CN107125020A - A kind of wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus - Google Patents
A kind of wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus Download PDFInfo
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- CN107125020A CN107125020A CN201710249157.1A CN201710249157A CN107125020A CN 107125020 A CN107125020 A CN 107125020A CN 201710249157 A CN201710249157 A CN 201710249157A CN 107125020 A CN107125020 A CN 107125020A
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Abstract
The invention discloses a kind of wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus, it is related to fungus growing technique field, is made up of the raw material of following parts by weight:15 20 parts of atlapulgite polyvinyl alcohol, 5 10 parts of water soluble chitosan, 35 parts of chitosan oligosaccharide ceramic, 12 parts of carbomer, 12 parts of pre-gelatinized potato starch, 0.5 1 parts of modified meerschaum particle, 0.5 1 parts of polyethylene glycol oxide, 0.3 0.5 parts of plant ash, 0.3 0.5 parts of polydextrose, 0.05 0.1 parts of poly-D-lysine.The wooden water conservation inorganic agent of the segment wood cultivated use section of the made black fungus of the present invention is easy to use, long action time and the normal growth for not interfering with black fungus.
Description
Technical field:
The present invention relates to fungus growing technique field, and in particular to a kind of wooden water conservation processing of the segment wood cultivated use section of black fungus
Agent.
Background technology:
Segment wood cultivated is the major way of cultivation of auricularia auricula, and cultivation ear tree is used as from the seeds of Fagaceae, Betulaceae.It is black
Needed before agaric inoculation sawed Duan Mu, frame is shone in high-land, drying, ventilation, place on the sunny side, it is fermented as early as possible.Often
Stirred once every 10 days or so, promote the wooden uniform drying of section.General frame shines 30-40 days, and Duan Mu has seven, most probably done, you can carry out
Inoculation.As Duan Mu has infection miscellaneous bacteria, insect, it can be smouldered before inoculation with cogongrass or branch, be degree to epidermis blackening, can both remove
Disease pest, can strengthen bark heat absorption, water absorbing properties, the growth of favourable black fungus mycelia again.
Duan Mu water absorbing properties directly affect the speed of growth of black fungus, and black fungus can not accurately be supplied by manually applying water
Real water requirement.In order to solve this problem, our company develops a kind of wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus,
Be sprayed on the Duan Mu before inoculation, be attached to water conservation inorganic agent on Duan Mu both can by the moisture in absorption air come to
Black fungus supply growth moisture, and the rainwater for exceeding black fungus water requirement can be absorbed or water is manually applied, and delay when moisture is reduced
The slow water release by absorption is to black fungus, so as to ensure the normal growth water requirement of black fungus.
The content of the invention:
The technical problems to be solved by the invention are to provide a kind of easy to use, long action time and do not interfere with black wood
The wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus of ear normal growth.
The technical problems to be solved by the invention are realized using following technical scheme:
A kind of wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus, is made up of the raw material of following parts by weight:
Atlapulgite -15-20 parts of polyvinyl alcohol, 5-10 parts of water soluble chitosan, chitosan oligosaccharide -3-5 parts of ceramic, card ripple
1-2 parts of resin, 1-2 parts of pre-gelatinized potato starch, 0.5-1 parts of modified meerschaum particle, 0.5-1 parts of polyethylene glycol oxide, plant ash
0.3-0.5 parts, 0.3-0.5 parts of polydextrose, 0.05-0.1 parts of poly-D-lysine;
Its preparation method comprises the following steps:
(1) carbomer and polyethylene glycol oxide are added into atlapulgite-polyvinyl alcohol, and with 5 DEG C/min heating speed
Degree is warming up to 115-120 DEG C of insulation grinding 15min, adds modified meerschaum particle and plant ash, continues in 115-120 DEG C of guarantor
Temperature grinding 10min, produces powder I;
(2) pre-gelatinized potato starch and polydextrose are added into chitosan oligosaccharide-ceramic, and with 5 DEG C/min heating
Speed is warming up to 110-115 DEG C of insulation grinding 15min, produces powder II;
(3) powder II, water soluble chitosan and poly-D-lysine are added into powder I, 0-5 DEG C of ring is placed in after being sufficiently mixed
Sealing and standing 2h in border, and 105-110 DEG C of insulation grinding 10min is warming up to 5 DEG C/min programming rate, produce water conservation processing
Agent;
Atlapulgite-the polyvinyl alcohol is to compare 10 by weight:1:0.05 atlapulgite, cold soluble type polyvinyl alcohol and N-
Hydroxyethyl acrylamide is warming up to obtained after 120-125 DEG C of insulation grinding 30min.
