CN107151113A - A kind of preparation method of novel energy-saving environment-friendly building materials - Google Patents
A kind of preparation method of novel energy-saving environment-friendly building materials Download PDFInfo
- Publication number
- CN107151113A CN107151113A CN201710543753.0A CN201710543753A CN107151113A CN 107151113 A CN107151113 A CN 107151113A CN 201710543753 A CN201710543753 A CN 201710543753A CN 107151113 A CN107151113 A CN 107151113A
- Authority
- CN
- China
- Prior art keywords
- mixture
- preparation
- powder
- building materials
- starch
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/28—Polysaccharides or derivatives thereof
- C04B26/285—Cellulose or derivatives thereof
Abstract
The present invention provides a kind of preparation method of novel energy-saving environment-friendly building materials, comprises the following steps:First, nano-oxide is added dispersion machine stirring to preheat, refractory material, which is slowly added into dispersion machine scattered stirring, obtains mixture one;2nd, SiO 2 powder and Neon SiC powder are taken, to silica and silicon carbide powder using absolute ethyl alcohol as decentralized medium, mixture two is obtained after disperseing;3rd, mixture three is obtained after adding water-soluble binder hydroxypropyl methyl cellulose, ball milling into mixture two;4th, mixture three is poured into powder dish, drying, sieving obtain mixture four after grinding;5th, mixture one, mixture four are well mixed with modified starch, it is compressing.Building material cost prepared by the present invention is cheap, and preparation method is simple, preparation method energy-saving and emission-reduction, and preparing product also has extraordinary fire resistance.
Description
Technical field
The invention belongs to building material technical field, and in particular to a kind of preparation method of novel energy-saving environment-friendly building materials.
Background technology
After 1970s, world climate warms, and earth energy is increasingly exhausted.In AND ENERGY RESOURCES CONSUMPTION IN CHINA, energy is built
Consumption accounts for the 30-40% of mankind's energy resource consumption, and it is to save the energy, raising building to use function to improve building heat preserving heat-proof quality
Important channel.Insulating moulding coating, which is applied over building surface, can effectively reduce the temperature of building surface and inside.In recent years,
With the popularization of building energy conservation, the advantages of insulating moulding coating is because of economy, convenient and good heat-insulation effect is increasingly paid close attention to by people.
Therefore, daily life of new, the compound insulating mold coating to the mankind is researched and developed to be of great immediate significance.
Existing insulating mold coating mainly uses organic polymeric emulsions, cenosphere, porous filler and heat reflection
The heat-insulated color stuffing such as material reaches the purpose of insulation, water proof anti-soil, a kind of as disclosed in Chinese patent ZL99114454.6
A kind of aquosity elastic heat preserving insulating paint and preparation method thereof disclosed in antiradiation insulating moulding coating, ZL200710075800.X,
Insulating mold coating disclosed in ZL200910061883.6, a kind of insulating moulding coating and its use disclosed in ZL200510000149.0
On the way, a kind of insulating moulding coating for reflecting sun heat ray etc. disclosed in ZL200710035834.6.Its Patent
A kind of insulating moulding coating for reflecting sun heat ray is made up of bottom-coating and painting coating disclosed in ZL200710035834.6, bottom
Apply and be made of hollow beads heat-barrier material, heat-reflecting material and macromolecule resin;Face is applied reflects heat ray using Surface coating
Composite, heat-reflecting material and macromolecule resin are made, due to containing a large amount of-C=0,-C-0-C, -0H in organic polymer
Deng extinction group, inorganic color stuffing is higher than to the degree of absorption of sunshine, so when the addition of organic polymeric emulsions
When bigger, film is also bigger to the uptake of sunshine, and the thermal conductivity factor of film also can be improved accordingly, can reduce the heat-insulated of coating
Effect.In order to reach the basic physical and chemical properties requirement of common exterior coating, this kind of existing traditional insulating moulding coating must be protected
Higher addition of the organic polymeric emulsions in coating is demonstrate,proved, causes its effect of heat insulation undesirable.And without cracking resistance,
Receive many restrictions in use.
In summary, it is therefore desirable to which a kind of construction material of more preferable energy-conserving and environment-protective improves the deficiencies in the prior art, pushes away
The development of dynamic building trade.
