CN107150390A - A kind of sofening treatment method of wicker - Google Patents
A kind of sofening treatment method of wicker Download PDFInfo
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- CN107150390A CN107150390A CN201710353468.2A CN201710353468A CN107150390A CN 107150390 A CN107150390 A CN 107150390A CN 201710353468 A CN201710353468 A CN 201710353468A CN 107150390 A CN107150390 A CN 107150390A
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- Prior art keywords
- wicker
- willow bark
- treatment method
- drying
- water content
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-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
- B27K3/50—Mixtures of different organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/003—Treating of wood not provided for in groups B27K1/00, B27K3/00 by using electromagnetic radiation or mechanical waves
- B27K5/0065—Ultrasonic treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/06—Softening or hardening of wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27L—REMOVING BARK OR VESTIGES OF BRANCHES; SPLITTING WOOD; MANUFACTURE OF VENEER, WOODEN STICKS, WOOD SHAVINGS, WOOD FIBRES OR WOOD POWDER
- B27L3/00—Debarking by chemical treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/20—Removing fungi, molds or insects
Abstract
The invention mainly relates to woodwork processing technique field, a kind of sofening treatment method of wicker is disclosed, including:Wicker immersion, primary drying, wicker enzymolysis, redrying, wicker fermentation, wicker ultrasound, three dryings;Method is simple, is easy to operation, safety and Health; without any toxic chemical, without using high temperature in processing procedure, the energy is saved; environmental protection; processing cost is saved, obtained wicker suppleness improves 11.7%, and the braiding rate of fractureing is reduced to 3.8%; color brilliant white; without processing vestige, the application value of wicker is added, income improves 9.2%;Tied up after wicker harvesting; retain willow bark; handled together with willow bark, it is simple and convenient, save the plenty of time for divesting willow bark; increase the protective effect of willow bark simultaneously; vestige is produced after avoiding processing, is placed in alcoholic solution and soaks after tying up, can antibacterial desinsection; the iuntercellular moisture of wicker can also be increased, soften wicker fiber.
Description
Technical field
The invention mainly relates to a kind of sofening treatment method of woodwork processing technique field, more particularly to wicker.
Background technology
Wicker, is exactly the branch of willow, can not only greening environment, moreover it is possible to be woven into various handicrafts, make full use of from
Right resource, greatly improves the value of wicker, while also enriching the life of people;Wicker it is flexible it is smooth be braiding
One of basis, but the wicker of different times harvesting, suppleness are different, very big limitation are caused to braiding, while also causing
The handicraft quality prepared is uneven, influences the sale of wicker products and uses;Being adopted the sofening treatment of existing woodwork more
With softening agent and high-temperature process, softening agent contains a variety of chemical reagent, pollutes environment, also human body can be damaged, at high temperature
Reason needs higher temperature, wastes the energy, and cost is higher.
The content of the invention
In order to make up the defect of prior art, it is an object of the invention to provide a kind of sofening treatment method of wicker.
A kind of sofening treatment method of wicker, comprises the following steps:
(1)Wicker soaks:Harvested wicker is placed in and tied up, retains willow bark, the plenty of time for divesting willow bark is saved, together
The protective effect of Shi Zengjia willow barks, it is to avoid vestige is produced after processing, often ties a diameter of 10 ~ 12cm, is placed in soak, normal temperature leaching
Bubble 8 ~ 10 hours, makes alcohol be dipped in wicker, can antibacterial desinsection, moreover it is possible to increase the iuntercellular moisture of wicker, softens wicker fiber,
Take out, obtain immersion wicker;
(2)Primary drying:Immersion wicker is placed in the environment that temperature is 38 ~ 40 DEG C, humidity is 56 ~ 58%, 10 ~ 12 are stood small
When, make alcoholic solution slow evaporation, increase space between cells, improve wicker pliability, obtain primary drying wicker;
