CN107132093A - Suitable for small size rod, the fixture of line sample metallographic sample preparation and its application method - Google Patents

Suitable for small size rod, the fixture of line sample metallographic sample preparation and its application method Download PDF

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Publication number
CN107132093A
CN107132093A CN201710343932.XA CN201710343932A CN107132093A CN 107132093 A CN107132093 A CN 107132093A CN 201710343932 A CN201710343932 A CN 201710343932A CN 107132093 A CN107132093 A CN 107132093A
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CN
China
Prior art keywords
dovetail groove
block
fixture
fixture block
sample
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710343932.XA
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Chinese (zh)
Inventor
邓丽萍
刘志锋
庄二鹏
卓掌筑
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Fuzhou University
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Fuzhou University
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Publication date
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Priority to CN201710343932.XA priority Critical patent/CN107132093A/en
Publication of CN107132093A publication Critical patent/CN107132093A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/286Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/32Polishing; Etching
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/286Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
    • G01N2001/2866Grinding or homogeneising

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

It is applied to small size rod the present invention relates to one kind, the fixture and its application method of line sample metallographic sample preparation, including first, second fixture block and it is respectively provided at first, first on second fixture block, second dovetail groove, described first, second dovetail groove is oppositely arranged, first fixture block is L-shaped block, dovetail groove is provided with the inner side in L-shaped block vertical edge portion, the dovetail groove is provided with the upside of L-shaped block cross edge, second fixture block is rectangular block, in rectangular block while provided with the dovetail coordinated with dovetail groove, the lower surface of the rectangular block is provided with the dovetail groove, the L-shaped block cross edge and the corresponding position of rectangular block are provided with perforation, fastening bolt is equipped with perforation.The present invention has advantages below:1. it is applied to the preparation of the small size line sample of different line footpaths;2. two fixture blocks of fixture are coordinated by dovetail groove ensures parallel to each other, uniform force, and then ensures that sample surfaces are smooth during grind away, improve sample preparation level.