The content of the invention
It is an object of the invention to provide a kind of preparation method of novel energy-saving environment-friendly building materials, lower cost for material of the present invention,
Preparation method is simple, and the graphene of addition can greatly promote the fusion performance of building materials, with extraordinary fire-retardant, crack resistance
Can, and the toughness and durability of the building materials are far longer than like product present in the market.
The invention provides following technical scheme:
A kind of preparation method of novel energy-saving environment-friendly building materials, comprises the following steps:
First, at 80-120 DEG C of dispersion machine temperature, nano-oxide is added dispersion machine stirring preheating 10-15min, dispersion machine is adjusted
Turn over speed is 800-1000rpm/min, and refractory material is slowly added into dispersion machine, disperses stirring 40-50min, is mixed
Compound one;
2nd, SiO 2 powder and Neon SiC powder are weighed in mass ratio, to the silica and carborundum powder weighed
End obtains mixture two using absolute ethyl alcohol as decentralized medium after disperseing;
3rd, water-soluble binder hydroxypropyl methyl cellulose is added into mixture two, using agate ball as abrading-ball, is carried out after ball milling
Obtain mixture three;
4th, mixture three is poured into powder dish together with agate abrading-ball, dries, sieves at 100-130 DEG C, take out agate
Mixture four is obtained after abrading-ball, grinding;
5th, mixture one, mixture four are well mixed with modified starch, it is compressing.
It is preferred that, the novel energy-saving environment-friendly building materials include the raw material of following parts by weight:It is 15-25 parts of nano-oxide, resistance to
Fiery material 22-34 parts, 20-30 parts of SiO 2 powder, 20-38 parts of Neon SiC powder, 10-23 parts of absolute ethyl alcohol, hydroxypropyl
23-27 parts of 22-32 parts of ylmethyl cellulose and modified starch.
It is preferred that, the nano-oxide of the step one is the zinc oxide with microcellular structure, magnesia, aluminum oxide, α oxygen
Change mixing any one or more in iron, titanium oxide and silica, the composition is with low cost, wide material sources, prepare simple.
It is preferred that, the refractory material of the step one is waste old ceramics roller rod or waste and old high alumina ceramic ball.
It is preferred that, the mass ratio of SiO 2 powder, silicon carbide powder and absolute ethyl alcohol that the step 2 is weighed is 4:
25, and the ultrasonic disperse 30-50min on supersonic cleaning machine, the proportioning and method are conducive to being more fully mixed composition, improved
Stock utilization, shortens the time prepared, improves preparation efficiency.
It is preferred that, the modified starch of the step 5 can be watered be configured to concentration be 30-35% starch milk mixed,
This method is conducive to components utilising more abundant.
It is preferred that, the modified starch of the step 5 is the acetate starch containing ester group, CPC 3005X, amino first
In acid esters starch, Succic Acid Ester Starch, phosphate ester starch, octenyl succinate starch and dodecenylsuccinic anhydride starch
Any one or more mixing.
It is preferred that, stand 2-3 days after the step 5 is compressing.
The beneficial effects of the invention are as follows:
The nano-oxide of the step one of the present invention is the zinc oxide with microcellular structure, magnesia, aluminum oxide, α iron oxide, oxygen
Change mixing any one or more in titanium and silica, the composition is with low cost, wide material sources, prepare simple.
The mass ratio of SiO 2 powder, silicon carbide powder and absolute ethyl alcohol that the step two of the present invention is weighed is 4:25,
And on supersonic cleaning machine ultrasonic disperse 30-50min, the proportioning and method be conducive to being more fully mixed composition, improves material
Expect utilization rate, shorten the time prepared, improve preparation efficiency.
The present invention step five modified starch can be watered be configured to concentration be 30-35% starch milk mixed, the party
Method is conducive to components utilising more abundant.
Lower cost for material of the present invention, preparation method is simple, and the graphene of addition can greatly promote the amalgamation of building materials
Can, raw material are not have the waste of resource and the transition of energy consumption in environment-friendly materials, preparation process, and the product of preparation also has
There is an extraordinary fire-retardant, cracking resistance, and the toughness and durability of the building materials are far longer than similar production present in the market
Product.
