CN107163466A - A kind of environment protecting thermal insulating material and preparation method thereof - Google Patents
A kind of environment protecting thermal insulating material and preparation method thereof Download PDFInfo
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- CN107163466A CN107163466A CN201710402385.8A CN201710402385A CN107163466A CN 107163466 A CN107163466 A CN 107163466A CN 201710402385 A CN201710402385 A CN 201710402385A CN 107163466 A CN107163466 A CN 107163466A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L29/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers
- C08L29/14—Homopolymers or copolymers of acetals or ketals obtained by polymerisation of unsaturated acetals or ketals or by after-treatment of polymers of unsaturated alcohols
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Abstract
The invention discloses a kind of environment protecting thermal insulating material and preparation method thereof, insulation material component includes 10 20 parts of polyvinyl butyral resin by weight, 5 10 parts of foam stabilizer, 8 18 parts of silicone oil, 3 10 parts of diatomite, 5 10 parts of activated carbon, 28 parts of the mica powder of lamellar structure, 4 12 parts of hollow glass micropearl, 3 10 parts of perforate expanded perlite, one 5 15 parts of fluorine dichloroethanes, 4 12 parts of dimethyl siloxane, 3 10 parts of 3 10 parts of xylitol and thickener, preparation technology of the present invention is simple, obtained insulation material high insulating effect, also have simultaneously nontoxic, insulation, the advantages of thermal conductivity is relatively low.
Description
Technical field
The present invention relates to insulation material preparing technical field, specially a kind of environment protecting thermal insulating material and preparation method thereof.
Background technology
Insulation material generally refers to the material that thermal conductivity factor is less than or equal to 0.12.Insulation material Materials quickly,
Good heat preservation technology and material are used in industry and building, can often be played a multiplier effect.Often used in building
One ton of mineral wool insulating product, can save one ton of oil for 1 year.The research and development of Abroad in Recent Years rigid foam is rapid, and
And be widely used.But domestic rigid foam is higher due to cost, relative development is slower, therefore domestic city
Field need further exploitation.And insulation material does not require nothing more than light weight, also require there is excellent compressive strength, modulus and size
Stability, with development in science and technology and the continuous improvement of living standard, environment-friendly insulating material turns into important research topic.
The content of the invention
It is an object of the invention to provide a kind of environment protecting thermal insulating material and preparation method thereof, to solve above-mentioned background technology
The problem of middle proposition.
To achieve the above object, the present invention provides following technical scheme：A kind of environment protecting thermal insulating material, insulation material component
Include 10-20 parts of polyvinyl butyral resin, 5-10 parts of foam stabilizer, 8-18 parts of silicone oil, 3-10 parts of diatomite, activity by weight
5-10 parts of charcoal, 4-12 parts of 2-8 parts of mica powder, the hollow glass micropearl of lamellar structure, 3-10 parts of perforate expanded perlite, a fluorine two
3-10 parts of 5-15 parts of chloroethanes, 4-12 parts of dimethyl siloxane, 3-10 parts of xylitol and thickener.
It is preferred that, composition proportion preferably is：15 parts of polyvinyl butyral resin, 8 parts of foam stabilizer, 13 parts of silicone oil, diatomite 7
Part, 8 parts of activated carbon, 8 parts of 5 parts of mica powder, the hollow glass micropearl of lamellar structure, 7 parts of perforate expanded perlite, the chloroethene of a fluorine two
7 parts of 10 parts of alkane, 8 parts of dimethyl siloxane, 7 parts of xylitol and thickener.
It is preferred that, its preparation method comprises the following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation technology of the present invention is simple, and obtained insulation material is protected
Temp effect is good, while also having nontoxic, insulation, the advantages of thermal conductivity is relatively low；It is very beneficial for industrialized production, fits
In popularization and application.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
The present invention provides following technical scheme：A kind of environment protecting thermal insulating material, insulation material component includes by weight
10-20 parts of polyvinyl butyral resin, 5-10 parts of foam stabilizer, 8-18 parts of silicone oil, 3-10 parts of diatomite, 5-10 parts of activated carbon, lamella
4-12 parts of 2-8 parts of mica powder, the hollow glass micropearl of structure, 3-10 parts of perforate expanded perlite, 5-15 parts of a fluorine dichloroethanes,
3-10 parts of 4-12 parts of dimethyl siloxane, 3-10 parts of xylitol and thickener.