Description

Suitable for small size rod, the fixture of line sample metallographic sample preparation and its application method
Technical field:
The present invention relates to suitable for small size rod, the fixture of line sample metallographic sample preparation and its application method.
Background technology:
Metal lographic examination is a kind of experimental method of common observation metal material microscopic structure, research of its result to metal material It is particularly significant, and the preparation quality of sample is to determine Success in Experiment whether key factor, therefore the preparation of sample must be added To pay attention to;Sample clamping shakiness, flour milling out-of-flatness often occur for some small samples, during sample preparation, causes sample system The second-rate situation of sample, it is necessary to using inlaying or gluing, then ground, polished again;Examination is prepared using inlaying Sample, process is relatively complicated, and the consuming time is long, and current existing sample preparation auxiliary fixture structure is complex, and handling sample is time-consuming, system Sample effect is not good;It is gluing, be related to the use of the chemical reagent such as acetone, and these chemical reagent to the health of operator extremely not Profit.Therefore, a kind of fixture for the small sample sample preparation for facilitating different line footpaths is designed, and harmful chemical agents can be avoided It is very necessary using just seeming.
The content of the invention:
It is applied to small size rod, the fixture of line sample metallographic sample preparation and its user it is an object of the invention to provide a kind of Method, this is simple, reasonable in design suitable for the clamp structure of small size rod, line sample metallographic sample preparation, is conducive to facilitating sample preparation.
The present invention is applied to small size rod, the fixture of line sample metallographic sample preparation, it is characterised in that:Including first, second Fixture block and first, second dovetail groove being respectively provided on first, second fixture block, first, second dovetail groove are oppositely arranged, institute The first fixture block is stated for L-shaped block, dovetail groove is provided with the inner side in L-shaped block vertical edge portion, the ladder is provided with the upside of L-shaped block cross edge Shape groove, second fixture block is rectangular block, in rectangular block while provided with the dovetail coordinated with dovetail groove, the following table of the rectangular block Face is provided with the dovetail groove, and the L-shaped block cross edge and the corresponding position of rectangular block are equipped with tight provided with perforation in perforation Fixing bolt.
Further, dovetail groove is symmetrical with provided with two groups of perforation and fastening bolt on above-mentioned L-shaped block cross edge and rectangular block.
Further, above-mentioned first, second fixture block is made up of aluminium.
Further, above-mentioned dovetail groove does not penetrate the first fixture block and the second fixture block.
Further, the bottom land of above-mentioned dovetail groove can pad and set cushion block.
The present invention is applied to small size rod, the application method of line sample metallographic sample preparation fixture, it is characterised in that:It is described suitable Fixture for small size rod, line sample metallographic sample preparation includes first, second fixture block and is respectively provided at first, second fixture block First, second dovetail groove, first, second dovetail groove is oppositely arranged, and first fixture block is L-shaped block, in L-shaped block vertical edge The inner side in portion is provided with dovetail groove, and the dovetail groove is provided with the upside of L-shaped block cross edge, and second fixture block is rectangular block, Rectangular block is while provided with the dovetail coordinated with dovetail groove, the lower surface of the rectangular block is provided with the dovetail groove, and the L-shaped block is horizontal Edge and the corresponding position of rectangular block are equipped with fastening bolt provided with perforation in perforation;In use, the second fixture block is placed To the cross edge upper surface of the first fixture block, and make the dovetail groove on the second fixture block relative with the dovetail groove in the first fixture block cross edge Set, by the first fixture block cross edge and the second fixture block on bolt lock, keep the first fixture block cross edge and the second fixture block still can be relative Motion, is put into small size line sample, and allow small size line sample to be exposed at outside dovetail groove one section, locking screw in dovetail groove Bolt, makes the dovetail groove of the first fixture block cross edge and the second fixture block clamp small size line sample;During sample preparation, Handheld clamp will be revealed One section of small size line sample is polished on sand paper outside dovetail groove;When having ground a sand paper, when changing a more fine sandpaper, Mould 90-degree angle is rotated, makes new, old polishing scratch vertical, to eliminate old polishing scratch;Due to the design of dovetail groove, A first, can be made Two fixture blocks and sample polishing plane are parallel to each other all the time, so as to ensure that sample flour milling is smooth;When sample in cross section flour milling is polished to Can stop grinding in same level with first, second fixture block bottom surface, then in addition enter metallographic prepare polishing, corrosion Down-stream.
The present invention has advantages below:1. it is applied to the preparation of the small size line sample of different line footpaths;2. the two of fixture Fixture block is coordinated by dovetail groove ensures parallel to each other, uniform force, and then ensures that sample surfaces are smooth during grind away, prepare sample Level is improved;3. clamp structure is simple, easy to process, simple to operate and can repeatedly use.
Brief description of the drawings:
Fig. 1 is the D structure schematic diagram of the first fixture block;
Fig. 2 is the D structure schematic diagram of the second fixture block;
Fig. 3 is the first fixture block, the D structure schematic diagram of the second fixture block assembled state;
Fig. 4 is the D structure schematic diagram at Fig. 3 another visual angle.
Embodiment:
The present invention will be further described in detail with reference to the accompanying drawings and detailed description.
The present invention includes the first fixture block 1, the and of the second fixture block 2 suitable for the fixture of small size rod, line sample metallographic sample preparation The first dovetail groove 3, the second dovetail groove 4 on first, second fixture block are respectively provided at, first, second dovetail groove is oppositely arranged, First fixture block 1 is L-shaped block, dovetail groove 5 is provided with the inner side in L-shaped block vertical edge portion 101, in the upside of L-shaped block cross edge 102 Provided with first dovetail groove 3, second fixture block 2 is rectangular block, in rectangular block while provided with the dovetail coordinated with dovetail groove 6, the lower surface of the rectangular block is provided with second dovetail groove 4, the L-shaped block cross edge 102 and the corresponding position of rectangular block Provided with perforation 7, fastening bolt 8 is equipped with perforation 7.
Further, in order to which stable connection is reliable, it is symmetrical with dovetail groove in above-mentioned L-shaped block cross edge 102 and rectangular block and sets There are two groups of perforation 7 and fastening bolt 8.
Further, in order to light, above-mentioned first, second fixture block is made up of aluminium.
Further, in order to easy to use, above-mentioned dovetail groove does not penetrate the first fixture block and the second fixture block.
Further, in order to adapt to different height of specimen, the bottom land of above-mentioned dovetail groove, which can be padded, sets cushion block.
The present invention is applied to small size rod, the application method of line sample metallographic sample preparation fixture, described to be applied to small size Rod, the fixture of line sample metallographic sample preparation include first, second fixture block and be respectively provided on first, second fixture block first, the Two dovetail grooves, first, second dovetail groove is oppositely arranged, and first fixture block is L-shaped block, the inner side in L-shaped block vertical edge portion Provided with dovetail groove, the dovetail groove is provided with the upside of L-shaped block cross edge, second fixture block is rectangular block, in rectangular block one Side is provided with the dovetail coordinated with dovetail groove, and the lower surface of the rectangular block is provided with the dovetail groove, the L-shaped block cross edge and square The corresponding position of shape block is equipped with fastening bolt provided with perforation in perforation;In use, the second fixture block is placed into the first folder The cross edge upper surface of block, and the dovetail groove on the second fixture block is oppositely arranged with the dovetail groove in the first fixture block cross edge, will First fixture block cross edge and the second fixture block on bolt lock, keep the first fixture block cross edge and the second fixture block still to can be movable relatively, It is put into small size line sample A in dovetail groove, and it is outer one section to allow small size line sample to be exposed at dovetail groove, clamping screw, makes the The dovetail groove of one fixture block cross edge and the second fixture block clamps small size line sample;During sample preparation, Handheld clamp will be exposed at dovetail groove Outer one section of small size line sample is polished on sand paper;When having ground a sand paper, when changing a more fine sandpaper, mould is rotated Have 90 ° of angles, make new, old polishing scratch vertical, to eliminate old polishing scratch;Due to the design of dovetail groove, can make the fixture blocks of A first, second and Sample polishing plane is parallel to each other all the time, so as to ensure that sample flour milling is smooth;Be polished to first when sample in cross section flour milling, the Two fixture block bottom surfaces can stop grinding in same level, and polishing, the down-stream of corrosion prepared by metallographic are then entered in addition.
The present invention has advantages below:1. it is applied to the preparation of the small size line sample of different line footpaths;2. the two of fixture Fixture block is coordinated by dovetail groove ensures parallel to each other, uniform force, and then ensures that sample surfaces are smooth during grind away, prepare sample Level is improved;3. clamp structure is simple, easy to process, simple to operate and can repeatedly use.
First, second fixture block upper surface 9, lower surface 10 are all burnishing surfaces, so common metallographic microscope is either used, Or inverted metallurgic microscope is observed, can conveniently it carry out;Furthermore it is also possible to easily prepare electron microscopic sample and carry out Relevant characterization is tested, it is to avoid hand-held difficulty, flour milling out-of-flatness, the problems such as be difficult to focusing.
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with Modification, should all belong to the covering scope of the present invention.

