CN107126813A - A kind of structure and control method of stepless varying duty pressure swing adsorption air separator - Google Patents

A kind of structure and control method of stepless varying duty pressure swing adsorption air separator Download PDF

Info

Publication number
CN107126813A
CN107126813A CN201710470771.0A CN201710470771A CN107126813A CN 107126813 A CN107126813 A CN 107126813A CN 201710470771 A CN201710470771 A CN 201710470771A CN 107126813 A CN107126813 A CN 107126813A
Authority
CN
China
Prior art keywords
product
air
product gas
plc
duration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710470771.0A
Other languages
Chinese (zh)
Inventor
蔡荣荣
沈强
孟翰武
李永春
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SMC ASIA GAS SYSTEM CHENGDU CO Ltd
Original Assignee
SMC ASIA GAS SYSTEM CHENGDU CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SMC ASIA GAS SYSTEM CHENGDU CO Ltd filed Critical SMC ASIA GAS SYSTEM CHENGDU CO Ltd
Priority to CN201710470771.0A priority Critical patent/CN107126813A/en
Publication of CN107126813A publication Critical patent/CN107126813A/en
Priority to TW107115710A priority patent/TWI657856B/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047Pressure swing adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/30Particle separators, e.g. dust precipitators, using loose filtering material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26Drying gases or vapours
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/80Water
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2258/00Sources of waste gases
    • B01D2258/06Polluted air
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40007Controlling pressure or temperature swing adsorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Separation Of Gases By Adsorption (AREA)

Abstract

The invention discloses a kind of structure and control method of stepless varying duty pressure swing adsorption air separator, including the air compressor being sequentially connected, air dryer, air cleaner, air cushioning tank, PSA air-separating plants, product gas surge tank and product stream gauge, product gas surge tank is communicated with product analysis instrument, and air compressor is connected with air;Product stream gauge is connected with product gas output channel, in addition to PLC, and PLC is connected with PSA air-separating plants, product gas surge tank, product stream gauge and product analysis instrument simultaneously.Invention increases automatic detection product gas pressure, product gas flow and product gas purity and electric signal is fully entered into PLC, analyzed and processed, it is determined that the real demand amount of instant product gas, automatic " STOPPING " step duration for calculating Load Regulation, realize that product purity is not raised and the decline of corresponding proportion air supply, so as to realize the energy-saving effect under reduction load condition.

