CN107149107A - A kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents - Google Patents
A kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents Download PDFInfo
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Abstract
The invention discloses a kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents, its step is：1）Raw material selection, cleaning；2）Peeling：3）Excystation clothing：Tangerine valve is first soaked in 0.4 % hydrochloric acid solution, is soaked in again after rinsing in 0.4 % sodium hydroxide solutions；4）Separate juice born of the same parents：Tangerine valve is immersed in 0.8 % hydrochloric acid solution and rinsed well；5）Juice born of the same parents' cure process：Under the conditions of 30 50 DEG C, it is immersed in 0.3 0.4 % calcium chloride solution after 30 50 min and rinses；6）Sealed storage：Liquid glucose is added in juice born of the same parents after cure process, is boiled after cooling, hot filling, vacuum sealing, normal temperature high voltage sterilizing is carried out.The present invention is conducive to improving the utilization rate of Xinhui citrus reticulata, improves the economic benefit of Xinhui citrus reticulata industry, while reducing cause and effect meat abandons the wasting of resources caused and environmental problem.
Description
Technical field
The invention belongs to food processing field, and in particular to a kind of utilization Xinhui citrus reticulata discards the production that pulp is processed into juice born of the same parents
Method.The committed step for producing juice born of the same parents is optimized the present invention, it is determined that optimal juice born of the same parents' processing technology.
Background technology
Xinhui citrus reticulata, scientific name citrus reticulata"Chachi” (Citrus reticulata cv.Chachiensis), also known as newly can wide old mandarin orange, old
Skin mandarin orange, newly can bright red mandarin orange, Rutaceae Citrus citrus reticulata"Chachi” kind, main product in Xinhui of Guangdong Province, be newly can traditional cultivation Citrus Cultivars,
The cultivation history of existing more than 700 years, because its pericarp has a medicinal and food therapy value and it is well-known at home and abroad, mainly for the production of dried orange peel and
New general tea, but because its pulp taste is sour and astringent, fruit seed is more, and pulp of the accounting again more than 80% is dropped, and abandons processing
Xinhui citrus reticulata pulp has more than 7000 tons every year.Abandoning for Xinhui citrus reticulata pulp can result in environmental pollution and the wasting of resources.Pulp is rich
Containing nutriment, throwing in environment can rot smelly quickly, cause the breeding of a large amount of drosophilas and microorganism growth, have a strong impact on environment
Health.Simultaneously as acidity is high, largely it is deposited in behind local area, the pH value for causing to stack ground soil is changed, destroyed
Original ecological balance, injures the biologies such as original plant, microorganism, protozoan, brings bigger environmental problem.
Substantial amounts of organic acid, nutriment are rich in Xinhui citrus reticulata pulp, it is also yellow containing natural complex, dietary fiber, class
Ketone.Pulp (containing fruit seed) 0.7-0.8g/100mL containing citric acid, containing sugared 10.1-10.3g/100mL, soluble solid is 11-
12%.Organic acid mainly contains citric acid, oxalic acid, lactic acid, tartaric acid, acetic acid, pyruvic acid, ketoglutaric acid, butanedioic acid in Xinhui citrus reticulata
Deng 8 kinds of organic acids, and citric acid and total acid content apparently higher than other fruit.In fruit seed rich in the nutrition such as limonin and
Bioactive substance, with edible and medical value well.