(3)Wicker is digested:In the water that primary drying wicker is dipped in 2 ~ 3 times of amounts of primary drying wicker weight, complex enzyme is added, in
40 ~ 42 DEG C of insulations are digested 3 ~ 4 hours, make the surface structure of wicker loose, it is to avoid to be broken during braiding, reduce the rate that fractures, and improve willow
Bar utilization rate, takes out, and obtains enzymolysis liquid and enzymolysis wicker;
(4)Redrying:Wicker will be digested to be placed in the baking oven that temperature is 67 ~ 69 DEG C, drying to water content is 28 ~ 30%, obtains two
Secondary dry wicker;
(5)Wicker ferments:Redrying wicker is dipped in step(3)Enzymolysis liquid in, add starch, make the mass concentration of starch
For 16 ~ 18%, it is well mixed, accesses Angel wine yeast, in 30 ~ 32 DEG C of ferment at constant temperature 3 ~ 4 days, is cooled to 21 ~ 23 DEG C of continuation
Fermentation 9 ~ 10 days, the alcohol and small molecule nutritional ingredient of generation quickly penetrate into wicker, kill the pathogenic microorganism remained in wicker
And insect, it is to avoid wicker is mouldy to damage by worms, while the original color of wicker can be kept, it is to avoid processing vestige, keeps wicker braiding
Attractive in appearance and safe, the taking-up of product, obtains fermentation wicker;
(6)Wicker ultrasound:Fermentation wicker is placed in ultrasonic liquid, in 52 ~ 54 DEG C, 28 ~ 30kHz ultrasounds 40 ~ 45 minutes, quickly gone
Except willow bark, Multiple components are contained in ultrasonic liquid, raw material sources are extensively, cheap, without toxic component, safety and Health, increase
The application process of potassium dihydrogen phosphate and willow bark, can soften wicker fiber, moreover it is possible to prevent wicker from changing colour, and suppress varied bacteria growing, keep away
Exempt from the mouldy service life damaged by worms, extend wicker, obtain ultrasonic wicker;
(7)Three dryings:In the baking oven that ultrasonic wicker is placed in 78 ~ 80 DEG C, drying to water content is 32 ~ 34%, it is cooled to 56 ~
58 DEG C, drying to water content is 15 ~ 17%, and uniform water spray is placed in the environment that humidity is 80 ~ 82% and stands 2 ~ 3 days, makes water content
For 23 ~ 25%, it is 10 ~ 12% to dry again to water content, gradually reduces drying temperature, keeps fibre strength, and reduction fractures rate, baking
Added water after dry, being placed in high humidity environment increases water content, then carry out low temperature drying, destroy the storage capacity of wicker fiber, it is to avoid
The moisture absorption, prevent it is mouldy damage by worms, keep wicker suppleness, obtain softening wicker.
The step(1)Soak, be the alcoholic solution that volume fraction is 13 ~ 15%.
The step(3)Complex enzyme, be made up of the raw material of following parts by weight:Cellulase 18 ~ 20, lignoenzyme 12 ~
14th, hemicellulase 10 ~ 12, pectase 4 ~ 6.
The step(5)Angel wine yeast, by re-activation, viable count is 109~1010CFU/ml。
The step(6)Ultrasonic liquid, be made up of the raw material of following parts by weight:Potassium dihydrogen phosphate 11 ~ 13, Herba humuli scandentis extract
1.3 ~ 1.5, extract of willow bark 1.1 ~ 1.3, all raw materials are mixed, and the stirring that adds water makes potassium dihydrogen phosphate to being completely dissolved
Mass concentration is 0.4 ~ 0.5%, obtains ultrasonic liquid.
Described Herba humuli scandentis extract, is to crush humulus grass, adds the water of 180 ~ 200 times of amounts of humulus grass weight, heating boil to
Volume is original 1/20, is added water to cook repeatedly 3 times, is filtered, merging filtrate, be slowly added into filtrate volume fraction for 92 ~
94% alcoholic solution, to final concentration of the 62 ~ 64% of alcohol, stands, filtering, except precipitation, by filtrate dry to water content be 7 ~
9%, obtain Herba humuli scandentis extract.
Described extract of willow bark, collects the willow bark produced in willow and wicker process, crushes, and adds willow
120 ~ 140 times of amounts of tare weight amount, the acetum that volume fraction is 1.7 ~ 1.9%, soak 3 ~ 4 hours, and it is original that heating, which is boiled to volume,
1/10 come, filter cleaner, it is 8 ~ 10% that filtrate, which is dried to water content, obtains extract of willow bark.
The step(7)Drying again, drying temperature be 51 ~ 53 DEG C.
The softening mold-proof method of the timber, obtained softening timber.