Description

A kind of structure and control method of stepless varying duty pressure swing adsorption air separator
Technical field
The invention belongs to PSA Gas separation field, and in particular to a kind of stepless varying duty pressure swing adsorption air separation The structure and control method of device.
Background technology
Pressure swing adsorption air separator produces nitrogen or oxygen, is current the most commonly used acquisition product nitrogen at normal temperatures One of device of gas and oxygen.
But the pressure swing adsorption air separator of prior art, is usually free of the specific aim measure of Load Regulation.Once The demand of product can cause the pressure rise in all-product line, transformation naturally less than flow at full capacity when user is Shi Jishiyong Absorption air-separating plant is experienced after this pressure rise automatically, causes the reduction of flow, while can cause product purity Automatic rise.This process is a kind of adaptive process, the result is that:The flow of device deviates and got over less than flow at full capacity Many, the pressure of product can be higher, and the purity of product correspondingly also can be higher.Although product purity carries after this flow-reduction Height, there is a small amount of energy-saving effect, but after being improved due to purity, the ratio of raw air amount and the product gas scale of construction also correspondingly rises Height, even if in the case of reducing the product gas scale of construction, the consumption of compressed air can not press corresponding flow linearly Reduction trend saves the energy, it is clear that the purity after flow-reduction is raised automatically, and this is a kind of waste of the energy.
The content of the invention
The technical problems to be solved by the invention are existing pressure swing adsorption air separator all pins without Load Regulation Energy waste is caused to property measure, its object is to provide a kind of stepless varying duty pressure swing adsorption air separator structure and Control method, the structure and control method are by reasonably controlling so that in the case of being basically unchanged of product purity, automatically Step-less adjustment control is carried out, so as to save the consumption of the energy.
The present invention is achieved through the following technical solutions:
A kind of structure of stepless varying duty pressure swing adsorption air separator, including air compressor, the sky being sequentially connected Gas dryer, air cleaner, air cushioning tank, PSA air-separating plants, product gas surge tank and product stream gauge, and Product gas surge tank is communicated with product analysis instrument, and the air compressor is connected with air;Product stream gauge and product gas Body output channel is connected, in addition to PLC, and PLC is buffered with PSA air-separating plants, product gas simultaneously Tank, product stream gauge and the connection of product analysis instrument.Nitrogen or oxygen are produced using pressure-variable adsorption separation air assembly at present, are to work as The modern the most commonly used device for obtaining product nitrogen gas and oxygen at normal temperatures, and pressure swing adsorption air separation process, not one Straight is all that flow is run, it is necessary to according to the demand of user's product when actual use, if product when user is actual use at full capacity Greater than flow at full capacity, now device is all oepration at full load, is not required to make any adjustments, once but user is real The demand of product is less than flow at full capacity when border is used, and it can cause the pressure rise in all-product line naturally, due to transformation Corresponding matching relationship is provided with inside absorption air-separating plant, when pressure swing adsorption air separator experiences this automatically Plant after pressure rise, cause the reduction of flow, while the automatic rise of product purity can be caused.This process is a kind of adaptive Process, the result is that:The flow of device deviates and more less than flow at full capacity, and the pressure of product can be higher, and product Purity correspondingly also can be higher.Although the raising of product purity after this flow-reduction, has a small amount of energy-saving effect, due to pure After degree is improved, the ratio of raw air amount and the product gas scale of construction is also correspondingly raised, even if reducing the situation of the product gas scale of construction Under, the consumption of compressed air can not save the energy by corresponding flow-reduction trend linearly, it is clear that flow-reduction Purity afterwards is raised automatically, and this is a kind of waste of the energy.And in some technical process, the purity of gas products is not got over High better, too the product of high-purity can influence subsequently to use on the contrary, cause unnecessary trouble.And in some technical process (such as Omnibus control system), product purity has limiting value, and product purity brings up to limiting value after flow-reduction, and purity is no longer improved, And flow is still being reduced, this has resulted in the bigger waste of the energy.But current pressure swing adsorption air separator is not Have and load is adjusted, cause the demand of product when user is Shi Jishiyong less than flow at full capacity, begin to energy occur Source is wasted.In the prior art, the purity of the pressure of product gas, the flow of product gas and product gas, is all probably isolated Instrument, it may be possible to type field, simply independently go observation pressure value, flow value and product purity, by observation respectively, The running status of judgment means is gone, necessary human intervention operation, such as regulation purity, regulation flow etc. is carried out.Partial devices Independent purity control valve, or product pressure maintaining valve, or flow control valve can be set, but the purpose of this control is to ensure dress The purity put is not less than the purity of setting, or product pressure stabilization is more than setting value, or flow value does not allow more than volume Definite value.And purity exceedes setting value, or product pressure is more than setting value, or user reduced using end traffic demand amount after draw The purity rise risen, not such control can solve power saving, and carry out pointedly multi-parameter regulation control.Existing In technology, the main purpose of PLC is, according to predetermined action sequence, to go to control the switch of the switch valve of more than 8 Action, so as to realize the purpose of pressure swing adsorption technique output products gas.
And the annexation of the present invention be perfect above-mentioned these measurement signals and PLC, all these signals with PLC acceptable standard signal enter in PLC analyzed, computing, understand that device was required at that time The actual negative charge values wanted.When finding that device load is less than rated load, PLC can send a signal, in device Original " boosting --- absorption generation product gas --- press --- decompression regeneration --- pressing --- is boosted " so Zhou Erfu In the circulation step of beginning, increase " STOPPING " step, i.e., step of " pausing ", the time length of the step is controlled by PLC The calculated result of device processed is determined.Simultaneously as being possible to go out suddenly for the usage amount of product gas in view of user Situation about now increasing, PLC be able to will be judged exactly according to the measurement signal being collected into, and existing side by side can do Go out reaction, implement to increase the measure of gas production.Therefore, this load down, to increase load to rated output, realizes two-way tune Section.
