CN107142082A - Smart lock water blocking leakage material fabrication process and its application method in a kind of pipeline - Google Patents
Smart lock water blocking leakage material fabrication process and its application method in a kind of pipeline Download PDFInfo
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- CN107142082A CN107142082A CN201710428815.3A CN201710428815A CN107142082A CN 107142082 A CN107142082 A CN 107142082A CN 201710428815 A CN201710428815 A CN 201710428815A CN 107142082 A CN107142082 A CN 107142082A
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/12—Materials for stopping leaks, e.g. in radiators, in tanks
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Abstract
The invention discloses smart lock water blocking leakage material fabrication process and its application method in a kind of pipeline, using diatomite, sepiolite, urea and oxalic acid as main material, by bakeing, scattered, centrifugation, removal of impurities, the step such as stir, remix and obtain this product；The present invention need to hold water quality according to liquid pipe and select the specific quality of this product, and pipeline is blended into after then being diluted with more than 80 DEG C pure water.Smart lock water blocking leakage material fabrication process and its application method do not contain noxious material in a kind of pipeline that the present invention is provided, will not be in water pipe residual hazard material, when there is leak source in pipeline, without where detecting leak source, without excavating comb line, directly using smart lock water loss circulation material in the pipeline that provides of the present invention can the time required to leak stopping, and this product leak stopping it is short, it is simple to operate.
Description
Technical field
The present invention relates to a kind of smart lock water leakage stopping technology, smart lock water loss circulation material system in more particularly to a kind of pipeline
Make method and its application method.
Background technology
The problem of Chinese cities and towns heating system leak is one universal, the daily water leakage in Chinese cities and towns is average in output
7~10% or so.Because most pipe network water pipeline is to be embedded in underground, it is difficult to touched, to being sealed with very for leak pipeline
Big difficulty, is all with excavating leak source sealed method again at present.However, this method first has to where judge leak source, then
The leak source ground judged is excavated, leak source and leakage cause is confirmed, joint is then changed again or the depot siding is repaired, or
Person's butt joint is tightened again, or sealant is first smeared at butt joint the method such as connects again again and repaired.Because being difficult to accurate
Judge leak source position, can not find leak source on the contrary after usually being excavated on the ground of buried pipeline, have to again bury, move to another place again
Excavate, untill finding leak source.And often leak source has many to a set of pipe-line system, the water leakage of single leak source may not
Greatly, also lose total water leakage even if finding several leak sources, after sealing to significantly reduce.In a word, this method, efficiency is very low.
The content of the invention
The invention aims to overcome the shortcomings of above-mentioned background technology, there is provided smart lock water blocking leakage material in a kind of pipeline
Expect preparation method and its application method, make its Automatic-searching leak source, leak stopping can be carried out without excavating comb line.
The preparation method of smart lock water loss circulation material in a kind of pipeline that the present invention is provided, it comprises the following steps：
S1：By the sepiolite of the diatomite of the mesh of 50 mesh -250 and the mesh of 50 mesh -250 using mass ratio as diatomite：Sepiolite=
0.5-2 ratios are mixed, and mixture is inserted into 180 DEG C of oven-bakeds 24 hours, and furnace cooling obtains A material；
S2：By urea and oxalic acid using mass ratio as urea：Oxalic acid=5-20, stirring and dissolving is to isopropanol and nothing at 42 DEG C
In water-ethanol, the solution after dissolving is slowly added dropwise in A material, ageing is standby, obtains B material；
S3：Take 10%-20%B material to be scattered in the mixed solution of absolute ethyl alcohol and acetonitrile, disperse 40 minutes, in stirring bar
The ammoniacal liquor that mass fraction is 27% is added under part, C material are obtained；
S4：In the mixed liquor that triethanolamine is dissolved in tetra-n-butyl titanate and absolute ethyl alcohol, stirring 20min is clear to solution
Clearly, mixed liquor is added drop-wise to dropwise under agitation in C material, continues to stir 2h, obtain D material；
S5：The pale precipitation in D material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation is dried
Be placed in after dry grinding in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to after 24 hours
Room temperature, obtains batch mixing E；
S6：Remaining mixed material B and batch mixing E are placed in batch mixer, to be stirred in the aqueous solution of 5% citric acid at 100 DEG C
Mix, sealed after air cooling, obtain final products F.
