CN107151007A - A kind of regeneration technology of printer waste carbon powder - Google Patents
A kind of regeneration technology of printer waste carbon powder Download PDFInfo
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- CN107151007A CN107151007A CN201710566190.7A CN201710566190A CN107151007A CN 107151007 A CN107151007 A CN 107151007A CN 201710566190 A CN201710566190 A CN 201710566190A CN 107151007 A CN107151007 A CN 107151007A
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- Prior art keywords
- carbon dust
- carbon powder
- carbon
- specific method
- regeneration
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Processing Of Solid Wastes (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
- Cleaning In Electrography (AREA)
Abstract
The invention belongs to printer field of material technology there is provided a kind of regeneration technology of printer waste carbon powder, it is specially：（1）, waste carbon powder regeneration：Waste carbon powder filtered, is dehydrated, being separated, mix it is outer add thing, secondary filter, obtain regeneration carbon dust；（2）, carbon dust purification：By wet purification, application of vacuum and high-temperature calcination, high-purity carbon dust is prepared.The present invention can effectively improve carbon dust and recycle efficiency and purity, reduce the pollution to environment.
Description
Technical field
The invention belongs to printer field of material technology, specifically, a kind of regeneration technology of printer waste carbon powder.
Background technology
Toner cartridge is the common construction store of laser printer, but toner cartridge is during use, carbon dust as in toner cartridge most
Important developer, but generally filling carbon dust 100% can not be consumed all, from the point of view of different toner cartridge structures, be had more than
10% carbon dust is left in toner cartridge bin.During toner cartridge regenerates, due to the manufacture craft of brand-new carbon dust and old carbon dust
With the difference of materials, under relatively uniform matching condition, different printing effects can be presented；Enterprise of the same trade was regenerating
It is general using directly all with changing the way of brand-new carbon dust in journey, the direct waste treatment of old carbon dust progress, this measure causes substantial amounts of
The waste of recycling resource, the pollution of the environment also resulted in.For this at present urgent need develop one kind can by brand-new carbon dust and
The technique that carbon dust is used in mixed way is reclaimed, under the conditions of with other each part match, even better than brand-new carbon dust can be reached
Print quality.
And current carbon dust preparation technology can't accomplish to prepare the higher carbon dust of purity, it is therefore desirable to processing technology
It is improved.
The content of the invention
For defect of the prior art, it is an object of the invention to provide a kind of regeneration work of printer waste carbon powder
Skill.
A kind of regeneration technology of the printer waste carbon powder provided according to the present invention, the printer waste carbon powder
Regeneration technology is specially：
（1）, waste carbon powder regeneration：Waste carbon powder filtered, is dehydrated, being separated, mix it is outer add thing, secondary filter, regenerated
Carbon dust；
（2）, carbon dust purification：By wet purification, application of vacuum and high-temperature calcination, high-purity carbon dust is prepared.
Preferably, the step（1）The specific method of middle filtering is：Waste carbon powder is filtered using screen cloth, removed
The larger carbon dust of particle and other impurities.
Preferably, the step（1）The specific method of middle dehydration is：Drying and processing is carried out to the carbon dust after filtering so that
Carbon dust moisture content after processing is between 0.031-0.045%.
Preferably, the step（1）The specific method of middle separation is：Carbon dust after dehydration is separated, retains particle diameter
For 6-13 μm of carbon dust.
Preferably, the step（1）The specific method for adding thing outside middle mixing is：It is addition in 6-13 μm of carbon dust to particle diameter
Acrylate, carbon black and silica flour, are mixed, stirring, and the acrylate, carbon black, silica flour mass ratio are 80-90:5-
9:2-5。
Preferably, the step（1）The specific method of middle secondary filter is：Using screen cloth to being mixed with the outer carbon dust for adding thing
Filtered, remove the larger carbon dust of particle and add thing outside.
Preferably, the step（2）The specific method of middle wet purification is：Use mass concentration for 10-15% hydrochloric acid and
Mass concentration is mixed for 11-13% hydrofluoric acid, and then regeneration carbon dust is put into mixed acid solution and soaks 24-48h, is dried.