Chitosan oligosaccharide-the ceramic is made up of the raw material of following parts by weight:10-15 parts of chitosan oligosaccharide, ceramic
3-5 parts, 1-2 parts of hydroxyethyl cellulose, 0.5-1 parts of PVPP, 0.1-0.3 parts of poly-aspartate, HPMA
0.05-0.1 parts, 50-80 parts of water, its preparation method is:PVPP and poly-aspartate are added into chitosan oligosaccharide, under grinding
115-120 DEG C of insulation grinding 15min is warming up to, ceramic, hydroxyethyl cellulose and HPMA is added, continues
In 115-120 DEG C of insulation grinding 15min, sealing and standing 1h in 0-5 DEG C of environment is then transferred to, and adds 50-55 DEG C of water, it is fully mixed
Close and stood after 50-55 DEG C of insulation in 30min, gained mixed liquor feeding spray dryer, dry gained particle through ultramicro grinding
Micro mist is made in machine, as chitosan oligosaccharide-ceramic.
The modified meerschaum particle is made by sepiolite powder is modified, and its specific method of modifying is:To sepiolite powder
Middle addition poloxamer and nanometer titanium dioxide, utilize microwave treater microwave treatment 5min, stand 30min follow-up after being sufficiently mixed
Continuous microwave treatment 5min, adds hydrogenated rosin glyceride and rilanit special, microwave treatment 5min again after being well mixed, most
Graininess is made by ball mill, modified meerschaum particle is produced.
The sepiolite powder, poloxamer, nanometer titanium dioxide, the weight ratio of hydrogenated rosin glyceride and rilanit special are
10-15:1-2:0.05-0.1:0.3-0.5:0.1-0.3。
The condition of work of the microwave treater is microwave frequency 2450MHz, power output 700W.
The beneficial effects of the invention are as follows:The wooden water conservation inorganic agent of the segment wood cultivated use section of the made black fungus of the present invention is easy to use,
It need to be only sprayed on when using on the Duan Mu before inoculation, the water conservation inorganic agent being attached on Duan Mu both can be by absorption air
Moisture come to black fungus supply growth moisture, and can absorb the rainwater for exceeding black fungus water requirement or manually apply water, and in water
Divide slowly by the water release of absorption to black fungus when reducing, so as to ensure the normal growth water requirement of black fungus;And act on
Time is long, does not interfere with black fungus normal growth.
Embodiment:
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) 1g carbomers and 0.5g polyethylene glycol oxides are added into 15g atlapulgites-polyvinyl alcohol, and with 5 DEG C/min
Programming rate be warming up to 115-120 DEG C insulation grinding 15min, add 0.5g modified meerschaums particle and 0.3g plant ash,
Continue, in 115-120 DEG C of insulation grinding 10min, to produce powder I;
(2) add 1g pre-gelatinized potato starch and 0.3g polydextroses into 5g chitosan oligosaccharides-ceramic, and with 5 DEG C/
Min programming rate is warming up to 110-115 DEG C of insulation grinding 15min, produces powder II;
(3) powder II, 5g water soluble chitosan and 0.05g poly-D-lysines are added into powder I, is placed in after being sufficiently mixed
Sealing and standing 2h in 0-5 DEG C of environment, and 105-110 DEG C of insulation grinding 10min is warming up to 5 DEG C/min programming rate, produce
Water conservation inorganic agent;
The preparation of atlapulgite-polyvinyl alcohol:By 10g atlapulgites, 1g cold soluble types polyvinyl alcohol and 0.05g N- hydroxyl second
Base acrylamide is warming up to obtained after 120-125 DEG C of insulation grinding 30min.