Intelligence in the application method of smart lock water loss circulation material, described pipeline in a kind of pipeline for the offer that the present invention is provided
Energy water lock loss circulation material F need to hold water quality according to liquid pipe and select the specific quality of this product, then dilute with 80 DEG C of pure water are more than
Pipeline is blended into after releasing.
Beneficial effect：Smart lock water blocking leaks material fabrication process and its application method not in a kind of pipeline that the present invention is provided
Containing noxious material, will not in water pipe residual hazard material, when leak source occurs in pipeline, without detect leak source where,
, directly can leak stopping, and this product using smart lock water loss circulation material in the pipeline that provides of the present invention without excavating comb line
It is short the time required to leak stopping, it is simple to operate.
Embodiment
With reference to embodiment, the present invention will be described in detail, the description of this part be only it is exemplary and explanatory, no
Reply protection scope of the present invention has any restriction effect.
The preparation method that embodiment of the present invention provides smart lock water loss circulation material in a kind of pipeline, it includes following step
Suddenly：
S1：By the sepiolite of the diatomite of the mesh of 50 mesh -250 and the mesh of 50 mesh -250 using mass ratio as diatomite：Sepiolite=
0.5-2 ratios are mixed, and mixture is inserted into 180 DEG C of oven-bakeds 24 hours, and furnace cooling obtains A material；
S2：By urea and oxalic acid using mass ratio as urea：Oxalic acid=5-20, stirring and dissolving is to isopropanol and nothing at 42 DEG C
In water-ethanol, the solution after dissolving is slowly added dropwise in A material, ageing is standby, obtains B material；
S3：Take 10%-20% B to expect to be scattered in the mixed solution of absolute ethyl alcohol and acetonitrile, disperse 40 minutes, in stirring
Under the conditions of add the ammoniacal liquor that mass fraction is 27%, obtain C material, specifically, the volume ratio of absolute ethyl alcohol and acetonitrile is anhydrous
Ethanol：Acetonitrile=3；
S4：In the mixed liquor that triethanolamine is dissolved in tetra-n-butyl titanate and absolute ethyl alcohol, stirring 20min is clear to solution
Clearly, mixed liquor is added drop-wise to dropwise under agitation in C material, continues to stir 2h, obtain D material；
S5：The pale precipitation in D material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation is dried
Be placed in after dry grinding in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to after 24 hours
Room temperature, obtains batch mixing E, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B is placed in batch mixer with batch mixing E, to be stirred in the aqueous solution of 5% citric acid at 100 DEG C,
Sealed after air cooling, obtain final products F.
For preferably using smart lock water loss circulation material in a kind of pipeline of the invention provided, the present embodiment additionally provides one
Smart lock water loss circulation material F need to be according to liquid-phase tube in the application method of smart lock water loss circulation material, described pipeline in kind pipeline
Road holds water quality and selectes the specific quality of this product, then with pipeline is blended into after more than 80 DEG C pure water dilutions, specifically, the pipeline
It is 5000 to hold water quality with smart lock water loss circulation material F mass ratioes in the pipeline:3, smart lock water blocking leakage material in the pipeline
The mass ratio for expecting F and 80 DEG C of pure water is 1:2.
