CN107141669A - Have rosewater artificial flowers and preparation method thereof - Google Patents

Have rosewater artificial flowers and preparation method thereof Download PDF

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Publication number
CN107141669A
CN107141669A CN201710530122.5A CN201710530122A CN107141669A CN 107141669 A CN107141669 A CN 107141669A CN 201710530122 A CN201710530122 A CN 201710530122A CN 107141669 A CN107141669 A CN 107141669A
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CN
China
Prior art keywords
parts
artificial flowers
rosewater
preparation
electrolytic cell
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710530122.5A
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Chinese (zh)
Inventor
张伟
程玉柱
张海民
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jieshou City Flower Co Ltd Seagate Simulation
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Jieshou City Flower Co Ltd Seagate Simulation
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Application filed by Jieshou City Flower Co Ltd Seagate Simulation filed Critical Jieshou City Flower Co Ltd Seagate Simulation
Priority to CN201710530122.5A priority Critical patent/CN107141669A/en
Publication of CN107141669A publication Critical patent/CN107141669A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L27/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
    • C08L27/02Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L27/12Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C08L27/18Homopolymers or copolymers or tetrafluoroethene
    • AHUMAN NECESSITIES
    • A41WEARING APPAREL
    • A41GARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
    • A41G1/00Artificial flowers, fruit, leaves, or trees; Garlands
    • A41G1/001Artificial flowers, fruit, leaves, or trees; Garlands characterised by their special functions
    • A41G1/006Diffusing perfume or the like
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24Acids; Salts thereof
    • C08K3/26Carbonates; Bicarbonates
    • C08K2003/262Alkali metal carbonates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/30Sulfur-, selenium- or tellurium-containing compounds
    • C08K2003/3045Sulfates
    • C08K2003/3072Iron sulfates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Rosewater artificial flowers of one kind tool and preparation method thereof, the artificial flowers are made up of the raw material proportioning of following parts by weight:45 55 parts of polytetrafluoroethylene (PTFE), 8 10 parts of polyethylene, 0.2 0.4 parts of sulfuric acid iron powder, 1.5 2.5 parts of powdered sodium carbonate, 35 parts of Flos Rosae Rugosas pollen, 0.5 1.0 parts of sodium chloride, 1.4 2.0 parts of wood rosin, 2 2.5 parts of Starex, 0.8 1.5 parts of silica flour, 0.5 1.2 parts of porcelain powder, red female 5 10 parts, 0.6 1.4 parts of talcum powder.Artificial flowers that the present invention is provided and preparation method thereof, profile, color not only with common artificial flowers, while the fragrance that true rose has can be given out, fragrance spread and overflow, closer to true flowers.