It is an advantage of the invention that:A kind of sofening treatment method for wicker that the present invention is provided, method is simple, is easy to operation,
Safety and Health, without any toxic chemical, is handled in processing procedure without using high temperature, the saving energy, environmental protection, saving
Cost, obtained wicker suppleness improves 11.7%, and the braiding rate of fractureing is reduced to 3.8%, and color brilliant white, no processing vestige is added
The application value of wicker, income improves 9.2%;Tied up after wicker harvesting, retain willow bark, carried out together with willow bark
Processing, it is simple and convenient, the plenty of time for divesting willow bark is saved, while increasing the protective effect of willow bark, it is to avoid produce trace after processing
Mark, is placed in alcoholic solution after tying up and carries out soak at room temperature, alcohol is dipped in wicker, can antibacterial desinsection, moreover it is possible to increase wicker
Iuntercellular moisture, soften wicker fiber;In the environment that wicker after immersion is placed in high temperature low humidity, primary drying is carried out, is made
Alcoholic solution slow evaporation, increases space between cells, improves wicker pliability;Wicker is placed in water after primary drying, added multiple
Synthase is digested, and makes the surface structure of wicker loose, it is to avoid to be broken during braiding, reduces the rate that fractures, and improves wicker utilization rate;Enzyme
Wicker is placed in low temperature baking oven after solution and baked, it is slow to reduce wicker moisture, keep wicker pliability;Wicker is soaked again
In enzymolysis liquid, add starch and Angel wine yeast is fermented, the alcohol and small molecule nutritional ingredient of generation quickly ooze
Enter wicker, kill the pathogenic microorganism remained in wicker and insect, it is to avoid wicker is mouldy to damage by worms, while the original of wicker can be kept
There is color and luster, it is to avoid processing vestige, keep the attractive in appearance and safe of wicker knitting;Wicker is placed in ultrasonic liquid after fermentation and surpassed
Sound, quickly removes and contains Multiple components in willow bark, ultrasonic liquid, and raw material sources are extensively, cheap, without toxic component, safety
The application process of health, increase potassium dihydrogen phosphate and willow bark, can soften wicker fiber, moreover it is possible to prevent wicker from changing colour, and suppress miscellaneous
Bacteria growing, it is to avoid mouldy to damage by worms, extends the service life of wicker;Finally wicker is placed in low temperature baking oven and dried, gradually
Drying temperature is reduced, fibre strength is kept, the rate that fractures is reduced, is added water after drying, being placed in high humidity environment increases water content, then enter
Row low temperature drying, destroy wicker fiber storage capacity, it is to avoid the moisture absorption, prevent it is mouldy damage by worms, keep wicker suppleness.
Embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of sofening treatment method of wicker, comprises the following steps:
(1)Wicker soaks:Harvested wicker is placed in and tied up, retains willow bark, the plenty of time for divesting willow bark is saved, together
The protective effect of Shi Zengjia willow barks, it is to avoid vestige is produced after processing, often ties a diameter of 10 ~ 12cm, is placed in soak, normal temperature leaching
Bubble 8 hours, makes alcohol be dipped in wicker, can antibacterial desinsection, moreover it is possible to increase the iuntercellular moisture of wicker, softens wicker fiber, takes
Go out, obtain immersion wicker;
(2)Primary drying:Immersion wicker is placed in the environment that temperature is 38 ~ 40 DEG C, humidity is 56 ~ 58%, 10 hours are stood,
Make alcoholic solution slow evaporation, increase space between cells, improve wicker pliability, obtain primary drying wicker;
(3)Wicker is digested:In the water that primary drying wicker is dipped in 2 times of amounts of primary drying wicker weight, complex enzyme is added, in 40
DEG C insulation enzymolysis 3 hours, makes the surface structure of wicker loose, it is to avoid to be broken during braiding, reduction fractures rate, improves wicker and utilize
Rate, takes out, and obtains enzymolysis liquid and enzymolysis wicker;
(4)Redrying:Wicker will be digested to be placed in the baking oven that temperature is 67 DEG C, drying to water content is 28 ~ 30%, obtains secondary
Dry wicker;
(5)Wicker ferments:Redrying wicker is dipped in step(3)Enzymolysis liquid in, add starch, make the mass concentration of starch
For 16%, it is well mixed, accesses Angel wine yeast, in 30 DEG C of ferment at constant temperature 3 days, is cooled to 21 DEG C and continues to ferment 9 days, production
Raw alcohol and small molecule nutritional ingredient quickly penetrates into wicker, kills the pathogenic microorganism remained in wicker and insect, it is to avoid willow
Bar is mouldy to damage by worms, while the original color of wicker can be kept, it is to avoid processing vestige, keeps the attractive in appearance of wicker knitting and peace
Entirely, take out, obtain fermentation wicker;
(6)Wicker ultrasound:Will fermentation wicker be placed in ultrasonic liquid, in 52 DEG C, 28kHz ultrasound 40 minutes, quickly remove willow bark, surpass
Contain Multiple components in sound liquid, raw material sources are extensively, cheap, without toxic component, safety and Health increases potassium dihydrogen phosphate
With the application process of willow bark, wicker fiber can be softened, moreover it is possible to prevent wicker from changing colour, suppress varied bacteria growing, it is to avoid mouldy to damage by worms,
Extend the service life of wicker, obtain ultrasonic wicker;
(7)Three dryings:In the baking oven that ultrasonic wicker is placed in 78 DEG C, drying to water content is 32%, is cooled to 56 DEG C, drying
It is 15% to water content, uniform water spray is placed in the environment that humidity is 80 ~ 82% and stands 2 days, and it is 23 ~ 25% to make water content, again
Drying to water content is 10 ~ 12%, gradually reduces drying temperature, keeps fibre strength, reduces the rate that fractures, adds water, be placed in after drying
Increase water content in high humidity environment, then carry out low temperature drying, destroy the storage capacity of wicker fiber, it is to avoid the moisture absorption, prevent mouldy
Damage by worms, keep wicker suppleness, obtain softening wicker.