Embodiment 1：
The preparation method that embodiment of the present invention provides smart lock water loss circulation material in a kind of pipeline, it includes following step
Suddenly：
S1：By the sepiolite of the diatomite of 100 mesh and 100 mesh using mass ratio as diatomite：Sepiolite=0.5 ratio is mixed
Close, wherein diatomite 500g, sepiolite 1000g, mixture is inserted into 180 DEG C of oven-bakeds 24 hours, furnace cooling obtains A1
Material；
S2：By urea 300g, oxalic acid 35g, at 42 DEG C stirring and dissolving into 500ml isopropanols and 500ml absolute ethyl alcohols,
Solution after dissolving is slowly added dropwise in A1 material, ageing is standby, obtains B1 material；
S3：300gB material are taken to be scattered in absolute ethyl alcohol with acetonitrile volume ratio in 3 mixed solution 100ml, to disperse 40min,
The ammoniacal liquor that 60ml mass fractions are 27% is added under agitation, obtains C1 material；
S4：Take 220ml tetra-n-butyl titanates and 200ml absolute ethyl alcohols to mix, 20g triethanolamines are dissolved in above-mentioned metatitanic acid four
In the mixed liquor of N-butyl and absolute ethyl alcohol, stirring 20min to solution is clarified, and mixed liquor is added drop-wise to dropwise under agitation
In C1 material, continue to stir 2h, obtain D1 material；
S5：The pale precipitation in D1 material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation is dried
Be placed in after dry grinding in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to after 24 hours
Room temperature, obtains batch mixing E1, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B 1 and batch mixing E1 are placed in batch mixer, with the water-soluble of 100ml5% citric acids at 100 DEG C
Stirred in liquid, sealed after air cooling, obtain final products F1.
Water capacity be 5000kg pipe-line system, with acupuncture break an aperture, open pipe-line system water circulation when
Waiting can substantially observe that water sprays from aperture.The 3kg samples for taking the present embodiment to provide are then pure with 80 DEG C more than 6kg
Pipeline is blended into after water dilution and starts timing, finds that water spray starts to slow down after 5 minutes, no longer leak is found after 7 minutes.
Embodiment 2：
The preparation method that embodiment of the present invention provides smart lock water loss circulation material in a kind of pipeline, it includes following step
Suddenly：
S1：By the sepiolite of the diatomite of 100 mesh and 100 mesh using mass ratio as diatomite：The mixing of the ratio of sepiolite=1,
Wherein diatomite 1000g, sepiolite 1000g, insert 180 DEG C of oven-bakeds 24 hours, furnace cooling obtains A2 by mixture
Material；
S2：By urea 300g, oxalic acid 35g, at 42 DEG C stirring and dissolving into 500ml isopropanols and 500ml absolute ethyl alcohols,
Solution after dissolving is slowly added dropwise in A2 material, ageing is standby, obtains B2 material；
S3：300gB material are taken to be scattered in absolute ethyl alcohol with acetonitrile volume ratio in 3 mixed solution 100ml, to disperse 40min,
The ammoniacal liquor that 60ml mass fractions are 27% is added under agitation, obtains C2 material；
S4：Take 220ml tetra-n-butyl titanates and 200ml absolute ethyl alcohols to mix, 20g triethanolamines are dissolved in above-mentioned metatitanic acid four
In the mixed liquor of N-butyl and absolute ethyl alcohol, stirring 20min to solution is clarified, and mixed liquor is added drop-wise to dropwise under agitation
In C2 material, continue to stir 2h, obtain D2 material；
S5：The pale precipitation in D2 material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation is dried
Be placed in after dry grinding in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to after 24 hours
Room temperature, obtains batch mixing E2, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B 2 and batch mixing E2 are placed in batch mixer, with the water-soluble of 100ml5% citric acids at 100 DEG C
Stirred in liquid, sealed after air cooling, obtain final products F2.
Water capacity be 5000kg pipe-line system, with acupuncture break an aperture, open pipe-line system water circulation when
Waiting can substantially observe that water sprays from aperture.The 3kg samples for taking the present embodiment to provide are then pure with 80 DEG C more than 6kg
Pipeline is blended into after water dilution and starts timing, finds that water spray starts to slow down after 3 minutes, no longer leak is found after 4 minutes.