Therefore, the utilization of pulp is discarded to Xinhui citrus reticulata, not only contributes to improve the utilization rate of Xinhui citrus reticulata, increase Xinhui citrus reticulata adds
Chemical product species, improves the economic benefit of Xinhui citrus reticulata industry, increases new deep processed product, is caused while reducing cause and effect meat and abandoning
The wasting of resources and environmental problem.Research at present to Xinhui citrus reticulata pulp is less, focuses primarily upon Xinhui citrus reticulata pericarp and plantation
The research of technology, only Bai Weidong are processed into fruit drink, fruit vinegar and debitterness technology to Xinhui citrus reticulata and studied.In the market has
The product for closing Xinhui citrus reticulata is mainly in pericarp Related product, such as new meeting Pu'er tea, Xinhui tangerine peel, and on the product base of pulp
It is blank on this.Present invention firstly provides discarding pulp using Xinhui citrus reticulata to be processed into juice born of the same parents' product, juice born of the same parents' process is mainly deposited
Juice born of the same parents wither it is flat, broken, fade and juice intracellular nutriment be lost in the problems such as, the present invention juice born of the same parents' processing technology is optimized
It can reduce in juice born of the same parents' process and lose, the quality of juice born of the same parents can be improved, the hardness of juice born of the same parents is largely improved by hardening, is carried
The sharp and clear sense that high juice born of the same parents chew.Production food industry juice born of the same parents can be applied to the every field of food processing, so as to reduce citrus Sheng
Produce waste of the season caused by storing the reasons such as improper, excess supply.
The content of the invention
It is an object of the invention to provide a kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents, existing market has been filled up empty
In vain, the utilization rate of Xinhui citrus reticulata pulp is improved, cause and effect meat is reduced and abandons the wasting of resources caused and environmental problem, comprehensive utilization ratio
It is high.
To achieve these goals, the present invention uses following technical scheme：
A kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents, comprises the following steps：
1) raw material selection, cleaning：The lossless complete Xinhui citrus reticulata fruit without insect pest of selection is cleaned, removal surface soil,
Impurity；
2) remove the peel：Xinhui citrus reticulata blanching 30-50s in 85-95 DEG C of hot water, removes the peel after pulling out, removes white network, point valve；
3) excystation clothing：Tangerine valve is soaked in 0.4% hydrochloric acid solution and soaked after 25-35min, is leached, HCl treatment liquid
Recycle, remove seed after the rinsing of tangerine valve；Then, then by the tangerine valve after rinsing it is immersed in 40-45 DEG C of 0.4% sodium hydroxide solution
Middle 15-20min, is leached, and rinses tangerine valve；
4) juice born of the same parents are separated：Tangerine valve is immersed in 0.8% hydrochloric acid solution after 20-25min, leached, HCl treatment liquid is returned
Receive and utilize, juice born of the same parents are rinsed with 200-300mL/s running water, so that juice born of the same parents separate；
5) juice born of the same parents cure process：Under the conditions of 30-50 DEG C, the juice born of the same parents after gradation are immersed in 0.3-0.4% calcium chloride
In solution after 30-50min, leach, rinse juice born of the same parents；
6) sealed storage：Syrup is added in juice born of the same parents after cure process, heating is cooled to 85-95 DEG C and carries out heat after boiling
It is filling, it is transferred to after to be cooled to 60-65 DEG C in vacuum seal bag and vacuumizes sealing, high pressure sterilization processing is made food industry
Use juice born of the same parents；The sugar concentration of addition is calculated according to following formula：
Y=(W3Z-W1X)/W2
Y- should match somebody with somebody the concentration %, W of syrup1- every tank adds the weight of juice born of the same parents, W2- every tank adds the weight of syrup, W3- per tank
Gross weight, soluble solid content % in juice born of the same parents before content %, the X- tinning of soluble solid when Z- requires can opening；
Soluble solid content (X) is 49-61% in wherein filling preceding juice born of the same parents, it is desirable to the content of soluble solid during can opening
(Z) it is 9-12%.
Preferably, step 5) in juice born of the same parents be immersed in 40 DEG C of 0.4% calcium chloride immersion and hardened for 50 minutes.
Compared with prior art, the present invention has advantages below and beneficial effect：
(1) process optimization processing can effectively improve the hardening effect of juice born of the same parents, substantially near 100%；
(2) process optimization and the damage and nutrition that can effectively reduce juice born of the same parents in processing technology using non-thermal sterilization processing are damaged
Lose；
(3) using the juice born of the same parents full grains of the discarded processing of Xinhui citrus reticulata, with higher sharp and clear sense, form is consistent, and juice born of the same parents are saturating
It is bright, no color differnece each other, without flat, broken, muddiness of withering.