Description

Have rosewater artificial flowers and preparation method thereof
Technical field
The present invention relates to artificial flowers technical field, and in particular to the rosewater artificial flowers of one kind tool and its preparation side Method.
Background technology
Artificial flowers, also known as artificial flower, silk flower, silk flower, artificial flowers can not only keep floridity for a long time, more can be according to season and need Ask and follow one's bent:Spring is very much in the air is arranged by you, and summer is refrigerant to write with facility, and autumn can be harvested with a piece of golden yellow represent, winter energy With meeting the eye on every side red as fire send come warm;It can be loved at any time with rose expression, tree peony transmission blessing can be plucked everywhere.Outward appearance remarkably true to life, Moulding in different poses and with different expressions, longer viewing period and more rich moulding gimmick are all the strong reasons that artificial flowers are liked in people's inner feelings. China, artificial flowers have become a kind of articles for use often, no matter open for business celebration, wedding celebration wedding feast, or office space, house ring Border, the figure for having artificial flowers, it was reported that the sales volume of artificial flowers is all increased with 40% speed every year.Abroad, particularly Europe Beautiful, Southeast Asia developed country, increasing people likes hand work, and artificial flowers are low, normally opened with its good and cheap, cost of upkeep Unbeaten particular advantages are more favored.
Existing artificial flowers are main to simulate true flowers in terms of profile and color two, reaches the effect mixed the spurious with the genuine, still The due fragrance of true flowers institute can not be given out, typically passes through the perfumes on artificial flowers surface.
The content of the invention
The present invention is to solve the above problems, provide a kind of rosewater artificial flowers of tool and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme:
The rosewater artificial flowers of one kind tool, the artificial flowers are made up of the raw material proportioning of following parts by weight:
45-55 parts of polytetrafluoroethylene (PTFE), 8-10 parts of polyethylene, 0.2-0.4 parts of sulfuric acid iron powder, powdered sodium carbonate 1.5-2.5 Part, 3-5 parts of Flos Rosae Rugosas pollen, 0.5-1.0 parts of sodium chloride, 1.4-2.0 parts of wood rosin, 2-2.5 parts of Starex, silica flour 0.8- 1.5 parts, 0.5-1.2 parts of porcelain powder, red 5-10 parts of mother, 0.6-1.4 parts of talcum powder.
It is preferred that, the artificial flowers are made up of the raw material proportioning of following parts by weight:
50 parts of polytetrafluoroethylene (PTFE), 9 parts of polyethylene, 2.5 parts of sulfuric acid iron powder, 2 parts of powdered sodium carbonate, 4 parts of Flos Rosae Rugosas pollen, chlorine Change 0.8 part of sodium, 1.7 parts of wood rosin, 2.3 parts of Starex, 1.1 parts of silica flour, 0.8 part of porcelain powder is red female 8 parts, talcum powder 1.0 Part.
The polytetrafluoroethylene (PTFE), polyethylene, red female granularity are 0.1-0.3mm.
It is preferred that, the polytetrafluoroethylene (PTFE), polyethylene, red female granularity are 0.2mm.
A kind of preparation method for having rosewater artificial flowers, comprises the following steps:
(1) each raw material is weighed by weight, and raw material is poured into electrolytic cell and stirred;
(2) by electrolytic cell airtight heating to boiling;
(3) electrolytic cell is electrolysed with power on;
(4) granular material in electrolytic cell is picked up, obtains compound;
(5) compound is melted in closed smelting furnace, melts postforming;
(6) it is cooled to 50-60 DEG C after to be formed and is put into former electrolytic cell and is cleaned.
In the step (1) 5~10Kg of raw material is added in electrolytic cell in every 100L water.
Ebuillition of heated keeps 20~30min in the step (2).
Supply voltage is risen to 4KV from 1KV in 20min in the step (3), current synchronization rises to 5A from 2A, terminate Deenergization, switching electric current flow direction, make supply voltage rise to 4KV from 1KV, current synchronization rises to from 2A in 20min again afterwards 5A, repeats switching electric current and flows to 2~3 times.
Temperature is 180~220 DEG C when being melted in the step (5).
Beneficial effects of the present invention are:Under high temperature, addition wood rosin, oil slick pine in polytetrafluoroethylene (PTFE), polyethylene, red mother Fragrant component, Flos Rosae Rugosas pollen fragrance is fully drawn in electrolytic cell and is formed in polytetrafluoroethylene (PTFE), polyethylene, red female particle surface Thin film, is infiltrated into inside artificial flowers during fusing, and addition sulfuric acid iron powder, powdered sodium carbonate can be in polytetrafluoroethylene (PTFE), poly- second Artificial flowers when alkene melts in shaping are internally formed tiny space, beneficial to the outside loss of Flos Rosae Rugosas pollen fragrance, while ferric sulfate Raw material can be electrolysed, in electrolytic process by powder, powdered sodium carbonate, sodium chloride in electrolytic cell as electrolyte in electrolytic cell Ion drives the movement of pollen molecular orientation, is contacted with polytetrafluoroethylene (PTFE), polyethylene particle surface and pollen molecule is attached to table Face, improves finally shaped emulation flowery odour, is found through experiments that, last obtained emulation flowery odour and the electric current being passed through, Voltage is directly proportional, and the preparation method provided is again placed in cleaning in electrolytic cell in last cooling, using waste heat to electrolysis Pollen molecule formation second adsorption in pond, the artificial flowers that the present invention is provided and preparation method thereof, not only with common artificial flowers Profile, color, while the fragrance that true rose has can be given out, fragrance spread and overflow, closer to true flowers.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below Embodiment is closed, the present invention is expanded on further.