Preferably, the step（2）In the specific method of application of vacuum be：Refer to the carbon dust after drying in calcining furnace
Calcine under vacuum condition, calcining heat is 400-500 DEG C.
Preferably, the step（2）In the specific method of high-temperature calcination be：Carbon dust Jing Guo application of vacuum is put into
Calcined in high-temperature calcination stove, vacuum level requirements during calcining are 10-2Carried out under the conditions of Pa, described calcining heat is 2300-
2500℃。
Compared with prior art, the present invention has following beneficial effect：
（1）A kind of regeneration technology for printer waste carbon powder that the present invention is provided, regeneration cartridge of the present invention to same color
Carbon dust in powder cabin is reclaimed, by adding several main steps such as thing, secondary filter outside filtering, dehydration, separation, mixing,
The performance of the remaining carbon dust regenerated in toner cartridge is brought up into the condition basically identical with brand-new carbon dust, and promotes production
Use.Meanwhile, the processes such as purifying technique, including wet purification, application of vacuum and high-temperature calcination are carried out to carbon dust.Due in carbon dust
Sulfur content it is higher, by the temperature control in vacuum process, element sulphur is volatilized, remove carbon dust in sulphur
Element, so as to avoid in high-temperature calcination stage, sulphur and iron, magnesium, the higher sulfide of carbon reaction generation sulfide boiling point increases carbon
The difficulty of powder purification.Again because, containing the element that boiling point is higher, such as iron, magnesium, titanium element only reach in calcining heat in carbon dust
To more than 2200 degree, high-boiling-point impurity could be preferably removed；
（2）The present invention can effectively improve carbon dust and recycle efficiency, reduce the pollution to environment.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.It should be understood that these embodiments be merely to illustrate the present invention without
For limiting the scope of the present invention.
Embodiment 1
A kind of regeneration technology for printer waste carbon powder that the present embodiment is provided, the regeneration work of the printer waste carbon powder
Skill is specially：
（1）, waste carbon powder regeneration：Waste carbon powder filtered, is dehydrated, being separated, mix it is outer add thing, secondary filter, regenerated
Carbon dust；
（2）, carbon dust purification：By wet purification, application of vacuum and high-temperature calcination, high-purity carbon dust is prepared.
Wherein, the step（1）The specific method of middle filtering is：Waste carbon powder is filtered using screen cloth, removal
The larger carbon dust of grain and other impurities.
Wherein, the step（1）The specific method of middle dehydration is：Drying and processing is carried out to the carbon dust after filtering so that place
Carbon dust moisture content after reason is 0.031%.
Wherein, the step（1）The specific method of middle separation is：Carbon dust after dehydration is separated, it is 6 to retain particle diameter
μm carbon dust.
Wherein, the step（1）The specific method for adding thing outside middle mixing is：Propylene is added into the carbon dust that particle diameter is 6 μm
Acid ester resin, carbon black and silica flour, are mixed, stirring, and the acrylate, carbon black, silica flour mass ratio are 90:5:5.
Wherein, the step（1）The specific method of middle secondary filter is：Entered using screen cloth to being mixed with the outer carbon dust for adding thing
Row filtering, removes the larger carbon dust of particle and adds thing outside.
Described screen cloth uses metallic sieve, and metallic sieve is that wire is made by certain technical method to reticulate
Product.It is that raw material is made into copper wire, stainless steel wire, iron wire, steel wire.It is general to use plain weave, twill, seat shape weaving method.Metal
Screened port is clear correct, wire side is flat very, has high temperature resistant, a characteristic such as wear-resisting, and stainless steel mesh can also be corrosion-resistant.
Wherein, the step（2）The specific method of middle wet purification is：Use hydrochloric acid and quality of the mass concentration for 15%
Concentration is mixed for 11% hydrofluoric acid, and then regeneration carbon dust is put into mixed acid solution and soaks 48h, is dried.
Wherein, the step（2）In the specific method of application of vacuum be：Refer to that the carbon dust after drying enters in calcining furnace
Calcined under row vacuum condition, calcining heat is 500 DEG C.