Brief description of the drawings
Fig. 1 is influence of the different disposal method to Xinhui citrus reticulata excystation clothing effect.
Fig. 2 is influence of the different disposal method to Xinhui citrus reticulata juice born of the same parents' dispersion effect.
Fig. 3 is influence of the different calcium chloride concentrations to Xinhui citrus reticulata juice born of the same parents' hardness.
Fig. 4 is influence of the calcium chloride different disposal time to Xinhui citrus reticulata juice born of the same parents' hardness.
Fig. 5 is influence of the calcium chloride different disposal temperature to Xinhui citrus reticulata juice born of the same parents' hardness.
Embodiment
Embodiment 1：The selection of excystation clothing method
Blanching is removed the peel, white network is removed, the tangerine valve of point valve carries out alkali after first acid, acid, enzyme process carry out excystation clothing after first alkali respectively
Processing, using full excystation clothing rate and soluble solid loss late as index, determines the excystation clothing best approach.
Experiment is comprised the following steps that：
1. Xinhui citrus reticulata blanching 30-50s in 85-95 DEG C of hot water, removes the peel, removes white network, point valve manually while hot after pulling out；
2. excystation clothing：
Method one：Alkali after first sour.According to tangerine valve and 0.4% hydrochloric acid mass ratio 1:1.5 ratio, both are mixed, often
Temperature processing 30min after, leach, reclaim HCl treatment liquid, flowing water rinse 3min after, then with tangerine valve with 0.4% sodium hydroxide it is molten
Liquid mass ratio is 1：1.5 ratio mixes both, and 15min is handled in 40 DEG C of water-baths, leaches, and flowing water rinses 3min.
Method two：It is sour after first alkali.Using tangerine valve and 0.4% sodium hydroxide solution mass ratio as 1：1.5 ratio incite somebody to action both
Mixing, handles 15min in 40 DEG C of water-baths, leaches, and flowing water is rinsed after 3min, then with tangerine valve and 0.4% hydrochloric acid mass ratio
For 1：1.5 ratios mix both, after normal temperature processing 30min, leach, reclaim HCl treatment liquid, flowing water rinses 3min.
Method three：Enzyme process.Using tangerine valve and 1% pectinase solution mass ratio as 1：1.5 ratio mixes both, 45
30min is handled in DEG C water-bath, is leached, pectinase treatment liquid is reclaimed, flowing water rinses 3min.
3. the standard of excystation clothing is that peel is easy to fall off, not cornerite, gizzard does not loosen, organized not soft rotten.Excystation
Drained after clothing, weigh full excystation clothing weight.
Experiments prove that (see Fig. 1), first the full excystation clothing rate of alkaline process is 92.13%, soluble solid loss late after acid
For 7.97%；The full excystation clothing rate of acid system is 46.98% after first alkali, and soluble solid loss late is 8.03%；The full excystation of enzyme process
Clothing rate is 71.08%, and soluble solid loss late is 2.78%.Therefore, the present invention uses the method for alkali after first acid to new meeting
The carry out excystation clothing of mandarin orange.
Embodiment 2：The selection of juice born of the same parents' process for dispersing
The tangerine valve of peel will be removed, direct acid soak, the immersion of direct alkali are carried out respectively, first acid, enzyme process enter after alkali, first alkali after acid
The processing of row gradation, using juice born of the same parents dispersion rate, soluble solid loss late and juice born of the same parents breakage rate as index, determines that juice born of the same parents are scattered optimal
Method.
Experiment is comprised the following steps that：
1. juice born of the same parents disperse：
Method one：Direct acid soak.With pulp and 0.8% hydrochloric acid solution mass ratio 1:1.5 ratio mixes both, often
After temperature processing 20min, leach, reclaim HCl treatment liquid, juice born of the same parents rinse 3min with 200-300mL/s running water.