The control mode that this programme is provided, situation of the demand less than flow at full capacity of product when user is Shi Jishiyong Under, the change of this demand reduction can be perceived by detection means, in the case of being basically unchanged of product purity, is entered automatically Row step-less adjustment is controlled.Because product purity is not raised, identical purity level when stilling remain in full production, therefore it is former The ratio of material air capacity and the product gas scale of construction does not also change correspondingly, so as to realize:As long as product gas flow is reduced, raw material Reduce to the basic linear ratio of the demand of compressed air, so as to save the consumption of the energy.Its specific control method is:
Air is sequentially entered into air compressor, air dryer, air cleaner, air cushioning tank, PSA along pipeline Air-separating plant, product gas surge tank and product stream gauge, a small amount of sample gas are entered in product analysis instrument, PLC controls Device processed is to PSA air-separating plants, product gas surge tank, product gas pressure transmitter, product stream gauge and product analysis Status information in instrument detected, the load condition in plant running, so as to issue instructions to PSA air-separating plants In all switching valve, utilize " STOPPING " step, the set of time of this step obtained by the calculating of PLC, The calculation formula of STOPPING durations is as follows:
(single column each cycle adsorbs duration+valve event interval to STOPPING durations (second)=metered flow of operating at full capacity x Duration+ press duration)/actual measurement reduction load after sign flow-single column each cycle absorption duration-valve event interval when It is long-to press duration,
Wherein:
Operate at full capacity metered flow --- the product stream value of design;
Single column each cycle adsorbs duration --- determined by the variety classes of molecular sieve;
Valve event interval duration --- consider the duration of valve event speed, according to valve species and the difference of bore, For any one duration between 0 second, or 0~2 second;
Press duration --- the duration according to determined by different pressure swing adsorption technique conditions;
Sign flow after the reduction load of actual measurement --- it is the product gas instantaneous delivery of actual measurement, or in a period Average discharge,
STOPPING durations be arranged on detect product purity it is below standard when, even if detecting traffic load has decline, this Load down program can not be performed;
When any one following situation is detected, PLC can send instruction immediately, stop load down regulation State, so that the state of the oepration at full load of recovery device immediately, so as to ensure the stabilization of device purity, adapts to user to product The change operating mode needs quickly increased or decreased of gas demand:
(A) when PLC perceives when increasing to metered flow of product flow;
(B) when the pressure that PLC perceives product conveyance conduit be reduced to below rated pressure 0.005 to During 0.015MPa, this value is set according to the field adjustable situation of device;
(C) when PLC is perceived:The product purity (%) of product purity difference (%)=actual measurement-user's license During minimum product purity (%)=0, i.e. only when product purity is higher than the minimum product purity that user permits, can hold The energy-conservation program of row reduction load.
Product gas pressure transmitter, and product gas pressure are provided between product gas surge tank and PLC Transmitter is connected with product gas surge tank and PLC simultaneously, and product gas pressure transmitter electric signal is controlled with PLC Device is connected.Be provided with two or more adsorption towers in PSA air-separating plants, and adsorption tower with air cushioning tank With the connection of product gas surge tank.Correspondingly, it is provided with the control switching valve of six or more.All control switching valves, Receive the control of PLC, between PLC and control switching valve, be connected control with electric signal.Air cleaner At least one, when air cleaner quantity is more than one, it is separately positioned between air compressor and air dryer, Between air dryer and air cushioning tank, and it is sequentially communicated.The entrance of product stream gauge is connected with product gas surge tank, Product stream gauge electricity consumption signal is connected with PLC, gas sample mouthful and product gas surge tank and the production of product analysis instrument The pipeline of product flowmeter connection is connected, and the electric signal of product analysis instrument is connected with PLC.Pass through above-mentioned various telecommunications Just can (pressure, flow and product be pure according to each detection means summary information in connection number with PLC, PLC Degree), the load condition analyzed in plant running can be calculated, so as to issue instructions to institute in PSA air-separating plants Some programme-control switching valves, in original running at full capacity control program, increase " STOPPING " step, this step Set of time by PLC calculating obtained by, its time span can be it is stepless, so as to realize step-less adjustment bear Lotus.In this regulation control process, " STOPPING " Step Time that PLC is sent is longer, illustrates the load of device Smaller, the time of air compressor load down unloading operation is also longer, or the air capacity asked for from compressed air pipe network is fewer, from And the purpose of energy-conservation can be realized.The continuous output of product gas after " STOPPING " step performs stage, reduction load, Dependent on the product gas surge tank set in system.Therefore the maximum stepless varying duty adjustable range of such device can reach 30~100%.
The present invention compared with prior art, has the following advantages and advantages:
(1) automatic detection product gas pressure, product gas flow and product gas purity are added and electric signal is complete Portion inputs PLC, is analyzed and processed, it is determined that the real demand amount of product gas immediately, calculates Load Regulation automatically " STOPPING " step duration, realize that product purity is not raised and the decline of corresponding proportion air supply, so as to realize drop Energy-saving effect in the case of underload;
(2) in the case where device flow is not done and changed, by the renewal of detection means, and corresponding electric signal and control The connection of system processed, is reasonably calculated, the mode of output control signal, realizes that pressure swing adsorption air separator load is adjusted The function of section;
(3) in the case where pressure swing adsorption air separator hardly increases purchase cost, it is possible to achieve user uses It is long-term energy-saving in process.
Brief description of the drawings
Accompanying drawing described herein is used for providing further understanding the embodiment of the present invention, constitutes one of the application Point, do not constitute the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is schematic flow sheet of the present invention.