Embodiment 1
The rosewater artificial flowers of one kind tool, the artificial flowers are made up of the raw material proportioning of following parts by weight:
45 parts of polytetrafluoroethylene (PTFE), 8 parts of polyethylene, 0.2 part of sulfuric acid iron powder, 1.5 parts of powdered sodium carbonate, 3 parts of Flos Rosae Rugosas pollen, 0.5 part of sodium chloride, 1.4 parts of wood rosin, 2 parts of Starex, 0.8 part of silica flour, 0.5 part of porcelain powder is red female 5 parts, talcum powder 0.6 Part.
The polytetrafluoroethylene (PTFE), polyethylene, red female granularity are 0.1-0.3mm.
A kind of preparation method for having rosewater artificial flowers, comprises the following steps:
(1) each raw material is weighed by weight, raw material is poured into electrolytic cell and stirred, and raw material is added in every 100L water 5~10Kg;
(2) 20~30min is kept to be fumigated to seething with excitement electrolytic cell airtight heating;
(3) electrolytic cell is electrolysed with power on, supply voltage is risen to 4KV from 1KV in 20min during electrolysis, Current synchronization rises to 5A from 2A, terminates rear deenergization, and switching electric current flow direction makes supply voltage from 1KV liters in 20min again To 4KV, current synchronization rises to 5A from 2A, repeats switching electric current and flows to 2~3 times;
(4) granular material in electrolytic cell is picked up, obtains compound;
(5) compound is melted in closed smelting furnace, it is 180~220 DEG C that temperature is controlled during fusing, melts postforming;
(6) it is cooled to 50-60 DEG C after to be formed and is put into former electrolytic cell and is cleaned.
Embodiment 2
The rosewater artificial flowers of one kind tool, the artificial flowers are made up of the raw material proportioning of following parts by weight:
50 parts of polytetrafluoroethylene (PTFE), 9 parts of polyethylene, 2.5 parts of sulfuric acid iron powder, 2 parts of powdered sodium carbonate, 4 parts of Flos Rosae Rugosas pollen, chlorine Change 0.8 part of sodium, 1.7 parts of wood rosin, 2.3 parts of Starex, 1.1 parts of silica flour, 0.8 part of porcelain powder is red female 8 parts, talcum powder 1.0 Part.
The polytetrafluoroethylene (PTFE), polyethylene, red female granularity are 0.1-0.3mm.
A kind of preparation method for having rosewater artificial flowers, comprises the following steps:
(1) each raw material is weighed by weight, raw material is poured into electrolytic cell and stirred, and raw material is added in every 100L water 5~10Kg;
(2) 20~30min is kept to be fumigated to seething with excitement electrolytic cell airtight heating;
(3) electrolytic cell is electrolysed with power on, supply voltage is risen to 4KV from 1KV in 20min during electrolysis, Current synchronization rises to 5A from 2A, terminates rear deenergization, and switching electric current flow direction makes supply voltage from 1KV liters in 20min again To 4KV, current synchronization rises to 5A from 2A, repeats switching electric current and flows to 2~3 times;
(4) granular material in electrolytic cell is picked up, obtains compound;
(5) compound is melted in closed smelting furnace, it is 180~220 DEG C that temperature is controlled during fusing, melts postforming;
(6) it is cooled to 50-60 DEG C after to be formed and is put into former electrolytic cell and is cleaned.
Embodiment 3
The rosewater artificial flowers of one kind tool, the artificial flowers are made up of the raw material proportioning of following parts by weight:
55 parts of polytetrafluoroethylene (PTFE), 10 parts of polyethylene, 0.4 part of sulfuric acid iron powder, 2.5 parts of powdered sodium carbonate, Flos Rosae Rugosas pollen 5 Part, 1.0 parts of sodium chloride, 2.0 parts of wood rosin, 2.5 parts of Starex, 1.5 parts of silica flour, 1.2 parts of porcelain powder is red female 10 parts, sliding 1.4 parts of stone flour.
The polytetrafluoroethylene (PTFE), polyethylene, red female granularity are 0.1-0.3mm.
A kind of preparation method for having rosewater artificial flowers, comprises the following steps:
(1) each raw material is weighed by weight, raw material is poured into electrolytic cell and stirred, and raw material is added in every 100L water 5~10Kg;
(2) 20~30min is kept to be fumigated to seething with excitement electrolytic cell airtight heating;
(3) electrolytic cell is electrolysed with power on, supply voltage is risen to 4KV from 1KV in 20min during electrolysis, Current synchronization rises to 5A from 2A, terminates rear deenergization, and switching electric current flow direction makes supply voltage from 1KV liters in 20min again To 4KV, current synchronization rises to 5A from 2A, repeats switching electric current and flows to 2~3 times;
(4) granular material in electrolytic cell is picked up, obtains compound;
(5) compound is melted in closed smelting furnace, it is 180~220 DEG C that temperature is controlled during fusing, melts postforming;
(6) it is cooled to 50-60 DEG C after to be formed and is put into former electrolytic cell and is cleaned.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and that described in above-described embodiment and specification is only the present invention Preference, be not intended to limit the present invention, without departing from the spirit and scope of the present invention, the present invention also have it is various Changes and improvements, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by institute Attached claims and its equivalent thereof.