Method two：Direct alkali immersion.With pulp and 0.3% sodium hydroxide solution mass ratio 1:1.5 ratio mixes both
Close, after normal temperature processing 20min, leach, juice born of the same parents rinse 3min with 200-300mL/s running water.
Method three：Alkali after first sour.With pulp and 0.8% hydrochloric acid solution mass ratio 1：1.5 ratios mix both, normal temperature
Handle after 20min, leach, reclaim HCl treatment liquid, rinsed with 200-300mL/s flowing water after 3min, then with pulp and 0.3%
Sodium hydroxide solution mass ratio is 1：1.5 ratio mixes both, normal temperature processing 5min, leaches, with 200-300mL/s flowing water
Rinse 3min.
Method four：It is sour after first alkali.With pulp and 0.3% sodium hydroxide solution mass ratio 1：1.5 ratio mixes both
Close, normal temperature processing 20min is leached, rinsed with 200-300mL/s flowing water after 3min, then with pulp and 0.8% hydrochloric acid solution matter
Amount is than being 1：1.5 ratios mix both, after normal temperature processing 5min, leach, reclaim HCl treatment liquid, flowed with 200-300mL/s
Water rinses 3min.
Method five：Enzyme process.Using mass ratio as 1：1.5 ratio mixing pulp and distilled water, adding mass fraction is
0.015% pectase, 0.01% cellulase, soak 50min at 50 DEG C, leach, and reclaim enzyme liquid, are flowed with 200-300mL/s
Water rinses 3min.
2. juice born of the same parents' damage testing uses decoration method, juice born of the same parents are soaked into 5min with 0.1% light blue solution, clear water floats after bleeding
Wash clean, chromomere is damaged juice born of the same parents.
Experiments prove that (see Fig. 2), direct acid soak juice born of the same parents dispersion rate is 99.02%, soluble solid loss late
For 8.95%, juice born of the same parents percentage of damage is 10.13%；Direct alkali immersion juice born of the same parents dispersion rate is 84.56%, soluble solid loss late
For 9.74%, juice born of the same parents percentage of damage is 13.56%；First alkaline process juice born of the same parents dispersion rate is 99.27%, soluble solid loss late after acid
For 14.12%, juice born of the same parents percentage of damage is 19.53%；Sour juice born of the same parents dispersion rate is 87.25%, soluble solid loss late after first alkali
For 13.41%, juice born of the same parents percentage of damage is 21.31%；Enzyme process juice born of the same parents dispersion rate is 73.78%, and soluble solid loss late is
2.87%, juice born of the same parents percentage of damage is 3.76%.Therefore, the present invention disperses the juice born of the same parents of Xinhui citrus reticulata using acid soak method.
Embodiment 3：Hardening process optimizes
After excystation clothing, juice born of the same parents' process for dispersing is determined, using juice born of the same parents hardness as evaluation index, different chlorinations are chosen respectively
Calcium concentration, time, temperature carry out single factor experiment, and by orthogonal test, it is determined that the parameter of optimal hardening process.