Mark and corresponding parts title in accompanying drawing:
1- air compressors, 2- air dryers, 3- air cleaners, 4- air cushioning tanks, 5-PSA air separation dress Put, 6- product gas surge tanks, 6P- product gas pressure transmitters, 7- product stream gauge, 8- product analysis instrument, 9-PLC controls Device.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment and accompanying drawing, to this Invention is described in further detail, and exemplary embodiment and its explanation of the invention is only used for explaining the present invention, does not make For limitation of the invention.
Embodiment 1:
As shown in figure 1, a kind of structure of stepless varying duty pressure swing adsorption air separator, its hardware configuration is included successively The air compressor 1 of connection, air dryer 2, air cleaner 3, air cushioning tank 4, PSA air-separating plants 5, product gas Body surge tank 6 and product stream gauge 7, and product gas surge tank 6 is communicated with product analysis instrument 8, the gas of product analysis instrument 8 takes The pipeline that sample mouthful is connected with product gas surge tank 6 and product stream gauge 7 is connected, and air compressor 1 is connected with air, Extract ambient air, the unstrpped gas separated after compression as air;Product stream gauge 7 is connected with product gas output channel Connect, the entrance of product stream gauge 7 is connected with product gas surge tank 6, PLC 9 simultaneously with PSA air-separating plants 5, Product gas surge tank 6, product stream gauge 7 and product analysis instrument 8 are connected, and product analysis instrument 8 and product stream gauge 9 all use telecommunications Number it is connected with PLC, product gas pressure transmitter is also provided between product gas surge tank 6 and PLC 9 6P, and product gas pressure transmitter 6P, while being connected with product gas surge tank 6 and PLC 9, product gas pressure becomes Device 6P electric signals are sent to be connected with PLC 9.Wherein air cleaner 3 is at least one, when air cleaner 3 is one, It is arranged between air dryer 2 and air cushioning tank 4, and when the quantity of air cleaner 3 is more than one, it is separately positioned on Between air compressor 1 and air dryer 2, between air dryer 2 and air cushioning tank 4, form air compressor 1, it is empty Air filter 3, air dryer 2, air cleaner 3 and air cushioning tank 4 are sequentially communicated.Wherein air cleaner 3 can be with It is the filter of Chalk-dust filtering type or the active carbon filter with removing lube vapor function.In the separation In device, two or more adsorption towers are provided with, correspondingly, the control switching valve of six or more are provided with.It is all Control switching valve, receive the programme-control of PLC, PLC and control switching valve between, use electric signal phase Connection control., just can be according to each detection means in PLC by the connection of above-mentioned various electric signals and PLC Summary information (pressure, flow and product purity), can calculate the load condition analyzed in plant running, so as to send Instruct to control switching valve all in PSA air-separating plants, in original running at full capacity control program, increase by one " STOPPING " step, the set of time of this step obtained by the calculating of PLC, its time span can be it is stepless, So as to realize step-less adjustment load.In this regulation control process, during " STOPPING " step that PLC is sent Between it is longer, illustrate that the load of device is smaller, the time of air compressor load down unloading operation is also longer, or from compressed air hose The air capacity that rete cord takes is fewer, so as to realize the purpose of energy-conservation.The maximum stepless varying duty adjustable range of such device can To reach 30~100%.When PLC perceives the unexpected increase of product flow, or pressure quick reduction, or purity goes out Existing downward trend, instruction can be sent immediately, stop load down adjustment state, so that the oepration at full load of recovery device immediately State, so as to ensure the stabilization of device purity, adapt to the change that quickly increases or decreases of the user to product gas demand Operating mode needs.
Its specific control method is:Air is sequentially entered into air compressor 1, air dryer 2, air along pipeline Filter 3, air cushioning tank 4, PSA air-separating plants 5, product gas surge tank 6 and product stream gauge 7, and enter production In product analyzer 8, PLC 9 is to PSA air-separating plants 5, product gas surge tank 6, product gas pressure transmitter Status information in 6P, product stream gauge 7 and product analysis instrument 8 detected, the load condition in plant running, so that Switching valves all in PSA air-separating plants 5 are issued instructions to, " STOPPING " step, the set of time of this step is utilized Obtained by the calculating of PLC 9, the calculation formula of STOPPING durations is as follows:
(single column each cycle adsorbs duration+valve event interval to STOPPING durations (second)=metered flow of operating at full capacity x Duration+ press duration)/actual measurement reduction load after sign flow-single column each cycle absorption duration-valve event interval when It is long-to press duration,
Wherein:
Operate at full capacity metered flow --- the product stream value of design;
Single column each cycle adsorbs duration --- determined by the variety classes of molecular sieve;
Valve event interval duration --- consider the duration of valve event speed, according to valve species and the difference of bore, For any one duration between 0 second, or 0~2 second;
Press duration --- the duration according to determined by different pressure swing adsorption technique conditions;
Sign flow after the reduction load of actual measurement --- can be the product gas instantaneous delivery or one of actual measurement Average flow rate value in the individual period.It can specifically be determined according to the product gas of user using characteristic, i.e. for continuous steady Surely gas is used, simply occurs the occasion of stable low discharge once in a while, gas instantaneous delivery value can be used;And for long-term with gaseity Occasion in fluctuation status, the sign flow that the flow value of low flow state in short-term can not be run as load down.Only Underrun state is in certain period of time for a long time when PLC is detected, then can be by the average discharge in the period The sign flow that value is run as load down.
STOPPING durations be arranged on detect product purity it is below standard when, even if detecting traffic load has decline, this Load down program can not be performed;
(2) any one situation is detected in (A), (B), (C) below, and PLC 9 can send finger immediately Order, stops load down adjustment state, so that the state of the oepration at full load of recovery device immediately, so as to ensure the steady of device purity It is fixed, adapt to the change operating mode needs that quickly increase or decrease of the user to product gas demand:
(A) when PLC perceives when increasing to metered flow of product flow;
(B) when the pressure that PLC perceives product conveyance conduit is reduced to a certain value below rated pressure, this value Set according to the field adjustable situation of device;
(C) when PLC is perceived:The product purity (%) of product purity difference (%)=actual measurement-user's license During minimum product purity (%)=0, i.e. only when product purity is higher than the minimum product purity that user permits, can hold The energy-conservation program of row reduction load.
