CN107156854A - A kind of preparation method of multielement folic acid - Google Patents
A kind of preparation method of multielement folic acid Download PDFInfo
- Publication number
- CN107156854A CN107156854A CN201710357345.6A CN201710357345A CN107156854A CN 107156854 A CN107156854 A CN 107156854A CN 201710357345 A CN201710357345 A CN 201710357345A CN 107156854 A CN107156854 A CN 107156854A
- Authority
- CN
- China
- Prior art keywords
- parts
- folic acid
- multielement
- add
- spinach
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 title claims abstract description 62
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 229960000304 folic acid Drugs 0.000 title claims abstract description 31
- 235000019152 folic acid Nutrition 0.000 title claims abstract description 31
- 239000011724 folic acid Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 235000009337 Spinacia oleracea Nutrition 0.000 claims abstract description 19
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 17
- 239000011573 trace mineral Substances 0.000 claims abstract description 17
- 244000298715 Actinidia chinensis Species 0.000 claims abstract description 13
- 235000009434 Actinidia chinensis Nutrition 0.000 claims abstract description 13
- 235000009436 Actinidia deliciosa Nutrition 0.000 claims abstract description 13
- 235000005979 Citrus limon Nutrition 0.000 claims abstract description 13
- 244000131522 Citrus pyriformis Species 0.000 claims abstract description 13
- 244000000626 Daucus carota Species 0.000 claims abstract description 13
- 235000002767 Daucus carota Nutrition 0.000 claims abstract description 13
- 241000238557 Decapoda Species 0.000 claims abstract description 13
- 244000068988 Glycine max Species 0.000 claims abstract description 13
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 13
- 235000021028 berry Nutrition 0.000 claims abstract description 13
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 9
- 239000011575 calcium Substances 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 244000300264 Spinacia oleracea Species 0.000 claims abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 239000008367 deionised water Substances 0.000 claims description 18
- 229910021641 deionized water Inorganic materials 0.000 claims description 18
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 18
- 150000003839 salts Chemical class 0.000 claims description 13
- 239000000843 powder Substances 0.000 claims description 12
- 239000012266 salt solution Substances 0.000 claims description 11
- 235000001465 calcium Nutrition 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 239000005445 natural material Substances 0.000 abstract description 2
- 238000003672 processing method Methods 0.000 abstract description 2
- 238000000605 extraction Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 241000219315 Spinacia Species 0.000 description 15
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of preparation method of multielement folic acid, mainly include the following steps that：A, natural folic acid and other trace elements are extracted from the leaf of spinach, Kiwi berry, lemon and carrot；B, extraction calcium and its trace element from dried shrimp and soybean；C, centrifugal filtration, adjust pH value；Graininess is made after D, drying, carry out disinfection packaging, processing method of the present invention is simple, and processing cost is low, the natural folic acid extracted using natural material, content is high, green safety high into yield, calcium and trace element are more, and stability is strong, are easy to storage.
Description
Technical field
The present invention relates to a kind of preparation method of multielement folic acid.
Background technology
Folic acid needs to absorb certain content daily, but eat as the indispensable trace element of the mankind particularly pregnant woman
It is less that water fruits and vegetables can be obtained, and nutrition leak is fast, so it is the important topic studied now therefrom to extract nutriment, by
Structure therein, great unstability will be destroyed by running into high temperature in folic acid, so also to extract to make certain difficulty.
The content of the invention
It is an object of the invention to provide a kind of preparation method of multielement folic acid, to solve to propose in above-mentioned background technology
The problem of.
To achieve the above object, the present invention provides following technical scheme：A kind of preparation method of multielement folic acid, main bag
Include following steps：
A kind of preparation method of multielement folic acid, it is characterised in that：Mainly include the following steps that：
A, fresh the leaf of spinach is taken, the leaf of spinach after cleaning and Kiwi berry, lemon and carrot after peeling put into squeezing together
Squeezed the juice in juice machine, add supercritical liq and folic acid and its trace element are extracted from mixed liquor, temperature is set to 30-50 DEG C；
B, add deionized water to be squeezed the juice the dried shrimp and soybean, calcium and trace element are extracted from mixture, temperature is set to 40-
60℃；
C, the product in mixture A, B mixed, add in centrifuge and shake, rotating speed is 6000-9000r/min, filtering
Go out after liquid to add appropriate salt solution regulation pH value, keep PH 4.0 ~ 5.0；
D, the mixture in step C carried out to be dried into white powder, temperature is 50-75 DEG C, by the powder after drying according to
A diameter of 0.5-1cm white particle is made in grinding tool, and it is carried out disinfection using ultraviolet ray sterilizer and packed after 5-10min
Into.