Wherein, the step（2）In the specific method of high-temperature calcination be：Carbon dust Jing Guo application of vacuum is put into height
Calcined in warm calcining furnace, vacuum level requirements during calcining are 10-2Carried out under the conditions of Pa, described calcining heat is 2300 DEG C.
Embodiment 2
A kind of regeneration technology for printer waste carbon powder that the present embodiment is provided, the regeneration work of the printer waste carbon powder
Skill is specially：
（1）, waste carbon powder regeneration：Waste carbon powder filtered, is dehydrated, being separated, mix it is outer add thing, secondary filter, regenerated
Carbon dust；
（2）, carbon dust purification：By wet purification, application of vacuum and high-temperature calcination, high-purity carbon dust is prepared.
Wherein, the step（1）The specific method of middle filtering is：Waste carbon powder is filtered using screen cloth, removal
The larger carbon dust of grain and other impurities.
Wherein, the step（1）The specific method of middle dehydration is：Drying and processing is carried out to the carbon dust after filtering so that place
Carbon dust moisture content after reason is 0.031%.
Wherein, the step（1）The specific method of middle separation is：Carbon dust after dehydration is separated, retaining particle diameter is
13 μm of carbon dust.
Wherein, the step（1）The specific method for adding thing outside middle mixing is：Propylene is added into the carbon dust that particle diameter is 13 μm
Acid ester resin, carbon black and silica flour, are mixed, stirring, and the acrylate, carbon black, silica flour mass ratio are 80:9:2.
Wherein, the step（1）The specific method of middle secondary filter is：Entered using screen cloth to being mixed with the outer carbon dust for adding thing
Row filtering, removes the larger carbon dust of particle and adds thing outside.
Described screen cloth uses metallic sieve, and metallic sieve is that wire is made by certain technical method to reticulate
Product.It is that raw material is made into copper wire, stainless steel wire, iron wire, steel wire.It is general to use plain weave, twill, seat shape weaving method.Metal
Screened port is clear correct, wire side is flat very, has high temperature resistant, a characteristic such as wear-resisting, and stainless steel mesh can also be corrosion-resistant.
Wherein, the step（2）The specific method of middle wet purification is：Use hydrochloric acid and quality of the mass concentration for 10%
Concentration is mixed for 13% hydrofluoric acid, and then regeneration carbon dust is put into mixed acid solution and soaks 24h, is dried.
Wherein, the step（2）In the specific method of application of vacuum be：Refer to that the carbon dust after drying enters in calcining furnace
Calcined under row vacuum condition, calcining heat is 400 DEG C.
Wherein, the step（2）In the specific method of high-temperature calcination be：Carbon dust Jing Guo application of vacuum is put into height
Calcined in warm calcining furnace, vacuum level requirements during calcining are 10-2Carried out under the conditions of Pa, described calcining heat is 2500 DEG C.
Embodiment 3
A kind of regeneration technology for printer waste carbon powder that the present embodiment is provided, the regeneration work of the printer waste carbon powder
Skill is specially：
（1）, waste carbon powder regeneration：Waste carbon powder filtered, is dehydrated, being separated, mix it is outer add thing, secondary filter, regenerated
Carbon dust；
（2）, carbon dust purification：By wet purification, application of vacuum and high-temperature calcination, high-purity carbon dust is prepared.
Wherein, the step（1）The specific method of middle filtering is：Waste carbon powder is filtered using screen cloth, removal
The larger carbon dust of grain and other impurities.
Wherein, the step（1）The specific method of middle dehydration is：Drying and processing is carried out to the carbon dust after filtering so that place
Carbon dust moisture content after reason is 0.035%.
Wherein, the step（1）The specific method of middle separation is：Carbon dust after dehydration is separated, it is 8 to retain particle diameter
μm carbon dust.
Wherein, the step（1）The specific method for adding thing outside middle mixing is：Propylene is added into the carbon dust that particle diameter is 8 μm
Acid ester resin, carbon black and silica flour, are mixed, stirring, and the acrylate, carbon black, silica flour mass ratio are 85:7:3.