Embodiment one：
Insulation material component by weight include 10 parts of polyvinyl butyral resin, 5 parts of foam stabilizer, 8 parts of silicone oil, 3 parts of diatomite,
5 parts of activated carbon, 4 parts of 2 parts of mica powder, the hollow glass micropearl of lamellar structure, 3 parts of perforate expanded perlite, a fluorine dichloroethanes 5
Part, 4 parts of dimethyl siloxane, 3 parts of xylitol and 3 parts of thickener.
The preparation method of the present embodiment comprises the following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Embodiment two：
Insulation material component includes 20 parts of polyvinyl butyral resin, 10 parts of foam stabilizer, 18 parts of silicone oil, diatomite 10 by weight
Part, 10 parts of activated carbon, 12 parts of 8 parts of mica powder, the hollow glass micropearl of lamellar structure, 10 parts of perforate expanded perlite, a fluorine two
10 parts of 15 parts of chloroethanes, 12 parts of dimethyl siloxane, 10 parts of xylitol and thickener.
The preparation method of the present embodiment comprises the following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Embodiment three：
Insulation material component by weight include 12 parts of polyvinyl butyral resin, 6 parts of foam stabilizer, 9 parts of silicone oil, 4 parts of diatomite,
6 parts of activated carbon, 6 parts of 3 parts of mica powder, the hollow glass micropearl of lamellar structure, 5 parts of perforate expanded perlite, a fluorine dichloroethanes 6
Part, 5 parts of dimethyl siloxane, 4 parts of xylitol and 4 parts of thickener.
The preparation method of the present embodiment comprises the following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Example IV：
Insulation material component includes 18 parts of polyvinyl butyral resin, 9 parts of foam stabilizer, 16 parts of silicone oil, diatomite 8 by weight
Part, 9 parts of activated carbon, 11 parts of 7 parts of mica powder, the hollow glass micropearl of lamellar structure, 9 parts of perforate expanded perlite, a fluorine dichloro
9 parts of 13 parts of ethane, 11 parts of dimethyl siloxane, 9 parts of xylitol and thickener.
The preparation method of the present embodiment comprises the following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Embodiment five：
Insulation material component includes 15 parts of polyvinyl butyral resin, 8 parts of foam stabilizer, 13 parts of silicone oil, diatomite 7 by weight
Part, 8 parts of activated carbon, 8 parts of 5 parts of mica powder, the hollow glass micropearl of lamellar structure, 7 parts of perforate expanded perlite, the chloroethene of a fluorine two
7 parts of 10 parts of alkane, 8 parts of dimethyl siloxane, 7 parts of xylitol and thickener.
The preparation method of the present embodiment comprises the following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Preparation technology of the present invention is simple, obtained insulation material high insulating effect, while also having nontoxic, thermal insulation separation
Heat, the advantages of thermal conductivity is relatively low；It is very beneficial for industrialized production, suitable for popularization and application.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of environment protecting thermal insulating material, it is characterised in that：Insulation material component includes polyvinyl butyral resin by weight
10-20 parts, 5-10 parts of foam stabilizer, 8-18 parts of silicone oil, 3-10 parts of diatomite, 5-10 parts of activated carbon, the mica powder 2-8 of lamellar structure
Part, 4-12 parts of hollow glass micropearl, 3-10 parts of perforate expanded perlite, 5-15 parts of a fluorine dichloroethanes, dimethyl siloxane 4-
3-10 parts of 12 parts, 3-10 parts of xylitol and thickener.