Embodiment 3：
The preparation method that embodiment of the present invention provides smart lock water loss circulation material in a kind of pipeline, it includes following step
Suddenly：
S1：By the sepiolite of the diatomite of 100 mesh and 100 mesh using mass ratio as diatomite：The mixing of the ratio of sepiolite=2,
Wherein diatomite 2000g, sepiolite 1000g, insert 180 DEG C of oven-bakeds 24 hours, furnace cooling obtains A3 by mixture
Material；
S2：By urea 300g, oxalic acid 35g, at 42 DEG C stirring and dissolving into 500ml isopropanols and 500ml absolute ethyl alcohols,
Solution after dissolving is slowly added dropwise in A3 material, ageing is standby, obtains B3 material；
S3：300gB material are taken to be scattered in absolute ethyl alcohol with acetonitrile volume ratio in 3 mixed solution 100ml, to disperse 40min,
The ammoniacal liquor that 60ml mass fractions are 27% is added under agitation, obtains C3 material；
S4：Take 220ml tetra-n-butyl titanates and 200ml absolute ethyl alcohols to mix, 20g triethanolamines are dissolved in above-mentioned metatitanic acid four
In the mixed liquor of N-butyl and absolute ethyl alcohol, stirring 20min to solution is clarified, and mixed liquor is added drop-wise to dropwise under agitation
In C3 material, continue to stir 2h, obtain D3 material；
S5：The pale precipitation in D3 material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation is dried
Be placed in after dry grinding in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to after 24 hours
Room temperature, obtains batch mixing E3, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B 3 and batch mixing E3 are placed in batch mixer, with the water-soluble of 100ml5% citric acids at 100 DEG C
Stirred in liquid, sealed after air cooling, obtain final products F3.
Water capacity be 5000kg pipe-line system, with acupuncture break an aperture, open pipe-line system water circulation when
Waiting can substantially observe that water sprays from aperture.The 3kg samples for taking the present embodiment to provide are then pure with 80 DEG C more than 6kg
Pipeline is blended into after water dilution and starts timing, finds that water spray starts to slow down after 6 minutes, no longer leak is found after 8 minutes.
Smart lock water loss circulation material can be without inspection in the pipeline that the present invention is provided it can be seen from above three embodiment
Leak hunting a little, leak can be blocked by being directly blended into this material configured.And embodiment 1-3 can be seen that when diatomite with
Sepiolite mass ratio is 1:It is most short the time required to playing leak stopping when 1, when diatomite and sepiolite mass ratio are 2:1 when
It is most long the time required to having waited leak stopping effect.
Smart lock water blocking leakage material fabrication process and its application method do not contain poisonous in a kind of pipeline that the present invention is provided
Material, will not be in water pipe residual hazard material, when leak source occurs in pipeline, without where detecting leak source, without excavating
Comb line, directly can be needed for leak stopping, and this product leak stopping using smart lock water loss circulation material in the pipeline that provides of the present invention
Time is short, simple to operate.
Obviously, those skilled in the art can carry out the essence of various changes and modification without departing from the present invention to the present invention
God and scope.So, if these modifications and variations of the present invention belong to the scope of the claims in the present invention and its equivalent technologies
Within, then the present invention is also intended to comprising including these changes and modification.
Claims (8)
1. the preparation method of smart lock water loss circulation material in a kind of pipeline, it is characterised in that：It comprises the following steps：
S1：By the sepiolite of the diatomite of the mesh of 50 mesh -250 and the mesh of 50 mesh -250 using mass ratio as diatomite：Sepiolite=0.5-2
Ratio is mixed, and mixture is inserted into 180 DEG C of oven-bakeds 24 hours, and furnace cooling obtains A material；
S2：By urea and oxalic acid using mass ratio as urea：Oxalic acid=20-5, stirring and dissolving is to isopropanol and anhydrous second at 42 DEG C
In alcohol, the solution after dissolving is slowly added dropwise in A material, ageing is standby, obtains B material；
S3：10%-20%B material are taken to be scattered in the mixed solution of absolute ethyl alcohol and acetonitrile, it is scattered 40 minutes, under agitation
The ammoniacal liquor that mass fraction is 27% is added, C material are obtained；
S4：In the mixed liquor that triethanolamine is dissolved in tetra-n-butyl titanate and absolute ethyl alcohol, stirring 20min to solution is clarified, will
Mixed liquor is added drop-wise in C material dropwise under agitation, continues to stir 2h, obtains D material；
S5：The pale precipitation in D material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation drying is ground
Be placed in after mill in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to room after 24 hours
Temperature, obtains batch mixing E；
S6：Remaining mixed material B and batch mixing E are placed in batch mixer, it is empty to be stirred in the aqueous solution of 5% citric acid at 100 DEG C
Sealed after cold, obtain final products F.