Experiment is comprised the following steps that：
1. the method disperseed by above-mentioned excystation clothing, juice born of the same parents obtains juice born of the same parents；
Hardened 2. juice born of the same parents are immersed in calcium chloride solution, handle 40min in 40 DEG C of water-baths, calcium chloride it is dense
Degree is respectively 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, is leached, and flowing water rinses 3min, as a result sees Fig. 3；
Juice born of the same parents' hardness is measured using Texture instrument, the location parameter of physical property measurement：Mode determination：ReturnTo
Start；Determine probe：P/2N needle probes (diameter 2mm), speed 5mm/s before test；Test speed 2mm/s；Speed after test
5mm/s；Paracentesis depth 0.1mm；Trigger power 3g；
Evaluation method：Juice born of the same parents hardness does not pierce rate as evaluation index under the conditions of power to trigger.30-35 juice born of the same parents are taken to enter at random
Row is punctured in experiment, puncture process, if resistance is close with trigger force suffered by probe, you can think that juice born of the same parents are not pierced；Conversely,
If resistance suffered by probe is much larger than trigger force, you can think that juice born of the same parents are pierced.Juice born of the same parents' sample as obtained by three repetition experiments
The average juice born of the same parents' hardness not pierced obtained by the different cure process conditions of rate (i.e. not by the percentage of piercing juice born of the same parents) evaluation；
3. juice born of the same parents are mixed with 0.4% calcium chloride solution, handled in 40 DEG C of water-baths, processing time is respectively
10min, 20min, 30min, 40min, 50min, are leached, and flowing water rinses 3min；As a result texture measurement is shown in Fig. 4 with 2；
4. juice born of the same parents are mixed with 0.4% calcium chloride solution, locate in 20 DEG C, 30 DEG C, 40 DEG C, 50 DEG C, 60 DEG C of water-baths
40min is managed, is leached, flowing water rinses 3min；As a result texture measurement is shown in Fig. 5 with 2；
According to above-mentioned Optimal Experimental, the present invention in 0.3-0.4% calcium chloride from being hardened, at 30-50 DEG C, immersion
30-50 minutes.Juice born of the same parents harden the optimal treatment condition tested：Juice born of the same parents are immersed in the calcium chloride solution that concentration is 0.4%,
50min is handled under the conditions of 40 DEG C, juice born of the same parents do not pierce rate and reach 98.12%.
The quadrature analysis that the different curing conditions of table 1 influence on juice born of the same parents hardness
Implement 4：The method that juice born of the same parents are processed using Xinhui citrus reticulata pulp
The present invention develops a kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents according to embodiment 1-3 Optimal Experimental,
Its step is：
1) raw material selection, cleaning：The lossless complete Xinhui citrus reticulata fruit without insect pest of selection is cleaned, removal surface soil,
Impurity；
2) remove the peel：Xinhui citrus reticulata blanching 30-50s in 85-95 DEG C of hot water, removes the peel after pulling out, removes white network, point valve；
3) excystation clothing：At normal temperatures, tangerine valve is soaked in 0.4% hydrochloric acid solution and soaked after 25-35min, leached, salt
Pickling agent is recycled, remove seed after the rinsing of tangerine valve；Then, then by the tangerine valve after rinsing it is immersed in 40-45 DEG C of 0.4% hydrogen-oxygen
Change 15-20min in sodium solution, leach, rinse tangerine valve；
4) juice born of the same parents are separated：Tangerine valve is immersed in 0.8% hydrochloric acid solution after 20-25min at normal temperatures, leached, hydrochloric acid
Treatment fluid is recycled, and juice born of the same parents are rinsed with 200-300mL/s running water, so that juice born of the same parents separate；
5) juice born of the same parents cure process：Under the conditions of 30-50 DEG C, the juice born of the same parents after gradation are immersed in 0.3-0.4% calcium chloride
In solution after 30-50min, leach, rinse juice born of the same parents；
6) sealed storage：Syrup is added in juice born of the same parents after cure process, heating is cooled to after 85-95 DEG C after boiling, entered
Row hot filling, is transferred in vacuum seal bag after to be cooled to 60-65 DEG C, carries out vacuumizing sealing immediately, then will be sealed
Soft Roll be installed in high-voltage apparatus container and (set pressure and dwell time as 500MPa, 5min) and killed at ambient temperature
Bacterium is handled, that is, food industry is made and uses juice born of the same parents；The sugar concentration of addition is calculated according to following formula：
Y=(W3Z-W1X)/W2
Y- should match somebody with somebody the concentration (%) of syrup, W1- every tank adds the weight (g) of juice born of the same parents, W2- every tank adds the weight of syrup
(g), W3- the gross weight (g) per tank, the content (%) of soluble solid during Z- requirement can openings, can in juice born of the same parents before X- tinnings
Dissolubility solid content %
Soluble solid content is 49-61% (X) in filling preceding juice born of the same parents, it is desirable to the soluble solid (Z) during can opening
Content be 9-12%.