For example:When device carries out making nitrogen by pressure swing adsorption, its metered flow of operating at full capacity is set as 100Nm3/ h, product Nitrogen gas purity 99.9%, the minimum product purity 99.8% of user's license, product pressure 0.6MPag.Process conditions are:Single column is every Cycle absorption duration 60 seconds, valve event interval duration 1 second presses duration 3 seconds.
1. when detecting the flow value stabilization in device 2 minutes in 90Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
(single column each cycle adsorbs duration+valve event interval to STOPPING durations (second)=metered flow of operating at full capacity x Duration+ press duration)/actual measurement reduction load after sign flow-single column each cycle absorption duration-valve event interval when Duration grow-is pressed, i.e.,
100x(60+1+3)/90-60-1-3
=7.1 (seconds)
That is PLC can send instruction implement STOPPING steps when a length of 7.1 seconds;
2. when detecting the flow value stabilization in device 2 minutes in 80Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=100x (60+1+3)/80-60-1-3=16 (second)
That is PLC can send instruction implement STOPPING steps when a length of 16 seconds;
3. when detecting the flow value stabilization in device 2 minutes in 70Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=100x (60+1+3)/70-60-1-3=27.4 (second)
That is PLC can send instruction implement STOPPING steps when a length of 27.4 seconds;
4. when detecting the flow value stabilization in device 2 minutes in 60Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=100x (60+1+3)/60-60-1-3=42.7 (second)
That is PLC can send instruction implement STOPPING steps when a length of 42.7 seconds;
5. when detecting the flow value stabilization in device 2 minutes in 50Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=100x (60+1+3)/50-60-1-3=64 (second)
That is PLC can send instruction implement STOPPING steps when a length of 64 seconds;
6. when detecting the flow value stabilization in device 2 minutes in 30Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=100x (60+1+3)/30-60-1-3=149.3 (second)
That is PLC can send instruction implement STOPPING steps when a length of 149.3 seconds.
Calculate above for being all suitable under any actual flow loading condiction, and be continuous, therefore be a kind of stepless The method of regulation.But it is not recommended that still carrying out this load down program below 30% load, it otherwise will appear from product gas pure The reduction of degree.
Above example, (can set), or work as when finding that product pressure is less than 0.59MPag according to field adjustable situation It was found that product purity (can be set) when being reduced to the 99.8% of user's license according to the requirement of user, i.e. product purity difference (%) During minimum product purity (%)=99.8%-99.8%=0 of the product purity (%) of=actual measurement-user's license, PLC Instruction will be sent, stops load down operation program immediately, and returns to oepration at full load program first, while in follow-up detection During, further according to new burden requirement, implement new spatial load forecasting, so as to reach the purity under new load down state, pressure The balance of power and flow.
Embodiment 2:
On the basis of above-described embodiment, two or more adsorption towers are provided with PSA air-separating plants 5, And adsorption tower is connected with air cushioning tank 4 and product gas surge tank 6.Adsorbent is filled with each adsorption tower, is inhaled Attached dose of species difference, this programme had both been applicable to adsorbent adsorption of oxygen, has produced the device of nitrogen, was equally applicable to adsorbent suction Attached nitrogen, the device for producing oxygen.That is swing adsorption nitrogen producing apparatus and the applicable this programme of pressure swing adsorption oxygen making device.
For example:When device carries out omnibus control system, metered flow of operating at full capacity is 50Nm3/ h, product oxygen is pure Degree 93%, product pressure 0.4MPag.Process conditions are:Single column each cycle absorption duration 75 seconds, valve event interval duration 1 second, Press duration 15 seconds.
1. when detecting the flow value stabilization in device 3 minutes in 50Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
(single column each cycle adsorbs duration+valve event interval to STOPPING durations (second)=metered flow of operating at full capacity x Duration+ press duration)/actual measurement reduction load after sign flow-single column each cycle absorption duration-valve event interval when Duration grow-is pressed, i.e.,
50x(75+1+15)/50-75-1-15
=0 (second)
That is PLC can send instruction implement STOPPING steps when a length of 0 second, i.e., do not reduce load;
2. when detecting the flow value stabilization in device 3 minutes in 40Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=50x (75+1+15)/40-75-1-15=22.8 (second)
That is PLC can send instruction implement STOPPING steps when a length of 22.8 seconds;
3. when detecting the flow value stabilization in device 3 minutes in 30Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=50x (75+1+15)/30-75-1-15=60.7 (second)
That is PLC can send instruction implement STOPPING steps when a length of 60.7 seconds;
4. when detecting the flow value stabilization in device 3 minutes in 15Nm3During/h, implement load down energy-conservation program STOPPING duration calculations are as follows,
According to calculating formula:
STOPPING durations (second)=50x (75+1+15)/15-75-1-15=212.3 (second)
That is PLC can send instruction implement STOPPING steps when a length of 212.3 seconds;
Calculate above for being all suitable under any actual flow loading condiction, and be continuous, therefore be a kind of stepless The method of regulation.Similarly for pressure swing adsorption oxygen making device also it is not recommended that still carrying out this load down journey below 30% load Sequence, otherwise will appear from the reduction of product gas purity.
Above example, (can set), or work as when finding that product pressure is less than 0.39MPag according to field adjustable situation It was found that product purity be reduced to user license 90% when (can be set according to the requirement of user), i.e., product purity difference (%)= During minimum product purity (%)=90%-90%=0 of the product purity (%) of actual measurement-user's license, PLC will be sent Instruction, stops load down operation program immediately, and returns to oepration at full load program first, while in follow-up detection process In, further according to new burden requirement, implement new spatial load forecasting so that reach the purity under new load down state, pressure with The balance of flow.
Embodiment 3:
On the basis of above-described embodiment, this programme applies also for vacuum pressure swing adsorption device for oxygen production, this kind of technical process During the desorption and regeneration of adsorption tower, vavuum pump has been used to carry out vacuumize process, other principles and pressure swing adsorption air point Identical from principle of device, the implementation method of this programme is identical.
Above-described embodiment, has been carried out further to the purpose of the present invention, technical scheme and beneficial effect Describe in detail, should be understood that the embodiment that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc. all should be included Within protection scope of the present invention.