The preparation of chitosan oligosaccharide-ceramic:0.5g PVPPs and the poly- asparagus fern ammonia of 0.1g are added into 10g chitosan oligosaccharides
115-120 DEG C of insulation grinding 15min is warming up under acid, grinding, 3g ceramics, 1g hydroxyethyl celluloses and 0.05g is added
HPMA, continues, in 115-120 DEG C of insulation grinding 15min, to be then transferred to sealing and standing 1h in 0-5 DEG C of environment, and
60g 50-55 DEG C water is added, is sufficiently mixed and stands 30min, gained mixed liquor feeding spray dryer after 50-55 DEG C of insulation
In, dry gained particle and micro mist is made through micronizer, as chitosan oligosaccharide-ceramic.
The preparation of modified meerschaum particle:1g poloxamers and 0.05g nanometer titanium dioxides are added into 10g sepiolite powders,
Microwave frequency 2450MHz, power output 700W microwave treater microwave treatment 5min are utilized after being sufficiently mixed, 30min is stood
Continue microwave treatment 5min afterwards, add 0.3g hydrogenated rosin glycerides and 0.1g rilanit specials, it is micro- again after being well mixed
Ripple handles 5min, and graininess most is made through ball mill afterwards, modified meerschaum particle is produced.
Embodiment 2
(1) 1g carbomers and 0.5g polyethylene glycol oxides are added into 20g atlapulgites-polyvinyl alcohol, and with 5 DEG C/min
Programming rate be warming up to 115-120 DEG C insulation grinding 15min, add 0.5g modified meerschaums particle and 0.5g plant ash,
Continue, in 115-120 DEG C of insulation grinding 10min, to produce powder I;
(2) add 2g pre-gelatinized potato starch and 0.5g polydextroses into 3g chitosan oligosaccharides-ceramic, and with 5 DEG C/
Min programming rate is warming up to 110-115 DEG C of insulation grinding 15min, produces powder II;
(3) powder II, 10g water soluble chitosan and 0.1g poly-D-lysines are added into powder I, is placed in after being sufficiently mixed
Sealing and standing 2h in 0-5 DEG C of environment, and 105-110 DEG C of insulation grinding 10min is warming up to 5 DEG C/min programming rate, produce
Water conservation inorganic agent;
The preparation of atlapulgite-polyvinyl alcohol:By 10g atlapulgites, 1g cold soluble types polyvinyl alcohol and 0.05g N- hydroxyl second
Base acrylamide is warming up to obtained after 120-125 DEG C of insulation grinding 30min.
The preparation of chitosan oligosaccharide-ceramic:1g PVPPs and 0.2g poly-aspartates are added into 15g chitosan oligosaccharides,
115-120 DEG C of insulation grinding 15min is warming up under grinding, 5g ceramics, 1g hydroxyethyl celluloses and 0.1g hydrolysis is added
HPMA, continues, in 115-120 DEG C of insulation grinding 15min, to be then transferred to sealing and standing 1h in 0-5 DEG C of environment, and add
60g 50-55 DEG C water, is sufficiently mixed and is stood after 50-55 DEG C of insulation in 30min, gained mixed liquor feeding spray dryer, done
Micro mist is made through micronizer in dry gained particle, as chitosan oligosaccharide-ceramic.
The preparation of modified meerschaum particle:2g poloxamers and 0.1g nanometer titanium dioxides are added into 15g sepiolite powders, is filled
Divide and microwave frequency 2450MHz, power output 700W microwave treater microwave treatment 5min are utilized after mixing, stand after 30min
Continue microwave treatment 5min, add 0.5g hydrogenated rosin glycerides and 0.3g rilanit specials, microwave again after being well mixed
5min is handled, graininess most is made through ball mill afterwards, modified meerschaum particle is produced.
Embodiment 3
Respectively to equivalent embodiment 1 and the made water conservation inorganic agent of embodiment 2, the made chitosan oligosaccharide-ceramic of embodiment 2 and
Modified meerschaum particle carries out water absorbing properties test, as a result as shown in table 1.