Claims (6)

1. a kind of be applied to small size rod, the fixture of line sample metallographic sample preparation, it is characterised in that:Including first, second fixture block With first, second dovetail groove being respectively provided on first, second fixture block, first, second dovetail groove is oppositely arranged, and described One fixture block is L-shaped block, dovetail groove is provided with the inner side in L-shaped block vertical edge portion, in the upside of L-shaped block cross edge provided with described trapezoidal Groove, second fixture block is rectangular block, in rectangular block while provided with the dovetail coordinated with dovetail groove, the lower surface of the rectangular block Provided with the dovetail groove, the L-shaped block cross edge and the corresponding position of rectangular block are equipped with fastening provided with perforation in perforation Bolt.
2. according to claim 1 be applied to small size rod, the fixture of line sample metallographic sample preparation, it is characterised in that:Institute State and dovetail groove is symmetrical with L-shaped block cross edge and rectangular block provided with two groups of perforation and fastening bolt.
3. according to claim 1 be applied to small size rod, the fixture of line sample metallographic sample preparation, it is characterised in that:Institute First, second fixture block is stated to be made up of aluminium.
4. according to claim 1 be applied to small size rod, the fixture of line sample metallographic sample preparation, it is characterised in that:Institute State dovetail groove and do not penetrate the first fixture block and the second fixture block.
5. according to claim 1 be applied to small size rod, the fixture of line sample metallographic sample preparation, it is characterised in that:Institute State the bottom land of dovetail groove and can pad and set cushion block.
6. a kind of be applied to small size rod, the application method of line sample metallographic sample preparation fixture, it is characterised in that:It is described to be applied to Small size rod, the fixture of line sample metallographic sample preparation include first, second fixture block and be respectively provided on first, second fixture block the First, the second dovetail groove, first, second dovetail groove is oppositely arranged, and first fixture block is L-shaped block, in L-shaped block vertical edge portion Inner side is provided with dovetail groove, the dovetail groove is provided with the upside of L-shaped block cross edge, second fixture block is rectangular block, in rectangle Block is while provided with the dovetail coordinated with dovetail groove, the lower surface of the rectangular block is provided with the dovetail groove, the L-shaped block cross edge With the corresponding position of rectangular block provided with perforation, fastening bolt is equipped with perforation;In use, the second fixture block is placed into The cross edge upper surface of one fixture block, and make the dovetail groove on the second fixture block is relative with the dovetail groove in the first fixture block cross edge to set Put, by the first fixture block cross edge and the second fixture block on bolt lock, keep the first fixture block cross edge and the second fixture block still can relative fortune It is dynamic, it is put into small size line sample in dovetail groove, and it is outer one section to allow small size line sample to be exposed at dovetail groove, clamping screw, The dovetail groove of the first fixture block cross edge and the second fixture block is set to clamp small size line sample;During sample preparation, Handheld clamp will be exposed at ladder The outer one section small size line sample of shape groove is polished on sand paper;When having ground a sand paper, when changing a more fine sandpaper, to turn 90 ° of angles of moving mold, make new, old polishing scratch vertical, to eliminate old polishing scratch;It due to the design of dovetail groove, can press from both sides A first, second Block and sample polishing plane are parallel to each other all the time, so as to ensure that sample flour milling is smooth;When sample in cross section flour milling is polished to and the First, the second fixture block bottom surface can stop grinding in same level, then in addition enter metallographic prepare polishing, corrosion it is follow-up Program.
CN201710343932.XA 2017-05-16 2017-05-16 Suitable for small size rod, the fixture of line sample metallographic sample preparation and its application method Pending CN107132093A (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109283027A (en) * 2018-11-05 2019-01-29 长沙岱勒新材料科技股份有限公司 Diamond wire metallographic specimen producing device and method
CN110411855A (en) * 2019-08-06 2019-11-05 无锡锡洲电磁线有限公司 Pole bend test device
CN110579384A (en) * 2019-08-28 2019-12-17 长江存储科技有限责任公司 Sample clamp