The step(1)Soak, be the alcoholic solution that volume fraction is 13%.
The step(3)Complex enzyme, be made up of the raw material of following parts by weight:Cellulase 18, lignoenzyme 12, half fibre
The plain enzyme 10 of dimension, pectase 4.
The step(5)Angel wine yeast, by re-activation, viable count is 109~1010CFU/ml。
The step(6)Ultrasonic liquid, be made up of the raw material of following parts by weight:Potassium dihydrogen phosphate 11, Herba humuli scandentis extract
1.3rd, extract of willow bark 1.1, all raw materials are mixed, and the stirring that adds water makes the mass concentration of potassium dihydrogen phosphate to being completely dissolved
For 0.4%, ultrasonic liquid is obtained.
Described Herba humuli scandentis extract, is to crush humulus grass, adds the water of 180 times of amounts of humulus grass weight, and heating is boiled to volume
For original 1/20, add water to cook 3 times, filter, merging filtrate repeatedly, the wine that volume fraction is 92% is slowly added into filtrate
Smart solution, to final concentration of the 62% of alcohol, stands, filtering, and except precipitation, it is 7 ~ 9% that filtrate, which is dried to water content, obtains humulus grass and carries
Take thing.
Described extract of willow bark, collects the willow bark produced in willow and wicker process, crushes, and adds willow
120 times of amounts of tare weight amount, the acetum that volume fraction is 1.7%, soak 3 hours, and it is original 1/10 that heating, which is boiled to volume,
Filter cleaner, it is 8 ~ 10% that filtrate, which is dried to water content, obtains extract of willow bark.
The step(7)Drying again, drying temperature be 51 DEG C.
The softening mold-proof method of the timber, obtained softening timber.
Embodiment 2
A kind of sofening treatment method of wicker, comprises the following steps:
(1)Wicker soaks:Harvested wicker is placed in and tied up, retains willow bark, the plenty of time for divesting willow bark is saved, together
The protective effect of Shi Zengjia willow barks, it is to avoid vestige is produced after processing, often ties a diameter of 10 ~ 12cm, is placed in soak, normal temperature leaching
Bubble 9 hours, makes alcohol be dipped in wicker, can antibacterial desinsection, moreover it is possible to increase the iuntercellular moisture of wicker, softens wicker fiber, takes
Go out, obtain immersion wicker;
(2)Primary drying:Immersion wicker is placed in the environment that temperature is 38 ~ 40 DEG C, humidity is 56 ~ 58%, 11 hours are stood,
Make alcoholic solution slow evaporation, increase space between cells, improve wicker pliability, obtain primary drying wicker;
(3)Wicker is digested:In the water that primary drying wicker is dipped in 2 times of amounts of primary drying wicker weight, complex enzyme is added, in 41
DEG C insulation enzymolysis 3 hours, makes the surface structure of wicker loose, it is to avoid to be broken during braiding, reduction fractures rate, improves wicker and utilize
Rate, takes out, and obtains enzymolysis liquid and enzymolysis wicker;
(4)Redrying:Wicker will be digested to be placed in the baking oven that temperature is 68 DEG C, drying to water content is 28 ~ 30%, obtains secondary
Dry wicker;
(5)Wicker ferments:Redrying wicker is dipped in step(3)Enzymolysis liquid in, add starch, make the mass concentration of starch
For 17%, it is well mixed, accesses Angel wine yeast, in 31 DEG C of ferment at constant temperature 3 days, is cooled to 22 DEG C and continues to ferment 9 days, production