Claims (7)

1. a kind of structure of stepless varying duty pressure swing adsorption air separator, it is characterised in that including the air being sequentially connected Compressor (1), air dryer (2), air cleaner (3), air cushioning tank (4), PSA air-separating plants (5), product gas Body surge tank (6) and product stream gauge (7), and product gas surge tank (6) is communicated with product analysis instrument (8), the air pressure Contracting machine (1) is connected with air;Product stream gauge (7) is connected with product gas output channel, in addition to PLC (9), PLC (9) with PSA air-separating plants (5), product gas surge tank (6), product stream gauge (7) and product while divide Analyzer (8) is connected.
2. a kind of structure of stepless varying duty pressure swing adsorption air separator according to claim 1, it is characterised in that Product gas pressure transmitter (6P), and product gas are provided between the product gas surge tank (6) and PLC (9) Body pressure transmitter (6P) with product gas surge tank (6) and PLC (9) while be connected.
3. a kind of structure of stepless varying duty pressure swing adsorption air separator according to claim 1, it is characterised in that Be provided with two or more adsorption towers in the PSA air-separating plants (5), and adsorption tower with air cushioning tank (4) connected with product gas surge tank (6).
4. a kind of structure of stepless varying duty pressure swing adsorption air separator according to claim 1, it is characterised in that The air cleaner (3) is at least one, and when air cleaner (3) quantity is more than one, it is separately positioned on air pressure Between contracting machine (1) and air dryer (2), between air dryer (2) and air cushioning tank (4), and it is sequentially communicated.
5. a kind of knot of stepless varying duty pressure swing adsorption air separator as claimed in any of claims 1 to 4 Structure, it is characterised in that the entrance of the product stream gauge (7) is connected with product gas surge tank (6).
6. a kind of structure of stepless varying duty pressure swing adsorption air separator according to claim 5, it is characterised in that The pipeline that the gas sample mouthful of the product analysis instrument (8) is connected with product gas surge tank (6) and product stream gauge (7) is connected Connect.
7. a kind of control method of stepless varying duty pressure swing adsorption air separator, it is characterised in that comprise the following steps:
(1) air sequentially enters air compressor (1), air dryer (2), air cleaner (3), air cushioning along pipeline Tank (4), PSA air-separating plants (5), product gas surge tank (6) and product stream gauge (7), sample gas enters product In analyzer (8), PLC (9) becomes to PSA air-separating plants (5), product gas surge tank (6), product gas pressure The status information in device (6P), product stream gauge (7) and product analysis instrument (8) is sent to be detected, it is negative in plant running Lotus situation, so as to issue instructions to switching valves all in PSA air-separating plants (5), utilizes " STOPPING " step, this step Rapid set of time is obtained by the calculating of PLC (9), and the calculation formula of STOPPING durations is as follows:
(single column each cycle adsorbs duration+valve event interval duration to STOPPING durations (second)=metered flow of operating at full capacity x + press duration)/the sign flow reduced after load surveyed-single column each cycle absorption duration-valve event interval duration- Press duration,
Wherein:
Operate at full capacity metered flow --- the product stream value of design;
Single column each cycle adsorbs duration --- determined by the variety classes of molecular sieve;
Valve event interval duration --- consider the duration of valve event speed, be 0 according to valve species and the difference of bore Second, or any one duration between 0~2 second;
Press duration --- the duration according to determined by different pressure swing adsorption technique conditions;
Sign flow after the reduction load of actual measurement --- for the product gas instantaneous delivery of actual measurement, or putting down in a period Equal flow,
STOPPING durations be arranged on detect product purity it is below standard when, even if detecting traffic load has decline, this drop is negative Lotus program can not be performed;
(2) any one situation is detected below, and PLC (9) can send instruction immediately, stops load down regulation State, so that the state of the oepration at full load of recovery device immediately, it is ensured that the stabilization of device purity, adapts to user to product gas The change operating mode needs quickly increased or decreased of demand:
(A) when PLC perceives when increasing to metered flow of product flow;
(B) when the pressure that PLC perceives product conveyance conduit is reduced to 0.005 to 0.015MPa below rated pressure When;
(C) when PLC is perceived:It is minimum that the product purity (%) of product purity difference (%)=actual measurement-user permits During product purity (%)=0, i.e. only when product purity is higher than the minimum product purity that user permits, drop can be performed The energy-conservation program of underload.
CN201710470771.0A 2017-06-20 2017-06-20 A kind of structure and control method of stepless varying duty pressure swing adsorption air separator Pending CN107126813A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201710470771.0A CN107126813A (en) 2017-06-20 2017-06-20 A kind of structure and control method of stepless varying duty pressure swing adsorption air separator
TW107115710A TWI657856B (en) 2017-06-20 2018-05-09 Structure and control method of stepless variable load pressure swing adsorption air separation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710470771.0A CN107126813A (en) 2017-06-20 2017-06-20 A kind of structure and control method of stepless varying duty pressure swing adsorption air separator