2. the preparation method of smart lock water loss circulation material in a kind of pipeline as claimed in claim 1, it is characterised in that：The S3
In, the volume ratio of absolute ethyl alcohol and acetonitrile is absolute ethyl alcohol：Acetonitrile=3.
3. the preparation method of smart lock water loss circulation material in a kind of pipeline as claimed in claim 1, it is characterised in that：The S5
Middle separation method is centrifuges, and seperator rotating speed is not less than 1000r/min.
4. the preparation method of smart lock water loss circulation material in a kind of pipeline as claimed in claim 1, it is characterised in that：
It comprises the following steps：
S1：By the sepiolite of the diatomite of 100 mesh and 100 mesh using mass ratio as diatomite：The mixing of the ratio of sepiolite=0.5, its
Middle diatomite 500g, sepiolite 1000g, 180 DEG C of oven-bakeds are inserted 24 hours by mixture, and furnace cooling obtains A1 material；
S2：By urea 300g, oxalic acid 35g, stirring and dissolving, will be molten into 500ml isopropanols and 500ml absolute ethyl alcohols at 42 DEG C
Solution after solution is slowly added dropwise in A1 material, and ageing is standby, obtains B1 material；
S3：300gB material are taken to be scattered in absolute ethyl alcohol with acetonitrile volume ratio in 3 mixed solution 100ml, scattered 40min is being stirred
The ammoniacal liquor that 60ml mass fractions are 27% is added under the conditions of mixing, C1 material are obtained；
S4：Take 220ml tetra-n-butyl titanates and 200ml absolute ethyl alcohols to mix, 20g triethanolamines are dissolved in the positive fourth of above-mentioned metatitanic acid four
In the mixed liquor of ester and absolute ethyl alcohol, stirring 20min to solution is clarified, and mixed liquor is added drop-wise to C1 material dropwise under agitation
In, continue to stir 2h, obtain D1 material；
S5：The pale precipitation in D1 material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation drying is ground
Be placed in after mill in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to room after 24 hours
Temperature, obtains batch mixing E1, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B 1 and batch mixing E1 are placed in batch mixer, with the aqueous solution of the citric acids of 100ml 5% at 100 DEG C
Sealed after middle stirring, air cooling, obtain final products F1.
5. the preparation method of smart lock water loss circulation material in a kind of pipeline as claimed in claim 1, it is characterised in that：
S1：By the sepiolite of the diatomite of 100 mesh and 100 mesh using mass ratio as diatomite：The mixing of the ratio of sepiolite=1, wherein
Diatomite 1000g, sepiolite 1000g, 180 DEG C of oven-bakeds are inserted 24 hours by mixture, and furnace cooling obtains A2 material；
S2：By urea 300g, oxalic acid 35g, stirring and dissolving, will be molten into 500ml isopropanols and 500ml absolute ethyl alcohols at 42 DEG C
Solution after solution is slowly added dropwise in A2 material, and ageing is standby, obtains B2 material；
S3：300gB material are taken to be scattered in absolute ethyl alcohol with acetonitrile volume ratio in 3 mixed solution 100ml, scattered 40min is being stirred
The ammoniacal liquor that 60ml mass fractions are 27% is added under the conditions of mixing, C2 material are obtained；
S4：Take 220ml tetra-n-butyl titanates and 200ml absolute ethyl alcohols to mix, 20g triethanolamines are dissolved in the positive fourth of above-mentioned metatitanic acid four
In the mixed liquor of ester and absolute ethyl alcohol, stirring 20min to solution is clarified, and mixed liquor is added drop-wise to C2 material dropwise under agitation
In, continue to stir 2h, obtain D2 material；
S5：The pale precipitation in D2 material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation drying is ground
Be placed in after mill in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to room after 24 hours
Temperature, obtains batch mixing E2, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B 2 and batch mixing E2 are placed in batch mixer, with the aqueous solution of the citric acids of 100ml 5% at 100 DEG C
Sealed after middle stirring, air cooling, obtain final products F2.