Raw alcohol and small molecule nutritional ingredient quickly penetrates into wicker, kills the pathogenic microorganism remained in wicker and insect, it is to avoid willow
Bar is mouldy to damage by worms, while the original color of wicker can be kept, it is to avoid processing vestige, keeps the attractive in appearance of wicker knitting and peace
Entirely, take out, obtain fermentation wicker;
(6)Wicker ultrasound:Will fermentation wicker be placed in ultrasonic liquid, in 53 DEG C, 29kHz ultrasound 40 minutes, quickly remove willow bark, surpass
Contain Multiple components in sound liquid, raw material sources are extensively, cheap, without toxic component, safety and Health increases potassium dihydrogen phosphate
With the application process of willow bark, wicker fiber can be softened, moreover it is possible to prevent wicker from changing colour, suppress varied bacteria growing, it is to avoid mouldy to damage by worms,
Extend the service life of wicker, obtain ultrasonic wicker;
(7)Three dryings:In the baking oven that ultrasonic wicker is placed in 79 DEG C, drying to water content is 32 ~ 34%, is cooled to 57 DEG C, baking
It is 15 ~ 17% to do to water content, and uniform water spray is placed in the environment that humidity is 80 ~ 82% and stands 2 days, and it is 23 ~ 25% to make water content,
It is 10 ~ 12% to dry again to water content, gradually reduces drying temperature, keeps fibre strength, reduces the rate that fractures, is added water after drying,
Being placed in high humidity environment increases water content, then carries out low temperature drying, destroys the storage capacity of wicker fiber, it is to avoid the moisture absorption, prevents
It is mouldy to damage by worms, wicker suppleness is kept, softening wicker is obtained.
The step(1)Soak, be the alcoholic solution that volume fraction is 14%.
The step(3)Complex enzyme, be made up of the raw material of following parts by weight:Cellulase 19, lignoenzyme 13, half fibre
The plain enzyme 11 of dimension, pectase 5.
The step(5)Angel wine yeast, by re-activation, viable count is 109~1010CFU/ml。
The step(6)Ultrasonic liquid, be made up of the raw material of following parts by weight:Potassium dihydrogen phosphate 12, Herba humuli scandentis extract
1.4th, extract of willow bark 1.2, all raw materials are mixed, and the stirring that adds water makes the mass concentration of potassium dihydrogen phosphate to being completely dissolved
For 0.4%, ultrasonic liquid is obtained.
Described Herba humuli scandentis extract, is to crush humulus grass, adds the water of 190 times of amounts of humulus grass weight, and heating is boiled to volume
For original 1/20, add water to cook 3 times, filter, merging filtrate repeatedly, the wine that volume fraction is 93% is slowly added into filtrate
Smart solution, to final concentration of the 63% of alcohol, stands, filtering, and except precipitation, it is 7 ~ 9% that filtrate, which is dried to water content, obtains humulus grass and carries
Take thing.
Described extract of willow bark, collects the willow bark produced in willow and wicker process, crushes, and adds willow
130 times of amounts of tare weight amount, the acetum that volume fraction is 1.8%, soak 3 hours, and it is original 1/10 that heating, which is boiled to volume,
Filter cleaner, it is 8 ~ 10% that filtrate, which is dried to water content, obtains extract of willow bark.
The step(7)Drying again, drying temperature be 52 DEG C.
The softening mold-proof method of the timber, obtained softening timber.