Embodiment
Embodiment 1
A kind of preparation method of novel energy-saving environment-friendly building materials, comprises the following steps:
First, at 120 DEG C of dispersion machine temperature, nano-oxide is added dispersion machine stirring preheating 14min, dispersion machine turn over speed is adjusted
For 1000rpm/min, refractory material is slowly added into dispersion machine, disperses stirring 50min, obtains mixture one;
2nd, SiO 2 powder and Neon SiC powder are weighed in mass ratio, to the silica and carborundum powder weighed
End obtains mixture two using absolute ethyl alcohol as decentralized medium after disperseing;
3rd, water-soluble binder hydroxypropyl methyl cellulose is added into mixture two, using agate ball as abrading-ball, is carried out after ball milling
Obtain mixture three;
4th, mixture three is poured into powder dish together with agate abrading-ball, dries, sieves at 130 DEG C, take out agate mill
Mixture four is obtained after ball, grinding;
5th, mixture one, mixture four are well mixed with modified starch, it is compressing.
Novel energy-saving environment-friendly building materials include the raw material of following parts by weight:25 parts of nano-oxide, 34 parts of refractory material, dioxy
30 parts of SiClx powder, 38 parts of Neon SiC powder, 13 parts of absolute ethyl alcohol, 22 parts of hydroxypropyl methyl cellulose and modified starch 27
Part.
The nano-oxide of step one is the zinc oxide with microcellular structure, magnesia, aluminum oxide, α iron oxide, titanium oxide
With mixing any one or more in silica, the composition is with low cost, wide material sources, prepares simple.
The refractory material of step one is waste old ceramics roller rod or waste and old high alumina ceramic ball.
The mass ratio of SiO 2 powder, silicon carbide powder and absolute ethyl alcohol that step 2 is weighed is 4:25, and in ultrasound
Ultrasonic disperse 50min on cleaning machine, the proportioning and method are conducive to being more fully mixed composition, improve stock utilization, contracting
The time of short preparation, improve preparation efficiency.
The modified starch of step 5 can be watered be configured to concentration be 30% starch milk mixed, this method is conducive into
Divide using more abundant.
The modified starch of step 5 is the acetate starch containing ester group, CPC 3005X, carbamate starch, fourth
Two acid esters starch, phosphate ester starch, the mixing of octenyl succinate starch and dodecenylsuccinic anhydride starch.
3 days are stood after step 5 is compressing.
Embodiment 2
A kind of preparation method of novel energy-saving environment-friendly building materials, comprises the following steps:
First, at 120 DEG C of dispersion machine temperature, nano-oxide is added dispersion machine stirring preheating 15min, dispersion machine turn over speed is adjusted
For 1000rpm/min, refractory material is slowly added into dispersion machine, disperses stirring 50min, obtains mixture one;
2nd, SiO 2 powder and Neon SiC powder are weighed in mass ratio, to the silica and carborundum powder weighed
End obtains mixture two using absolute ethyl alcohol as decentralized medium after disperseing;
3rd, water-soluble binder hydroxypropyl methyl cellulose is added into mixture two, using agate ball as abrading-ball, is carried out after ball milling
Obtain mixture three;
4th, mixture three is poured into powder dish together with agate abrading-ball, dries, sieves at 130 DEG C, take out agate mill
Mixture four is obtained after ball, grinding;
5th, mixture one, mixture four are well mixed with modified starch, it is compressing.
Novel energy-saving environment-friendly building materials include the raw material of following parts by weight:15 parts of nano-oxide, 22 parts of refractory material, dioxy
20 parts of SiClx powder, 28 parts of Neon SiC powder, 10 parts of absolute ethyl alcohol, 22 parts of hydroxypropyl methyl cellulose and modified starch 23
Part.
The nano-oxide of step one is the zinc oxide with microcellular structure, magnesia, aluminum oxide, α iron oxide, titanium oxide
With the mixing of silica, the composition is with low cost, wide material sources, prepares simple.
The refractory material of step one is waste old ceramics roller rod or waste and old high alumina ceramic ball.