It is preferred that, multielement folic acid component includes by weight in the step：150-200 parts of the leaf of spinach, Kiwi berry
60-80 parts, 20-40 parts of lemon, 80-120 parts of carrot, 35-50 parts of supercritical liq, 60-80 parts of dried shrimp, 80-120 parts of soybean,
1-3 parts of salt, deionized water 200-300.
It is preferred that, what the salt solution in the step C was allocated by appropriate salt and deionized water, concentration is 1mol/L.
Compared with prior art, the beneficial effects of the invention are as follows：Processing method of the present invention is simple, and processing cost is low, uses
The natural folic acid that natural material is extracted, content is high, high into yield, green safety, and calcium and trace element are more, and stability
By force, it is easy to storage.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
Embodiment one：
A kind of preparation method of multielement folic acid, is mainly included the following steps that：
A, fresh the leaf of spinach is taken, the leaf of spinach after cleaning and Kiwi berry, lemon and carrot after peeling put into squeezing together
Squeezed the juice in juice machine, add supercritical liq and folic acid and its trace element are extracted from mixed liquor, temperature is set to 40 DEG C；
B, add deionized water to be squeezed the juice the dried shrimp and soybean, calcium and trace element are extracted from mixture, temperature is set to 50
℃；
C, the product in mixture A, B mixed, add in centrifuge and shake, rotating speed is 7000r/min, filters out liquid
After add appropriate salt solution regulation pH value, keep PH 4.0 ~ 5.0；
D, the mixture in step C carried out to be dried into white powder, temperature is 65 DEG C, by the powder after drying according to grinding tool
A diameter of 0.5cm white particle is made, it is carried out disinfection to pack after 8min using ultraviolet ray sterilizer completes.
In the present embodiment, multielement folic acid component includes by weight in the step：150 parts of the leaf of spinach, Kiwi berry
80 parts, 40 parts of lemon, 80 parts of carrot, 50 parts of supercritical liq, 80 parts of dried shrimp, 80 parts of soybean, 2 parts of salt, 200 parts of deionized water.
In the present embodiment, what the salt solution in step C was allocated by appropriate salt and deionized water, concentration is 1mol/L.
Embodiment two：
A kind of preparation method of multielement folic acid, is mainly included the following steps that：
A, fresh the leaf of spinach is taken, the leaf of spinach after cleaning and Kiwi berry, lemon and carrot after peeling put into squeezing together
Squeezed the juice in juice machine, add supercritical liq and folic acid and its trace element are extracted from mixed liquor, temperature is set to 30 DEG C；
B, add deionized water to be squeezed the juice the dried shrimp and soybean, calcium and trace element are extracted from mixture, temperature is set to 60
℃；
C, the product in mixture A, B mixed, add in centrifuge and shake, rotating speed is 9000r/min, filters out liquid
After add appropriate salt solution regulation pH value, keep PH 4.0 ~ 5.0；
D, the mixture in step C carried out to be dried into white powder, temperature is 75 DEG C, by the powder after drying according to grinding tool
A diameter of 1cm white particle is made, it is carried out disinfection to pack after 10min using ultraviolet ray sterilizer completes.
In the present embodiment, multielement folic acid component includes by weight in the step：200 parts of the leaf of spinach, Kiwi berry
80 parts, 40 parts of lemon, 100 parts of carrot, 40 parts of supercritical liq, 70 parts of dried shrimp, 100 parts of soybean, 2 parts of salt, deionized water 300
Part.
In the present embodiment, what the salt solution in step C was allocated by appropriate salt and deionized water, concentration is 1mol/L.
Embodiment three：
A kind of preparation method of multielement folic acid, is mainly included the following steps that：
A, fresh the leaf of spinach is taken, the leaf of spinach after cleaning and Kiwi berry, lemon and carrot after peeling put into squeezing together
Squeezed the juice in juice machine, add supercritical liq and folic acid and its trace element are extracted from mixed liquor, temperature is set to 40 DEG C；
B, add deionized water to be squeezed the juice the dried shrimp and soybean, calcium and trace element are extracted from mixture, temperature is set to 50
℃；
C, the product in mixture A, B mixed, add in centrifuge and shake, rotating speed is 6000r/min, filters out liquid
After add appropriate salt solution regulation pH value, keep PH 4.0 ~ 5.0；
D, the mixture in step C carried out to be dried into white powder, temperature is 75 DEG C, by the powder after drying according to grinding tool
A diameter of 1cm white particle is made, it is carried out disinfection to pack after 10min using ultraviolet ray sterilizer completes.