Embodiment 3
A kind of sofening treatment method of wicker, comprises the following steps:
(1)Wicker soaks:Harvested wicker is placed in and tied up, retains willow bark, the plenty of time for divesting willow bark is saved, together
The protective effect of Shi Zengjia willow barks, it is to avoid vestige is produced after processing, often ties a diameter of 10 ~ 12cm, is placed in soak, normal temperature leaching
Bubble 10 hours, makes alcohol be dipped in wicker, can antibacterial desinsection, moreover it is possible to increase the iuntercellular moisture of wicker, softens wicker fiber, takes
Go out, obtain immersion wicker;
(2)Primary drying:Immersion wicker is placed in the environment that temperature is 38 ~ 40 DEG C, humidity is 56 ~ 58%, 12 hours are stood,
Make alcoholic solution slow evaporation, increase space between cells, improve wicker pliability, obtain primary drying wicker;
(3)Wicker is digested:In the water that primary drying wicker is dipped in 3 times of amounts of primary drying wicker weight, complex enzyme is added, in 42
DEG C insulation enzymolysis 4 hours, makes the surface structure of wicker loose, it is to avoid to be broken during braiding, reduction fractures rate, improves wicker and utilize
Rate, takes out, and obtains enzymolysis liquid and enzymolysis wicker;
(4)Redrying:Wicker will be digested to be placed in the baking oven that temperature is 69 DEG C, drying to water content is 28 ~ 30%, obtains secondary
Dry wicker;
(5)Wicker ferments:Redrying wicker is dipped in step(3)Enzymolysis liquid in, add starch, make the mass concentration of starch
For 18%, it is well mixed, accesses Angel wine yeast, in 32 DEG C of ferment at constant temperature 4 days, is cooled to 23 DEG C and continues to ferment 10 days, production
Raw alcohol and small molecule nutritional ingredient quickly penetrates into wicker, kills the pathogenic microorganism remained in wicker and insect, it is to avoid willow
Bar is mouldy to damage by worms, while the original color of wicker can be kept, it is to avoid processing vestige, keeps the attractive in appearance of wicker knitting and peace
Entirely, take out, obtain fermentation wicker;
(6)Wicker ultrasound:Will fermentation wicker be placed in ultrasonic liquid, in 54 DEG C, 30kHz ultrasound 45 minutes, quickly remove willow bark, surpass
Contain Multiple components in sound liquid, raw material sources are extensively, cheap, without toxic component, safety and Health increases potassium dihydrogen phosphate
With the application process of willow bark, wicker fiber can be softened, moreover it is possible to prevent wicker from changing colour, suppress varied bacteria growing, it is to avoid mouldy to damage by worms,
Extend the service life of wicker, obtain ultrasonic wicker;
(7)Three dryings:In the baking oven that ultrasonic wicker is placed in 80 DEG C, drying to water content is 32 ~ 34%, is cooled to 58 DEG C, baking
It is 15 ~ 17% to do to water content, and uniform water spray is placed in the environment that humidity is 80 ~ 82% and stands 3 days, and it is 23 ~ 25% to make water content,
It is 10 ~ 12% to dry again to water content, gradually reduces drying temperature, keeps fibre strength, reduces the rate that fractures, is added water after drying,
Being placed in high humidity environment increases water content, then carries out low temperature drying, destroys the storage capacity of wicker fiber, it is to avoid the moisture absorption, prevents
It is mouldy to damage by worms, wicker suppleness is kept, softening wicker is obtained.
The step(1)Soak, be the alcoholic solution that volume fraction is 15%.
The step(3)Complex enzyme, be made up of the raw material of following parts by weight:Cellulase 20, lignoenzyme 14, half fibre
The plain enzyme 12 of dimension, pectase 6.
The step(5)Angel wine yeast, by re-activation, viable count is 109~1010CFU/ml。
The step(6)Ultrasonic liquid, be made up of the raw material of following parts by weight:Potassium dihydrogen phosphate 13, Herba humuli scandentis extract
1.5th, extract of willow bark 1.3, all raw materials are mixed, and the stirring that adds water makes the mass concentration of potassium dihydrogen phosphate to being completely dissolved
For 0.5%, ultrasonic liquid is obtained.
Described Herba humuli scandentis extract, is to crush humulus grass, adds the water of 200 times of amounts of humulus grass weight, and heating is boiled to volume
For original 1/20, add water to cook 3 times, filter, merging filtrate repeatedly, the wine that volume fraction is 94% is slowly added into filtrate
Smart solution, to final concentration of the 64% of alcohol, stands, filtering, and except precipitation, it is 7 ~ 9% that filtrate, which is dried to water content, obtains humulus grass and carries
Take thing.
Described extract of willow bark, collects the willow bark produced in willow and wicker process, crushes, and adds willow
140 times of amounts of tare weight amount, the acetum that volume fraction is 1.9%, soak 4 hours, and it is original 1/10 that heating, which is boiled to volume,
Filter cleaner, it is 8 ~ 10% that filtrate, which is dried to water content, obtains extract of willow bark.
The step(7)Drying again, drying temperature be 53 DEG C.
The softening mold-proof method of the timber, obtained softening timber.
Comparative example 1
Step(1)In tie up before divest willow bark, remaining method, be the same as Example 1.
Comparative example 2
Removal step(1), remaining method, be the same as Example 1.
Comparative example 3
Removal step(2), remaining method, be the same as Example 1.