Publications (1)

Publication Number Publication Date
CN107126813A true CN107126813A (en) 2017-09-05

Family

ID=59735715

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710470771.0A Pending CN107126813A (en) 2017-06-20 2017-06-20 A kind of structure and control method of stepless varying duty pressure swing adsorption air separator

Country Status (2)

Country Link
CN (1) CN107126813A (en)
TW (1) TWI657856B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111921338A (en) * 2020-07-31 2020-11-13 苏州成于思气体科技有限公司 Energy-saving equipment of PSA gas separation system
CN112495137A (en) * 2020-11-12 2021-03-16 杭州汉德空分设备有限公司 Pressure swing adsorption oxygen generating equipment
CN114659028A (en) * 2022-03-23 2022-06-24 乔治洛德方法研究和开发液化空气有限公司 Method and apparatus for controlling gas supply of gas supply system
CN114768470A (en) * 2022-05-09 2022-07-22 上海瑞气气体科技有限公司 Pressure swing adsorption gas separation equipment and method, and regulation metering control system and method

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1171286A (en) * 1996-06-19 1998-01-28 美国Boc氧气集团有限公司 Pressure swing adsorption process turndown control
JP3781187B2 (en) * 2001-06-29 2006-05-31 大陽日酸株式会社 Operation method of pressure fluctuation adsorption gas separation device
CN201199326Y (en) * 2008-04-29 2009-02-25 华东理工大学 Automation observe and control system for gas separation experimental equipment
CN203159227U (en) * 2013-04-10 2013-08-28 广东胜捷工业安全技术有限公司 Intelligent nitrogen-making device
CN205709868U (en) * 2016-04-20 2016-11-23 苏州杜尔气体化工装备有限公司 A kind of swing adsorption nitrogen producing apparatus