Claims (10)

1. the rosewater artificial flowers of one kind tool, it is characterised in that the artificial flowers by following parts by weight raw material proportioning system Into:
45-55 parts of polytetrafluoroethylene (PTFE), 8-10 parts of polyethylene, 0.2-0.4 parts of sulfuric acid iron powder, 1.5-2.5 parts of powdered sodium carbonate, rose Rare pollen 3-5 parts, 0.5-1.0 parts of sodium chloride, 1.4-2.0 parts of wood rosin, 2-2.5 parts of Starex, 0.8-1.5 parts of silica flour, 0.5-1.2 parts of porcelain powder, red 5-10 parts of mother, 0.6-1.4 parts of talcum powder.
2. a kind of rosewater artificial flowers of tool as claimed in claim 1, it is characterised in that the artificial flowers are by following heavy The raw material proportioning of amount part is made:
50 parts of polytetrafluoroethylene (PTFE), 9 parts of polyethylene, 2.5 parts of sulfuric acid iron powder, 2 parts of powdered sodium carbonate, 4 parts of Flos Rosae Rugosas pollen, sodium chloride 0.8 part, 1.7 parts of wood rosin, 2.3 parts of Starex, 1.1 parts of silica flour, 0.8 part of porcelain powder is red female 8 parts, 1.0 parts of talcum powder.
3. the rosewater artificial flowers of tool as claimed in claim 1 a kind of, it is characterised in that the polytetrafluoroethylene (PTFE), poly- Ethene, red female granularity are 0.1-0.3mm.
4. the rosewater artificial flowers of tool as claimed in claim 1 a kind of, it is characterised in that the polytetrafluoroethylene (PTFE), poly- Ethene, red female granularity are 0.2mm.
5. a kind of preparation method for having rosewater artificial flowers, it is characterised in that comprise the following steps:
(1) each raw material is weighed by weight, and raw material is poured into electrolytic cell and stirred;
(2) by electrolytic cell airtight heating to boiling;
(3) electrolytic cell is electrolysed with power on;
(4) granular material in electrolytic cell is picked up, obtains compound;
(5) compound is melted in closed smelting furnace, melts postforming;
(6) it is cooled to 50-60 DEG C after to be formed and is put into former electrolytic cell and is cleaned.
6. a kind of preparation method for having rosewater artificial flowers as claimed in claim 5, it is characterised in that the step (1) 5~10Kg of raw material is added in every 100L water in electrolytic cell.
7. a kind of preparation method for having rosewater artificial flowers as claimed in claim 5, it is characterised in that the step (2) ebuillition of heated keeps 20~30min in.
8. a kind of preparation method for having rosewater artificial flowers as claimed in claim 5, it is characterised in that the step (3) supply voltage is risen to 4KV from 1KV in 20min in, current synchronization rises to 5A from 2A, terminate rear deenergization, switching electricity Stream flow direction, makes supply voltage rise to 4KV from 1KV, current synchronization rises to 5A from 2A in 20min again.
9. a kind of preparation method for having rosewater artificial flowers as claimed in claim 8, it is characterised in that repeat to switch Current direction 2~3 times.
10. a kind of preparation method for having rosewater artificial flowers as claimed in claim 5, it is characterised in that the step Temperature is 180~220 DEG C when being melted suddenly in (5).
CN201710530122.5A 2017-07-03 2017-07-03 Have rosewater artificial flowers and preparation method thereof Pending CN107141669A (en)

Priority Applications (1)

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CN201710530122.5A CN107141669A (en) 2017-07-03 2017-07-03 Have rosewater artificial flowers and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201710530122.5A CN107141669A (en) 2017-07-03 2017-07-03 Have rosewater artificial flowers and preparation method thereof

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CN107141669A true CN107141669A (en) 2017-09-08

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107446325A (en) * 2017-09-20 2017-12-08 界首市希捷仿真花卉有限公司 A kind of artificial flowers modified plastics
KR20220107548A (en) * 2021-01-25 2022-08-02 조정환 Method of preparing artificial flower having excellent durability using double creped paper

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105295110A (en) * 2015-11-04 2016-02-03 南京邮电大学 Anti-bacterial artificial flower and preparation method thereof
CN106398269A (en) * 2016-08-31 2017-02-15 宁小孟 Flower and plant fine hair-like plastic

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105295110A (en) * 2015-11-04 2016-02-03 南京邮电大学 Anti-bacterial artificial flower and preparation method thereof
CN106398269A (en) * 2016-08-31 2017-02-15 宁小孟 Flower and plant fine hair-like plastic

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王莲英 等: "《中国牡丹品种图志(续志)》", 30 June 2015, 中国林业出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107446325A (en) * 2017-09-20 2017-12-08 界首市希捷仿真花卉有限公司 A kind of artificial flowers modified plastics
KR20220107548A (en) * 2021-01-25 2022-08-02 조정환 Method of preparing artificial flower having excellent durability using double creped paper
KR102430641B1 (en) 2021-01-25 2022-08-16 조정환 Method of preparing artificial flower having excellent durability using double creped paper

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Application publication date: 20170908