Comparative example 4
Removal step(3), remaining method, be the same as Example 1.
Comparative example 5
Removal step(4), remaining method, be the same as Example 1.
Comparative example 6
Removal step(5), remaining method, be the same as Example 1.
Comparative example 7
Removal step(6), remaining method, be the same as Example 1.
Comparative example 8
Removal step(7), remaining method, be the same as Example 1.
Comparative example 9
The steam softening method of existing wicker.
The bating effect of embodiment and comparative example wicker softening method:
In Anhui Province Funan area, summer harvesting white willow 1300kg is randomly divided into 13 groups, respectively every group of 100kg, embodiment
Group, comparative example group and blank group, each group carry out sofening treatment according to the method for the group respectively, and blank group does not carry out any processing,
Other method all sames, are detected after being disposed, and it is 35 DEG C to be placed in temperature, and humidity is mould proof anti-to be carried out in 85% environment
The bating effect of the effect detection of moth, embodiment and comparative example wicker softening method is shown in Table 1.
Table 1:The bating effect of embodiment and comparative example wicker softening method
Project | Suppleness is improved(%) | Fracture rate(%) | Occur it is mouldy damage by worms/(my god) | Color and luster |
Embodiment 1 | 11.1 | 3.9 | 24~25 | Natural brilliant white |
Embodiment 2 | 11.7 | 3.8 | 23~24 | Natural brilliant white |
Embodiment 3 | 11.3 | 4.1 | 24~25 | Natural brilliant white |
Comparative example 1 | 10.8 | 5.2 | 22~23 | Dimness jaundice |
Comparative example 2 | 7.5 | 6.3 | 18~19 | Natural brilliant white |
Comparative example 3 | 7.1 | 7.4 | 16~17 | Natural brilliant white |
Comparative example 4 | 8.3 | 7.9 | 15~16 | Natural brilliant white |
Comparative example 5 | 7.2 | 8.1 | 15~16 | Natural brilliant white |
Comparative example 6 | 8.0 | 8.6 | 16~17 | Natural brilliant white |
Comparative example 7 | 7.3 | 7.9 | 13~14 | Natural brilliant white |
Comparative example 8 | 8.2 | 7.9 | 11~12 | Dimness jaundice |
Comparative example 9 | 5.4 | 9.5 | 8~9 | Dimness jaundice |
Blank group | — | 11.2 | 4~5 | Natural brilliant white |
Note:"-" indicate without.
Show from the result of table 1, the sofening treatment method of embodiment wicker, the suppleness of wicker improves, fractureed after processing
Rate and the appearance mouldy time damaged by worms are substantially better than comparative example, and natural in color brilliant white does not handle vestige, illustrate present invention offer
The sofening treatment method of wicker there is good bating effect.
Claims (9)
1. a kind of sofening treatment method of wicker, it is characterised in that comprise the following steps:
(1)Wicker soaks:Harvested wicker is placed in and tied up, retains willow bark, often ties a diameter of 10 ~ 12cm, be placed in leaching
Steep in liquid, soak at room temperature 8 ~ 10 hours, take out, obtain immersion wicker;
(2)Primary drying:Immersion wicker is placed in the environment that temperature is 38 ~ 40 DEG C, humidity is 56 ~ 58%, 10 ~ 12 are stood small
When, obtain primary drying wicker;
(3)Wicker is digested:In the water that primary drying wicker is dipped in 2 ~ 3 times of amounts of primary drying wicker weight, complex enzyme is added, in
40 ~ 42 DEG C of insulations are digested 3 ~ 4 hours, are taken out, and obtain enzymolysis liquid and enzymolysis wicker;
(4)Redrying:Wicker will be digested to be placed in the baking oven that temperature is 67 ~ 69 DEG C, drying to water content is 28 ~ 30%, obtains two
Secondary dry wicker;
(5)Wicker ferments:Redrying wicker is dipped in step(3)Enzymolysis liquid in, add starch, make the mass concentration of starch
For 16 ~ 18%, it is well mixed, accesses Angel wine yeast, in 30 ~ 32 DEG C of ferment at constant temperature 3 ~ 4 days, is cooled to 21 ~ 23 DEG C of continuation
Fermentation 9 ~ 10 days, takes out, obtains fermentation wicker;
(6)Wicker ultrasound:Fermentation wicker is placed in ultrasonic liquid, in 52 ~ 54 DEG C, 28 ~ 30kHz ultrasounds 40 ~ 45 minutes, obtains ultrasonic
Wicker;
(7)Three dryings:In the baking oven that ultrasonic wicker is placed in 78 ~ 80 DEG C, drying to water content is 32 ~ 34%, it is cooled to 56 ~
58 DEG C, drying to water content is 15 ~ 17%, and uniform water spray is placed in the environment that humidity is 80 ~ 82% and stands 2 ~ 3 days, makes water content
For 23 ~ 25%, it is 10 ~ 12% to dry again to water content, obtains softening wicker.
