and the controller are electrically connected with, and the controller is according to the pressure of the distance-transmission pressure gauge (42)
Display automatically adjusts to second regulating valve (41).
4. the system of sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production according to claim 1, it is characterised in that also
Including the 3rd regulating valve (21), the 3rd regulating valve (21) is installed on the recovery tube (3) and second regulating valve (41)
Between the delivery pipe (2) on.
5. the system of sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production according to claim 1, it is characterised in that also
Including the 4th regulating valve (31), the 4th regulating valve (31) is installed on the recovery tube (3).
6. according to the system that sodium hypochlorite reaction speed is controlled in a kind of any one of claim 1 to 5 chlor-alkali production, it is special
Levy and be, chlorine delivery pipe is the chlorine output pipe of electrolytic cell during chlor-alkali production in the chlorine production.
7. the system of sodium hypochlorite reaction speed is controlled in a kind of chlor-alkali production according to claim 6, it is characterised in that institute
The output chlorine tube for stating electrolytic cell is connected with downstream user end.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710487743.XA CN107166171A (en) | 2017-06-23 | 2017-06-23 | A kind of system that sodium hypochlorite reaction speed is controlled in chlor-alkali production |
Applications Claiming Priority (1)
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CN201710487743.XA CN107166171A (en) | 2017-06-23 | 2017-06-23 | A kind of system that sodium hypochlorite reaction speed is controlled in chlor-alkali production |
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CN107166171A true CN107166171A (en) | 2017-09-15 |
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CN201710487743.XA Pending CN107166171A (en) | 2017-06-23 | 2017-06-23 | A kind of system that sodium hypochlorite reaction speed is controlled in chlor-alkali production |
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Cited By (1)
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CN111059467A (en) * | 2019-12-17 | 2020-04-24 | 攀枝花钢企欣宇化工有限公司 | Chlorate decomposition gas pressure protection device |
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