In the present embodiment, multielement folic acid component includes by weight in the step：175 parts of the leaf of spinach, Kiwi berry
65 parts, 24 parts of lemon, 105 parts of carrot, 40 parts of supercritical liq, 77 parts of dried shrimp, 110 parts of soybean, 3 parts of salt, deionized water 300
Part.
In the present embodiment, what the salt solution in step C was allocated by appropriate salt and deionized water, concentration is 1mol/L.
Example IV：
A kind of preparation method of multielement folic acid, is mainly included the following steps that：
A, fresh the leaf of spinach is taken, the leaf of spinach after cleaning and Kiwi berry, lemon and carrot after peeling put into squeezing together
Squeezed the juice in juice machine, add supercritical liq and folic acid and its trace element are extracted from mixed liquor, temperature is set to 35 DEG C；
B, add deionized water to be squeezed the juice the dried shrimp and soybean, calcium and trace element are extracted from mixture, temperature is set to 40
℃；
C, the product in mixture A, B mixed, add in centrifuge and shake, rotating speed is 9000r/min, filters out liquid
After add appropriate salt solution regulation pH value, keep PH 4.0 ~ 5.0；
D, the mixture in step C carried out to be dried into white powder, temperature is 60 DEG C, by the powder after drying according to grinding tool
A diameter of 0.7cm white particle is made, it is carried out disinfection to pack after 8min using ultraviolet ray sterilizer completes.
In the present embodiment, multielement folic acid component includes by weight in the step：170 parts of the leaf of spinach, Kiwi berry
75 parts, 25 parts of lemon, 120 parts of carrot, 50 parts of supercritical liq, 80 parts of dried shrimp, 120 parts of soybean, 2 parts of salt, deionized water 250
Part.
In the present embodiment, what the salt solution in step C was allocated by appropriate salt and deionized water, concentration is 1mol/L.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of preparation method of multielement folic acid, it is characterised in that：Mainly include the following steps that：
A, fresh the leaf of spinach is taken, the leaf of spinach after cleaning and Kiwi berry, lemon and carrot after peeling put into squeezing together
Squeezed the juice in juice machine, add supercritical liq and folic acid and its trace element are extracted from mixed liquor, temperature is set to 30-50 DEG C；
B, add deionized water to be squeezed the juice the dried shrimp and soybean, calcium and trace element are extracted from mixture, temperature is set to 40-
60℃；
C, the product in mixture A, B mixed, add in centrifuge and shake, rotating speed is 6000-9000r/min, filtering
Go out after liquid to add appropriate salt solution regulation pH value, keep PH 4.0 ~ 5.0；
D, the mixture in step C carried out to be dried into white powder, temperature is 50-75 DEG C, by the powder after drying according to
A diameter of 0.5-1cm white particle is made in grinding tool, and it is carried out disinfection using ultraviolet ray sterilizer and packed after 5-10min
Into.
2. a kind of preparation method of multielement folic acid according to claim 1, it is characterised in that：Multielement in the step
Folic acid component includes by weight：150-200 parts of the leaf of spinach, 60-80 parts of Kiwi berry, 20-40 parts of lemon, carrot 80-120
Part, 35-50 parts of supercritical liq, 60-80 parts of dried shrimp, 80-120 parts of soybean, 1-3 parts of salt, deionized water 200-300.
3. a kind of preparation method of multielement folic acid according to claim 1, it is characterised in that：Salt in the step C
Water is allocated by appropriate salt and deionized water, and concentration is 1mol/L.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710357345.6A CN107156854A (en) | 2017-05-19 | 2017-05-19 | A kind of preparation method of multielement folic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710357345.6A CN107156854A (en) | 2017-05-19 | 2017-05-19 | A kind of preparation method of multielement folic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107156854A true CN107156854A (en) | 2017-09-15 |
Family
ID=59816739
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710357345.6A Pending CN107156854A (en) | 2017-05-19 | 2017-05-19 | A kind of preparation method of multielement folic acid |
Country Status (1)
| Country | Link |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106083857A (en) * | 2016-06-06 | 2016-11-09 | 大连民族大学 | A kind of method extracting folic acid from Actinidia arguta Sieb.et Zucc |
| CN106518878A (en) * | 2016-10-14 | 2017-03-22 | 天津理工大学 | Method for extracting folic acid from spinach leaf powder |
-
2017
- 2017-05-19 CN CN201710357345.6A patent/CN107156854A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106083857A (en) * | 2016-06-06 | 2016-11-09 | 大连民族大学 | A kind of method extracting folic acid from Actinidia arguta Sieb.et Zucc |
| CN106518878A (en) * | 2016-10-14 | 2017-03-22 | 天津理工大学 | Method for extracting folic acid from spinach leaf powder |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170915 |
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