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090071333A1 (en) * 2006-10-04 2009-03-19 Air Products And Chemicals, Inc. Performance Stability in Shallow Beds in Pressure Swing Adsorption Systems
CN201245433Y (en) * 2008-04-30 2009-05-27 珠海市奥吉赛科技有限公司 Energy-saving air separation oxygen production apparatus
CN203820458U (en) * 2014-04-30 2014-09-10 赣州川汇气体设备制造有限公司 PSA (Pressure Swing Adsorption) nitrogen production output device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1171286A (en) * 1996-06-19 1998-01-28 美国Boc氧气集团有限公司 Pressure swing adsorption process turndown control
JP3781187B2 (en) * 2001-06-29 2006-05-31 大陽日酸株式会社 Operation method of pressure fluctuation adsorption gas separation device
CN201199326Y (en) * 2008-04-29 2009-02-25 华东理工大学 Automation observe and control system for gas separation experimental equipment
CN203159227U (en) * 2013-04-10 2013-08-28 广东胜捷工业安全技术有限公司 Intelligent nitrogen-making device
CN205709868U (en) * 2016-04-20 2016-11-23 苏州杜尔气体化工装备有限公司 A kind of swing adsorption nitrogen producing apparatus

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111921338A (en) * 2020-07-31 2020-11-13 苏州成于思气体科技有限公司 Energy-saving equipment of PSA gas separation system
CN112495137A (en) * 2020-11-12 2021-03-16 杭州汉德空分设备有限公司 Pressure swing adsorption oxygen generating equipment
CN112495137B (en) * 2020-11-12 2022-04-19 杭州汉德空分设备有限公司 Pressure swing adsorption oxygen generating equipment
CN114659028A (en) * 2022-03-23 2022-06-24 乔治洛德方法研究和开发液化空气有限公司 Method and apparatus for controlling gas supply of gas supply system
CN114768470A (en) * 2022-05-09 2022-07-22 上海瑞气气体科技有限公司 Pressure swing adsorption gas separation equipment and method, and regulation metering control system and method
CN114768470B (en) * 2022-05-09 2024-01-26 上海瑞气气体科技有限公司 Pressure swing adsorption gas separation equipment and method, and metering adjustment control system and method

Also Published As

Publication number Publication date
TWI657856B (en) 2019-05-01
TW201904647A (en) 2019-02-01

Similar Documents

Publication Publication Date Title
CN107126813A (en) A kind of structure and control method of stepless varying duty pressure swing adsorption air separator
CN106365123B (en) A kind of list lobe pump double acting medical molecular sieve oxygen generation system and method for producing oxygen through
CN211419580U (en) Energy-saving modular pressure swing adsorption nitrogen making system
CN201002974Y (en) Energy-saving hollow fibrous membrane separation nitrogen producing machine
CN109113130A (en) A kind of method of secondary water-supply force (forcing) pump persistent pressure
CN208894828U (en) A kind of filter rod forming machine concentration technique wind power dedusting system
CN201637226U (en) Device for recycling high-purity tail nitrogen gas through air separation
CN205080411U (en) Full -automatic frequency conversion control system
CN205527752U (en) Industry frequency conversion nitrogen generator
CN110203895A (en) A kind of the circulatory purification system and circulatory purification method of helium
CN206188389U (en) Pressure swing adsorption nitrogen making machine
CN203829882U (en) Product gas output device of high-purity high-pressure gas production device
CN205118663U (en) Gas appliances's high -low pressure adjusting device
CN205223358U (en) Automatic integrated control system that supplies of hydrogen
CN113813752A (en) Metering control system, gas separation device, control method, and storage medium
CN203620478U (en) Intelligent control device for pressure swing adsorption equipment
CN203656578U (en) Wide-gas inflow constant-flow CNG compression plant
CN209025822U (en) A kind of energy-saving control system for industrial air compression system
CN202116301U (en) Oxygen and oxygen-enriched air preparation device
CN203829880U (en) Raw material gas preprocessing device special for high-purity high-pressure gas preparation device
CN205933226U (en) DBD type ozone generator system
CN203829881U (en) PSA (Pressure Swing Adsorption) technology based high-purity and high-pressure gas production device
CN207004751U (en) A kind of nitrogen compressor system
CN206308017U (en) A kind of energy conserving system of varying-voltage adsorption nitrogen machine
CN103723684A (en) Oxygen generator with cyclic filtration function

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170905

RJ01 Rejection of invention patent application after publication