The water absorbing properties test result of table 1
Project | Water absorbent rate ml/g |
The water conservation inorganic agent of embodiment 1 | 291.3 |
The water conservation inorganic agent of embodiment 2 | 302.6 |
2 chitosan oligosaccharides of embodiment-ceramic | 168.2 |
The modified meerschaum particle of embodiment 2 | 126.4 |
Chitosan oligosaccharide | 39.5 |
Ceramic | 15.8 |
Sepiolite powder | 13.2 |
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (5)
1. a kind of wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus, it is characterised in that be made up of the raw material of following parts by weight:
Atlapulgite -15-20 parts of polyvinyl alcohol, 5-10 parts of water soluble chitosan, chitosan oligosaccharide -3-5 parts of ceramic, carbomer
1-2 parts, 1-2 parts of pre-gelatinized potato starch, 0.5-1 parts of modified meerschaum particle, 0.5-1 parts of polyethylene glycol oxide, plant ash 0.3-
0.5 part, 0.3-0.5 parts of polydextrose, 0.05-0.1 parts of poly-D-lysine;
Its preparation method comprises the following steps:
(1) carbomer and polyethylene glycol oxide are added into atlapulgite-polyvinyl alcohol, and with 5 DEG C/min programming rate liter
Temperature adds modified meerschaum particle and plant ash, continuation is ground in 115-120 DEG C of insulation to 115-120 DEG C of insulation grinding 15min
10min is ground, powder I is produced;
(2) pre-gelatinized potato starch and polydextrose are added into chitosan oligosaccharide-ceramic, and with 5 DEG C/min programming rate
110-115 DEG C of insulation grinding 15min is warming up to, powder II is produced;
(3) powder II, water soluble chitosan and poly-D-lysine are added into powder I, is placed in after being sufficiently mixed in 0-5 DEG C of environment
Sealing and standing 2h, and 105-110 DEG C of insulation grinding 10min is warming up to 5 DEG C/min programming rate, produce water conservation inorganic agent;
Atlapulgite-the polyvinyl alcohol is to compare 10 by weight:1:0.05 atlapulgite, cold soluble type polyvinyl alcohol and N- hydroxyl second
Base acrylamide is warming up to obtained after 120-125 DEG C of insulation grinding 30min.
2. the wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus according to claim 1, it is characterised in that the shell is few
Sugar-ceramic is made up of the raw material of following parts by weight:10-15 parts of chitosan oligosaccharide, 3-5 parts of ceramic, hydroxy ethyl fiber
Plain 1-2 parts, 0.5-1 parts of PVPP, 0.1-0.3 parts of poly-aspartate, 0.05-0.1 parts of HPMA, water 50-
80 parts, its preparation method is:PVPP and poly-aspartate are added into chitosan oligosaccharide, 115-120 DEG C is warming up under grinding
Insulation grinding 15min, adds ceramic, hydroxyethyl cellulose and HPMA, continues in 115-120 DEG C of insulation
15min is ground, sealing and standing 1h in 0-5 DEG C of environment is then transferred to, and adds 50-55 DEG C of water, is sufficiently mixed after 50-55 DEG C of guarantor
Temperature is stood in 30min, gained mixed liquor feeding spray dryer, dries gained particle and micro mist is made through micronizer, be
Chitosan oligosaccharide-ceramic.
3. the wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus according to claim 1, it is characterised in that:The modified sea
Afrodite particle is made by sepiolite powder is modified, and its specific method of modifying is:Poloxamer is added into sepiolite powder and is received
Rice titanium dioxide, utilizes microwave treater microwave treatment 5min after being sufficiently mixed, stand and continue microwave treatment 5min after 30min, then
Hydrogenated rosin glyceride and rilanit special are added, microwave treatment 5min again after being well mixed most is made through ball mill afterwards
It is granular, produce modified meerschaum particle.
4. the wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus according to claim 3, it is characterised in that:The sepiolite
Powder, poloxamer, nanometer titanium dioxide, the weight ratio of hydrogenated rosin glyceride and rilanit special are 10-15:1-2:0.05-
0.1:0.3-0.5:0.1-0.3。
5. the wooden water conservation inorganic agent of the segment wood cultivated use section of black fungus according to claim 3, it is characterised in that:At the microwave
The condition of work for managing device is microwave frequency 2450MHz, power output 700W.
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Patent Citations (7)
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CN101693812A (en) * | 2009-09-24 | 2010-04-14 | 无锡信达胶脂材料有限公司 | Process for preparing water-retaining agent used for edible mushroom cultivation fungus sticks |
CN101768397A (en) * | 2010-02-05 | 2010-07-07 | 无锡信达胶脂材料有限公司 | Heat preservation and water-retaining agent for flower mushroom culture and preparation method thereof |
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