2. the sofening treatment method of wicker according to claim 1, it is characterised in that the step(1)Soak, be body
Fraction is 13 ~ 15% alcoholic solution.
3. the sofening treatment method of wicker according to claim 1, it is characterised in that the step(3)Complex enzyme, by with
The raw material of lower parts by weight is made:Cellulase 18 ~ 20, lignoenzyme 12 ~ 14, hemicellulase 10 ~ 12, pectase 4 ~ 6.
4. the sofening treatment method of wicker according to claim 1, it is characterised in that the step(5)Angel grape wine
Yeast, by re-activation, viable count is 109~1010CFU/ml。
5. the sofening treatment method of wicker according to claim 1, it is characterised in that the step(6)Ultrasonic liquid, by with
The raw material of lower parts by weight is made:Potassium dihydrogen phosphate 11 ~ 13, Herba humuli scandentis extract 1.3 ~ 1.5, extract of willow bark 1.1 ~ 1.3, by institute
There is raw material mixing, the stirring that adds water is to being completely dissolved, and the mass concentration for making potassium dihydrogen phosphate is 0.4 ~ 0.5%, obtains ultrasonic liquid.
6. the sofening treatment method of wicker according to claim 5, it is characterised in that described Herba humuli scandentis extract, is by humulus
Grass meal is broken, adds the water of 180 ~ 200 times of amounts of humulus grass weight, it is original 1/20 that heating, which is boiled to volume, and 3 are added water to cook repeatedly
Secondary, filtering, merging filtrate is slowly added to the alcoholic solution that volume fraction is 92 ~ 94% into filtrate, final concentration of to alcohol
62 ~ 64%, stand, filtering, except precipitation, it is 7 ~ 9% that filtrate, which is dried to water content, obtains Herba humuli scandentis extract.
7. the sofening treatment method of wicker according to claim 5, it is characterised in that described extract of willow bark, is collected
The willow bark produced in willow and wicker process, is crushed, and it is 1.7 to add 120 ~ 140 times of amounts of willow bark weight, volume fraction
~ 1.9% acetum, soaks 3 ~ 4 hours, and it is original 1/10 that heating, which is boiled to volume, filter cleaner, by filtrate dry to
Water content is 8 ~ 10%, obtains extract of willow bark.
8. the sofening treatment method of wicker according to claim 1, it is characterised in that the step(7)Drying again, dry
Dry temperature is 51 ~ 53 DEG C.
9. according to the sofening treatment method of any one of claim 1 ~ 8 wicker, obtained softening wicker.
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CN107599097A (en) * | 2017-09-20 | 2018-01-19 | 阜南佳利工艺品有限公司 | A kind of softening method of ash |
CN108748537A (en) * | 2018-06-26 | 2018-11-06 | 阜南县永盛工艺品有限公司 | A kind of thick purple willow softening agent |
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CN106003333A (en) * | 2016-07-13 | 2016-10-12 | 阜南县猛发工艺品有限公司 | Wicker product anti-pest and anti-mildew method capable of enhancing wicker knitting capacity |
CN106042117A (en) * | 2016-07-13 | 2016-10-26 | 阜南县大喜柳编工艺品有限公司 | Fading method for wheat straw |
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CN107599097A (en) * | 2017-09-20 | 2018-01-19 | 阜南佳利工艺品有限公司 | A kind of softening method of ash |
CN109000206A (en) * | 2018-04-26 | 2018-12-14 | 阜南县慧宏柳木工艺品有限公司 | A kind of preparation method of color-change resistant wicker plaiting article lampshade |
CN108748537A (en) * | 2018-06-26 | 2018-11-06 | 阜南县永盛工艺品有限公司 | A kind of thick purple willow softening agent |
CN109049223A (en) * | 2018-09-30 | 2018-12-21 | 德保县广鑫贸易有限公司 | A kind of rattan plaited rattan sofening treatment liquid and preparation method thereof |
CN110561579A (en) * | 2019-08-15 | 2019-12-13 | 阜阳创启工艺品有限公司 | Recycling method of waste Chinese wolfberry and willow bark |
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