The full excystation clothing rate of Xinhui citrus reticulata juice born of the same parents prepared using the above method is soluble solid during excystation clothing up to 91.78%
Shape thing loss late is reduced to 6.56%；Juice born of the same parents dispersion rate is up to 99.02%, and juice born of the same parents' percentage of damage is reduced to 10.13%, soluble solid
Thing loss late is reduced to 7.95%；Unhardened processing juice born of the same parents do not pierce rate for 49.47%, and the unbroken rate of juice born of the same parents reaches after cure process
98.14%, hardening effect lifting 98.38%.
Claims (2)
1. a kind of method that utilization Xinhui citrus reticulata pulp processes juice born of the same parents, it is characterised in that comprise the following steps：
1) raw material selection, cleaning：The lossless complete Xinhui citrus reticulata fruit without insect pest of selection is cleaned, and removes surface soil, impurity；
2) remove the peel：Xinhui citrus reticulata blanching 30-50s in 85-95 DEG C of hot water, removes the peel after pulling out, removes white network, point valve；
3) excystation clothing：Tangerine valve is soaked in 0.4% hydrochloric acid solution and soaked after 25-35min, is leached, HCl treatment liquid is reclaimed
Utilize, remove seed after the rinsing of tangerine valve；Then, then by the tangerine valve after rinsing it is immersed in 40-45 DEG C of 0.4% sodium hydroxide solution
15-20min, is leached, and rinses tangerine valve；
4) juice born of the same parents are separated：Tangerine valve is immersed in 0.8% hydrochloric acid solution after 20-25min, leached, HCl treatment liquid reclaims profit
With by juice born of the same parents with 200-300mL/s running water flushing, so that juice born of the same parents separate；
5) juice born of the same parents cure process：Under the conditions of 30-50 DEG C, the juice born of the same parents after gradation are immersed in 0.3-0.4% calcium chloride solution
After middle 30-50min, leach, rinse juice born of the same parents；
6) sealed storage：Syrup is added in juice born of the same parents after cure process, heating is cooled to 85-95 DEG C and carries out hot filling after boiling
Fill, be transferred to after to be cooled to 60-65 DEG C in vacuum seal bag and vacuumize sealing, high pressure sterilization processing is made food industry and uses
Juice born of the same parents；The sugar concentration of addition is calculated according to following formula：
Y=(W3Z-W1X)/W2
Y- should match somebody with somebody the concentration %, W of syrup1- every tank adds the weight of juice born of the same parents, W2- every tank adds the weight of syrup, W3- total per tank
Weight, soluble solid content % in juice born of the same parents before content %, the X- tinning of soluble solid during Z- requirement can openings；Wherein
Soluble solid content is 49-61% in filling preceding juice born of the same parents, it is desirable to which the content of soluble solid during can opening is 9-12%.
2. the method that utilization Xinhui citrus reticulata pulp according to claim 1 processes juice born of the same parents, it is characterised in that step 5) in juice born of the same parents
Immersion in 40 DEG C of 0.4% calcium chloride is immersed in be hardened within 50 minutes.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2020253232A1 (en) * | 2019-06-20 | 2020-12-24 | 浙江大学 | Citrus piece processing method directly utilizing acid-alkali process water |
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| CN102488151A (en) * | 2011-11-17 | 2012-06-13 | 中国农业科学院柑桔研究所 | Technology for producing citrus juice sac through peeling and capsule dressing removal of whole fruits |
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| WO2020253232A1 (en) * | 2019-06-20 | 2020-12-24 | 浙江大学 | Citrus piece processing method directly utilizing acid-alkali process water |
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