The mass ratio of SiO 2 powder, silicon carbide powder and absolute ethyl alcohol that step 2 is weighed is 4:25, and in ultrasound
Ultrasonic disperse 30min on cleaning machine, the proportioning and method are conducive to being more fully mixed composition, improve stock utilization, contracting
The time of short preparation, improve preparation efficiency.
The modified starch of step 5 can be watered be configured to concentration be 30% starch milk mixed, this method is conducive into
Divide using more abundant.
The modified starch of step 5 is the acetate starch containing ester group, CPC 3005X, carbamate starch, fourth
Two acid esters starch, phosphate ester starch, the mixing of octenyl succinate starch and dodecenylsuccinic anhydride starch.
2 days are stood after step 5 is compressing.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality
Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention
God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (8)
1. a kind of preparation method of novel energy-saving environment-friendly building materials, it is characterised in that comprise the following steps:
First, at 80-120 DEG C of dispersion machine temperature, nano-oxide is added dispersion machine stirring preheating 10-15min, dispersion machine is adjusted
Turn over speed is 800-1000rpm/min, and refractory material is slowly added into dispersion machine, disperses stirring 40-50min, is mixed
Compound one;
2nd, SiO 2 powder and Neon SiC powder are weighed in mass ratio, to the silica and carborundum powder weighed
End obtains mixture two using absolute ethyl alcohol as decentralized medium after disperseing;
3rd, water-soluble binder hydroxypropyl methyl cellulose is added into mixture two, using agate ball as abrading-ball, is carried out after ball milling
Obtain mixture three;
4th, mixture three is poured into powder dish together with agate abrading-ball, dries, sieves at 100-130 DEG C, take out agate
Mixture four is obtained after abrading-ball, grinding;
5th, mixture one, mixture four are well mixed with modified starch, it is compressing.
2. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 1, it is characterised in that the new section
Energy environment-friendly building materials include the raw material of following parts by weight:15-25 parts of nano-oxide, 22-34 parts of refractory material, SiO 2 powder
20-30 parts, 20-38 parts of Neon SiC powder, 10-23 parts of absolute ethyl alcohol, 22-32 parts of hydroxypropyl methyl cellulose and modified shallow lake
23-27 parts of powder.
3. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 2, it is characterised in that the step one
Nano-oxide be the zinc oxide with microcellular structure, magnesia, aluminum oxide, α iron oxide, titanium oxide and silica in it is any
Plant or a variety of mixing.
4. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 3, it is characterised in that the step one
Refractory material be waste old ceramics roller rod or waste and old high alumina ceramic ball.
5. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 1, it is characterised in that the step 2
The mass ratio of the SiO 2 powder, silicon carbide powder and the absolute ethyl alcohol that weigh is 4:25, and the ultrasound point on supersonic cleaning machine
Dissipate 30-50min.
6. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 1, it is characterised in that the step 5
Modified starch can be watered be configured to concentration be 30-35% starch milk mixed.
7. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 1, it is characterised in that the step 5
Modified starch be the acetate starch containing ester group, CPC 3005X, carbamate starch, Succic Acid Ester Starch, phosphorus
Any of acid esters starch, octenyl succinate starch and dodecenylsuccinic anhydride starch or a variety of mixing.