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Publication number Priority date Publication date Assignee Title
CN2156044Y (en) * 1992-08-06 1994-02-16 李涛 multifunctional square
CN202479960U (en) * 2011-12-20 2012-10-10 中国直升机设计研究所 Clamp for grinding lamellar metallographic specimen
JP2013200232A (en) * 2012-03-26 2013-10-03 Toppan Printing Co Ltd Observation sample preparation tool
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CN105699159A (en) * 2016-04-22 2016-06-22 大唐东北电力试验研究所有限公司 Metallographic specimen clamping device
CN205520941U (en) * 2016-04-26 2016-08-31 四川建筑职业技术学院 Metallographic specimen grinds anchor clamps
CN205786026U (en) * 2016-06-24 2016-12-07 福州大学 A kind of auxiliary clamp being applicable to small size wire rod and thin plate sample metallographic sample preparation
CN206862735U (en) * 2017-05-16 2018-01-09 福州大学 Suitable for rod, the fixture of wire rod metallographic specimen

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2156044Y (en) * 1992-08-06 1994-02-16 李涛 multifunctional square
CN202479960U (en) * 2011-12-20 2012-10-10 中国直升机设计研究所 Clamp for grinding lamellar metallographic specimen
JP2013200232A (en) * 2012-03-26 2013-10-03 Toppan Printing Co Ltd Observation sample preparation tool
JP5898822B1 (en) * 2016-01-29 2016-04-06 株式会社ミラック光学 Work holding device and dovetail sliding stage with work holding device
CN105699159A (en) * 2016-04-22 2016-06-22 大唐东北电力试验研究所有限公司 Metallographic specimen clamping device
CN205520941U (en) * 2016-04-26 2016-08-31 四川建筑职业技术学院 Metallographic specimen grinds anchor clamps
CN205786026U (en) * 2016-06-24 2016-12-07 福州大学 A kind of auxiliary clamp being applicable to small size wire rod and thin plate sample metallographic sample preparation
CN206862735U (en) * 2017-05-16 2018-01-09 福州大学 Suitable for rod, the fixture of wire rod metallographic specimen

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109283027A (en) * 2018-11-05 2019-01-29 长沙岱勒新材料科技股份有限公司 Diamond wire metallographic specimen producing device and method
CN109283027B (en) * 2018-11-05 2023-10-13 长沙岱勒新材料科技股份有限公司 Diamond wire metallographic specimen manufacturing device and method
CN110411855A (en) * 2019-08-06 2019-11-05 无锡锡洲电磁线有限公司 Pole bend test device
CN110579384A (en) * 2019-08-28 2019-12-17 长江存储科技有限责任公司 Sample clamp

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