Wherein, the step（1）The specific method of middle secondary filter is：Entered using screen cloth to being mixed with the outer carbon dust for adding thing
Row filtering, removes the larger carbon dust of particle and adds thing outside.
Described screen cloth uses metallic sieve, and metallic sieve is that wire is made by certain technical method to reticulate
Product.It is that raw material is made into copper wire, stainless steel wire, iron wire, steel wire.It is general to use plain weave, twill, seat shape weaving method.Metal
Screened port is clear correct, wire side is flat very, has high temperature resistant, a characteristic such as wear-resisting, and stainless steel mesh can also be corrosion-resistant.
Wherein, the step（2）The specific method of middle wet purification is：Use hydrochloric acid and quality of the mass concentration for 12%
Concentration is mixed for 12% hydrofluoric acid, and then regeneration carbon dust is put into mixed acid solution and soaks 38h, is dried.
Wherein, the step（2）In the specific method of application of vacuum be：Refer to that the carbon dust after drying enters in calcining furnace
Calcined under row vacuum condition, calcining heat is 450 DEG C.
Wherein, the step（2）In the specific method of high-temperature calcination be：Carbon dust Jing Guo application of vacuum is put into height
Calcined in warm calcining furnace, vacuum level requirements during calcining are 10-2Carried out under the conditions of Pa, described calcining heat is 2400 DEG C.
Compared with prior art, the present invention has following beneficial effect：
（1）A kind of regeneration technology for printer waste carbon powder that the present invention is provided, regeneration cartridge of the present invention to same color
Carbon dust in powder cabin is reclaimed, by adding several main steps such as thing, secondary filter outside filtering, dehydration, separation, mixing,
The performance of the remaining carbon dust regenerated in toner cartridge is brought up into the condition basically identical with brand-new carbon dust, and promotes production
Use.Meanwhile, the processes such as purifying technique, including wet purification, application of vacuum and high-temperature calcination are carried out to carbon dust.Due in carbon dust
Sulfur content it is higher, by the temperature control in vacuum process, element sulphur is volatilized, remove carbon dust in sulphur
Element, so as to avoid in high-temperature calcination stage, sulphur and iron, magnesium, the higher sulfide of carbon reaction generation sulfide boiling point increases carbon
The difficulty of powder purification.Again because, containing the element that boiling point is higher, such as iron, magnesium, titanium element only reach in calcining heat in carbon dust
To more than 2200 degree, high-boiling-point impurity could be preferably removed；
（2）The present invention can effectively improve carbon dust and recycle efficiency, reduce the pollution to environment.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (9)
1. a kind of regeneration technology of printer waste carbon powder, it is characterised in that：The regeneration work of the printer waste carbon powder
Skill is specially：
（1）, waste carbon powder regeneration：Waste carbon powder filtered, is dehydrated, being separated, mix it is outer add thing, secondary filter, regenerated
Carbon dust；
（2）, carbon dust purification：By wet purification, application of vacuum and high-temperature calcination, high-purity carbon dust is prepared.
2. a kind of regeneration technology of printer waste carbon powder according to claim 1, it is characterised in that：The step
（1）The specific method of middle filtering is：Waste carbon powder is filtered using screen cloth, the larger carbon dust of particle is removed and other is miscellaneous
Matter.
3. a kind of regeneration technology of printer waste carbon powder according to claim 1 or 2, it is characterised in that：The step
Suddenly（1）The specific method of middle dehydration is：Drying and processing is carried out to the carbon dust after filtering so that the carbon dust moisture content after processing exists
Between 0.031-0.045%.
4. a kind of regeneration technology of printer waste carbon powder according to claim 1 or 3, it is characterised in that：The step
Suddenly（1）The specific method of middle separation is：Carbon dust after dehydration is separated, retains the carbon dust that particle diameter is 6-13 μm.
5. a kind of regeneration technology of printer waste carbon powder according to claim 1 or 4, it is characterised in that：The step
Suddenly（1）The specific method for adding thing outside middle mixing is：It is addition acrylate, carbon black and silicon in 6-13 μm of carbon dust to particle diameter
Powder, is mixed, stirring, and the acrylate, carbon black, silica flour mass ratio are 80-90:5-9:2-5.