8. a kind of preparation method of novel energy-saving environment-friendly building materials according to claim 1, it is characterised in that the step 5
2-3 days are stood after compressing.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710543753.0A CN107151113A (en) | 2017-07-05 | 2017-07-05 | A kind of preparation method of novel energy-saving environment-friendly building materials |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710543753.0A CN107151113A (en) | 2017-07-05 | 2017-07-05 | A kind of preparation method of novel energy-saving environment-friendly building materials |
Publications (1)
Publication Number | Publication Date |
---|---|
CN107151113A true CN107151113A (en) | 2017-09-12 |
Family
ID=59795216
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710543753.0A Withdrawn CN107151113A (en) | 2017-07-05 | 2017-07-05 | A kind of preparation method of novel energy-saving environment-friendly building materials |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN107151113A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108035504A (en) * | 2017-12-29 | 2018-05-15 | 丰城铭雪智能环保装饰材料有限公司 | A kind of calcium sulfate floor |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102795805A (en) * | 2012-08-02 | 2012-11-28 | 成都新柯力化工科技有限公司 | Energy-saving phase-change constant-temperature building material and preparation method thereof |
CN103121813A (en) * | 2013-01-28 | 2013-05-29 | 熊建珍 | EPS (polystyrene foam) insulating building board and preparation technology thereof |
CN104877496A (en) * | 2015-04-24 | 2015-09-02 | 安徽华强防水防腐材料有限公司 | Important component of crack-resistant insulated flame-retardant building material coating |
CN106751273A (en) * | 2016-12-14 | 2017-05-31 | 四川熹玥广告传媒有限公司 | A kind of environmental protection and energy saving material and preparation method thereof |
-
2017
- 2017-07-05 CN CN201710543753.0A patent/CN107151113A/en not_active Withdrawn
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102795805A (en) * | 2012-08-02 | 2012-11-28 | 成都新柯力化工科技有限公司 | Energy-saving phase-change constant-temperature building material and preparation method thereof |
CN103121813A (en) * | 2013-01-28 | 2013-05-29 | 熊建珍 | EPS (polystyrene foam) insulating building board and preparation technology thereof |
CN104877496A (en) * | 2015-04-24 | 2015-09-02 | 安徽华强防水防腐材料有限公司 | Important component of crack-resistant insulated flame-retardant building material coating |
CN106751273A (en) * | 2016-12-14 | 2017-05-31 | 四川熹玥广告传媒有限公司 | A kind of environmental protection and energy saving material and preparation method thereof |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108035504A (en) * | 2017-12-29 | 2018-05-15 | 丰城铭雪智能环保装饰材料有限公司 | A kind of calcium sulfate floor |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104877496B (en) | Crack-resistant insulated flame-retardant building material coating | |
CN107163855B (en) | A kind of silica aerogel reflective insulation exterior wall paint and preparation method thereof | |
CN102533011B (en) | Thermosetting reflection thermal insulation coating and preparation method thereof | |
CN103497559B (en) | Weather resistant exterior wall putty powder | |
CN105860717B (en) | Colour reflective insulating moulding coating and its preparation, construction method | |
CN102826810B (en) | Reflective heat-insulation powder coating and preparation method thereof | |
CN106588108A (en) | Building heat preservation material | |
CN106590133B (en) | A kind of building inside and outside wall powder of lacquer putty for use on and preparation method thereof | |
CN107987601A (en) | A kind of two-component insulation putty for architectural exterior wall and preparation method thereof | |
CN108795200A (en) | Lightweight complex building heat insulating coatings and preparation method thereof | |
CN107474672A (en) | A kind of Elastic anti-crack artificial granite heat reflection coatings and preparation method thereof | |
CN107500647A (en) | A kind of ceramic microsphere energy-saving ceramic tile glue and preparation method thereof | |
CN106752239A (en) | A kind of outer wall flexible water proof putty and preparation method thereof | |
CN111233415A (en) | Anti-cracking gypsum-based plastering mortar and preparation method thereof | |
CN107446404A (en) | A kind of external thermal insulation wall surface water proof flexible material | |
CN104387885A (en) | Natural-fiber-added anti-aging high-weather-resistance outer wall paint and preparation method thereof | |
CN107226675A (en) | A kind of preparation method of the fire-retardant building materials of novel energy-conserving | |
CN108821675A (en) | A kind of kervit microbead insulated sand slurry and preparation method thereof | |
CN107352909A (en) | Celular glass insulating system special plastering rubber cement and preparation method thereof and application method | |
CN107151113A (en) | A kind of preparation method of novel energy-saving environment-friendly building materials | |
CN108410245A (en) | A kind of heat insulating inner wall putty and preparation method | |
CN107828337A (en) | A kind of high-performance heat insulating coatings | |
CN101845276A (en) | Acidproof latex paint and preparation method thereof | |
CN104927502A (en) | Important component factor for elastic building-material heat-insulation weather-resistant waterproof coating | |
CN106830979A (en) | A kind of imitative volcanic rock porous material |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170912 |
|
WW01 | Invention patent application withdrawn after publication |