6. the preparation method of smart lock water loss circulation material in a kind of pipeline as claimed in claim 1, it is characterised in that：
S1：By the sepiolite of the diatomite of 100 mesh and 100 mesh using mass ratio as diatomite：The mixing of the ratio of sepiolite=2, wherein
Diatomite 2000g, sepiolite 1000g, 180 DEG C of oven-bakeds are inserted 24 hours by mixture, and furnace cooling obtains A3 material；
S2：By urea 300g, oxalic acid 35g, stirring and dissolving, will be molten into 500ml isopropanols and 500ml absolute ethyl alcohols at 42 DEG C
Solution after solution is slowly added dropwise in A3 material, and ageing is standby, obtains B3 material；
S3：300gB material are taken to be scattered in absolute ethyl alcohol with acetonitrile volume ratio in 3 mixed solution 100ml, scattered 40min is being stirred
The ammoniacal liquor that 60ml mass fractions are 27% is added under the conditions of mixing, C3 material are obtained；
S4：Take 220ml tetra-n-butyl titanates and 200ml absolute ethyl alcohols to mix, 20g triethanolamines are dissolved in the positive fourth of above-mentioned metatitanic acid four
In the mixed liquor of ester and absolute ethyl alcohol, stirring 20min to solution is clarified, and mixed liquor is added drop-wise to C3 material dropwise under agitation
In, continue to stir 2h, obtain D3 material；
S5：The pale precipitation in D3 material is taken out, is separated, precipitation is then washed with absolute ethyl alcohol 4 times, precipitation drying is ground
Be placed in after mill in Muffle furnace 400 DEG C of roastings remove impurity it is follow-up it is continuous be warming up to needed at temperature insulation be air-cooled to room after 24 hours
Temperature, obtains batch mixing E3, specifically, and separation method is centrifuges, and seperator rotating speed is not less than 1000r/min；
S6：Remaining mixed material B 3 and batch mixing E3 are placed in batch mixer, with the aqueous solution of the citric acids of 100ml 5% at 100 DEG C
Sealed after middle stirring, air cooling, obtain final products F3.
7. the application method of smart lock water loss circulation material in a kind of pipeline, it is characterised in that：Smart lock water blocking in described pipeline
The specific quality of the selected this product of water quality need to be held according to liquid pipe by leaking material F, be blended into after then being diluted with more than 80 DEG C pure water
Pipeline.
8. the application method of smart lock water loss circulation material in a kind of pipeline as claimed in claim 7, the pipeline holds water quality
It is (500 with smart lock water loss circulation material F mass ratioes in the pipeline:3)-(10000:3), smart lock water blocking leaks in the pipeline
The mass ratio of material F and 80 DEG C of pure water is 1:2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710428815.3A CN107142082B (en) | 2017-06-08 | 2017-06-08 | Smart lock water blocking leakage material fabrication process and its application method in a kind of pipeline |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710428815.3A CN107142082B (en) | 2017-06-08 | 2017-06-08 | Smart lock water blocking leakage material fabrication process and its application method in a kind of pipeline |
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| CN107142082B CN107142082B (en) | 2019-01-22 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1103100A (en) * | 1993-11-24 | 1995-05-31 | 彭吕元 | Sepiolite heat insulating, water-proof stop leakage paste and use |
| CN103174428A (en) * | 2013-03-15 | 2013-06-26 | 金川集团股份有限公司 | Method of implementing grouting and water plugging of shaft through chemical grout |
| CN104893639A (en) * | 2015-06-09 | 2015-09-09 | 青岛科技大学 | Pipeline emergency plugging agent |
-
2017
- 2017-06-08 CN CN201710428815.3A patent/CN107142082B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1103100A (en) * | 1993-11-24 | 1995-05-31 | 彭吕元 | Sepiolite heat insulating, water-proof stop leakage paste and use |
| CN103174428A (en) * | 2013-03-15 | 2013-06-26 | 金川集团股份有限公司 | Method of implementing grouting and water plugging of shaft through chemical grout |
| CN104893639A (en) * | 2015-06-09 | 2015-09-09 | 青岛科技大学 | Pipeline emergency plugging agent |
Non-Patent Citations (1)
| Title |
|---|
| 张超，等: "石油工程纤维承压堵漏技术在塔里木碳酸盐岩地层的研究与应用", 《石化技术》 * |
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|---|---|
| CN107142082B (en) | 2019-01-22 |
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