2. a kind of environment protecting thermal insulating material according to claim 1, it is characterised in that：It is preferred that composition proportion be：Poly- second
15 parts of enol butyral, 8 parts of foam stabilizer, 13 parts of silicone oil, 7 parts of diatomite, 8 parts of activated carbon, 5 parts of the mica powder of lamellar structure, sky
8 parts of heart glass microballoon, 7 parts of perforate expanded perlite, 10 parts of a fluorine dichloroethanes, 8 parts of dimethyl siloxane, 7 parts of xylitol with
And 7 parts of thickener.
3. realize a kind of preparation method of environment protecting thermal insulating material described in claim 1, it is characterised in that：Its preparation method bag
Include following steps：
A, will polyvinyl butyral resin, foam stabilizer, silicone oil, diatomite mix after add stirred tank in be stirred, stir speed (S.S.)
For 3000 revs/min, mixing time is 30min, obtains mixture A；
B, addition activated carbon, the mica powder of lamellar structure, hollow glass micropearl, perforate expanded perlite, mixing in mixture A
Add and be stirred continuously in heating vessel in heating, heating process afterwards, heating-up temperature is 60 DEG C, and the heat time is 30min, Zhi Houhuan
Slow cool down obtains mixture B to normal temperature；
C, a fluorine dichloroethanes, dimethyl siloxane, xylitol and thickener are added in mixture B, added after mixing double
In screw extruder, extrusion temperature is 200 DEG C, as insulation material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710402385.8A CN107163466A (en) | 2017-06-01 | 2017-06-01 | A kind of environment protecting thermal insulating material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710402385.8A CN107163466A (en) | 2017-06-01 | 2017-06-01 | A kind of environment protecting thermal insulating material and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107163466A true CN107163466A (en) | 2017-09-15 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710402385.8A Pending CN107163466A (en) | 2017-06-01 | 2017-06-01 | A kind of environment protecting thermal insulating material and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111140155A (en) * | 2019-12-30 | 2020-05-12 | 江苏黑马森田机器人有限公司 | High-strength zipper type quick door |
| CN111140131A (en) * | 2019-12-30 | 2020-05-12 | 江苏黑马森田机器人有限公司 | High-strength hard high-speed door |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1072645A1 (en) * | 1999-07-30 | 2001-01-31 | A.W. Faber- Castell Unternehmensverwaltung GmbH & Co. | Composite material |
| CN102304261A (en) * | 2011-07-29 | 2012-01-04 | 常州大学 | Transparent heat-insulation polyvinyl alcohol poly-butyraldehyde nanocomposite and preparation method thereof |
| CN104194222A (en) * | 2014-09-17 | 2014-12-10 | 江苏欣润塑胶有限公司 | Heat-conducting composite plastic with insulation function |
| CN106587752A (en) * | 2016-12-19 | 2017-04-26 | 青岛巨能管道设备有限公司 | Heat-insulation coating material |
-
2017
- 2017-06-01 CN CN201710402385.8A patent/CN107163466A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1072645A1 (en) * | 1999-07-30 | 2001-01-31 | A.W. Faber- Castell Unternehmensverwaltung GmbH & Co. | Composite material |
| CN102304261A (en) * | 2011-07-29 | 2012-01-04 | 常州大学 | Transparent heat-insulation polyvinyl alcohol poly-butyraldehyde nanocomposite and preparation method thereof |
| CN104194222A (en) * | 2014-09-17 | 2014-12-10 | 江苏欣润塑胶有限公司 | Heat-conducting composite plastic with insulation function |
| CN106587752A (en) * | 2016-12-19 | 2017-04-26 | 青岛巨能管道设备有限公司 | Heat-insulation coating material |
Non-Patent Citations (2)
| Title |
|---|
| 李远才等: "《铸造造型材料实用手册》", 30 June 2015, 机械工业出版社 * |
| 陈玉成: "《秦皇岛市科学技术志》", 31 December 1994, 中国科学技术出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111140155A (en) * | 2019-12-30 | 2020-05-12 | 江苏黑马森田机器人有限公司 | High-strength zipper type quick door |
| CN111140131A (en) * | 2019-12-30 | 2020-05-12 | 江苏黑马森田机器人有限公司 | High-strength hard high-speed door |
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Application publication date: 20170915 |
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