6. a kind of regeneration technology of printer waste carbon powder according to claim 1 or 5, it is characterised in that：The step
Suddenly（1）The specific method of middle secondary filter is：Filtered using screen cloth to being mixed with the outer carbon dust for adding thing, remove particle larger
Carbon dust and add thing outside.
7. a kind of regeneration technology of printer waste carbon powder according to claim 1, it is characterised in that：The step
（2）The specific method of middle wet purification is：Use the hydrogen fluorine that mass concentration is 11-13% for 10-15% hydrochloric acid and mass concentration
Regeneration carbon dust, is then put into mixed acid solution and soaks 24-48h, dry by acid mixing.
8. a kind of regeneration technology of printer waste carbon powder according to claim 1, it is characterised in that：The step
（2）In the specific method of application of vacuum be：Refer to that the carbon dust after drying carries out calcining under vacuum condition in calcining furnace, calcining
Temperature is 400-500 DEG C.
9. a kind of regeneration technology of printer waste carbon powder according to claim 1, it is characterised in that：The step
（2）In the specific method of high-temperature calcination be：Carbon dust Jing Guo application of vacuum is put into high-temperature calcination stove and calcined, during calcining
Vacuum level requirements 10-2Carried out under the conditions of Pa, described calcining heat is 2300-2500 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710566190.7A CN107151007A (en) | 2017-07-12 | 2017-07-12 | A kind of regeneration technology of printer waste carbon powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710566190.7A CN107151007A (en) | 2017-07-12 | 2017-07-12 | A kind of regeneration technology of printer waste carbon powder |
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| CN107151007A true CN107151007A (en) | 2017-09-12 |
Family
ID=59796933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201710566190.7A Withdrawn CN107151007A (en) | 2017-07-12 | 2017-07-12 | A kind of regeneration technology of printer waste carbon powder |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109775700A (en) * | 2019-02-13 | 2019-05-21 | 山东天岳先进材料科技有限公司 | The recycling of waste and old graphite crucible and high-purity carbon dust |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1332044A (en) * | 2001-07-20 | 2002-01-23 | 大连东泰产业废弃物处理有限公司 | Waste duplicator ink powder treating process |
| CN101246349A (en) * | 2008-03-19 | 2008-08-20 | 湛江惠能墨业有限公司 | Wasted ink powder classification method and reclaiming utilization method after specification |
| CN104355304A (en) * | 2014-10-31 | 2015-02-18 | 峨嵋半导体材料研究所 | 5N high-purity carbon dust preparation process |
| CN104914700A (en) * | 2015-06-30 | 2015-09-16 | 珠海市科力莱科技有限公司 | Double-component color toner recycling process |
| CN105116697A (en) * | 2014-09-11 | 2015-12-02 | 天津市中环天佳电子有限公司 | Nonmagnetic negative electricity laser printer ink powder |
-
2017
- 2017-07-12 CN CN201710566190.7A patent/CN107151007A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1332044A (en) * | 2001-07-20 | 2002-01-23 | 大连东泰产业废弃物处理有限公司 | Waste duplicator ink powder treating process |
| CN101246349A (en) * | 2008-03-19 | 2008-08-20 | 湛江惠能墨业有限公司 | Wasted ink powder classification method and reclaiming utilization method after specification |
| CN105116697A (en) * | 2014-09-11 | 2015-12-02 | 天津市中环天佳电子有限公司 | Nonmagnetic negative electricity laser printer ink powder |
| CN104355304A (en) * | 2014-10-31 | 2015-02-18 | 峨嵋半导体材料研究所 | 5N high-purity carbon dust preparation process |
| CN104914700A (en) * | 2015-06-30 | 2015-09-16 | 珠海市科力莱科技有限公司 | Double-component color toner recycling process |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109775700A (en) * | 2019-02-13 | 2019-05-21 | 山东天岳先进材料科技有限公司 | The recycling of waste and old graphite crucible and high-purity carbon dust |
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Application publication date: 20170912 |