CN107118625A - Mould the preparation method of rattan article antioxidant coating - Google Patents
Mould the preparation method of rattan article antioxidant coating Download PDFInfo
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- CN107118625A CN107118625A CN201710325547.2A CN201710325547A CN107118625A CN 107118625 A CN107118625 A CN 107118625A CN 201710325547 A CN201710325547 A CN 201710325547A CN 107118625 A CN107118625 A CN 107118625A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D103/00—Coating compositions based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09D103/02—Starch; Degradation products thereof, e.g. dextrin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/0427—Coating with only one layer of a composition containing a polymer binder
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2303/00—Characterised by the use of starch, amylose or amylopectin or of their derivatives or degradation products
- C08J2303/02—Starch; Degradation products thereof, e.g. dextrin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Engineering & Computer Science (AREA)
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- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
- Anti-Oxidant Or Stabilizer Compositions (AREA)
Abstract
The present invention provides a kind of preparation method for moulding rattan article antioxidant coating, specifically includes following steps：By each raw material grind is into 50 100 mesh traditional Chinese medicine fine powders and sends into freezing in 5 DEG C of freezers；Material is boiled and melted, progress vulcanizing treatment in vulcanizing tank is then fed into and obtains material one；It is placed in agitator tank and stirs after each raw material is mixed, mixing speed is 3000r/mim, whipping temp is 60 70 DEG C, obtains material two；Tannin acid, guar gum ether, lauric monoglyceride, ethanol mixing are taken, material two is added into solution and is warming up to 53 55 DEG C and keeps the temperature 10 minutes, material three is obtained；Material three is added into activated yeast and material four is obtained within one week in fermentation process in anaerobic environment；Its pH value is set to be 7.1 7.2 with sodium hydroxide titration material four.Coating of the present invention is directly applied on modeling rattan, nontoxic free from extraneous odour, and coating damage resistant, and the peeling that do not ftracture under high temperature and low temperature, and the absorbability to ultraviolet is weak, greatly protects modeling rattan.
Description
Technical field
The present invention relates to technical field of coatings, and in particular to a kind of preparation method of modeling rattan article antioxidant coating.
Background technology
Rattan plaited typically by beat rattan (pruning the knot on rattan), pick rattan, wash rattan, shine rattan, stubborn rattan, draw rattan (digging rattan), cut rattan,
More than ten procedures such as bleach, dye, weaving, painting.Rattan plaited is main using rattan branch, rattan core or bamboo as skeleton, then with rattan peel or
Tender rattan core braiding is formed, the characteristics of giving full play to rattan softness, be not easily broken.
On color, mostly using the light yellow of former rattan, or processing, bleaching are white, ivory white, it appears soft elegance,
Some are then equipped with coffee color, brown etc..Rattan furniture is using thick rattan as skeleton, through following closely frame, then with rattan peel, the braiding of rattan core
Into finally painting or paint.
Rattan-weaved products is increasingly liked because of its elegant, simple outward appearance by masses.It is to utilize plastic extrusion to mould rattan
The plastic products for the similar Rattan-shaped being made.Due to natural rattan plaited material, supply falls short of demand, so many products are using modeling now
The rattan imitating of rattan etc carries out being compiled into rattan woven ware imitation product to meet the market demand.In order to ensure the service life for moulding rattan article,
So coating can be used to smear modeling rattan.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of preparation method for moulding rattan article antioxidant coating.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of preparation method for moulding rattan article antioxidant coating, specifically includes following steps：
A. white 6-8 parts 10-20 parts of greater celandine, 10-16 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 6-10 parts of sweet wormwood, tangerine, 3.5-4.5 parts of bitter dish, west are taken
2-6 parts of safflower, 2-6 parts of rhizoma menispermi, by each raw material grind into 50-100 mesh traditional Chinese medicine fine powders, traditional Chinese medicine fine powder is mixed thoroughly simultaneously with glutinous paste
Freezing one week in -5 DEG C of freezers of feeding；
B. the material after above-mentioned freezing is boiled and melted, be then fed into vulcanizing tank and carry out vulcanizing treatment 1 hour, vulcanizing treatment
Terminate to obtain material one；
C. 1-2 parts of 3,4- dimethoxy cinnamic acids, 1-2 parts of linalool, 6-8 parts of Pyrolin, oleanonic acid 2-4 are taken
Part, 1-1.5 parts of isoquercitrin, 1-1.5 parts of dichloro coumarone, β -1-1.5 parts of gurjunene, 120-160 parts of purified water, by each raw material
It is placed in agitator tank and stirs after mixing, mixing speed is 3000r/mim, whipping temp is 60-70 DEG C, obtains material two；
D. 3.2-3.4 parts of tannin acid, 3.2-3.4 parts of guar gum ether, 0.1-0.3 parts of lauric monoglyceride, ethanol 50- are taken
60 parts of mixing, are heated to 50 DEG C, keep 50 DEG C of temperature 20 minutes, and material two is then added into solution and 53-55 DEG C is warming up to
And keep the temperature 10 minutes, 1-3 parts of chitosan is then added into mixed liquor, then with 240-260nm ultraviolet irradiation 3
Minute, obtain material three；
E. material three is added into activated yeast and is in fermentation process one week in anaerobic environment, then taken out product and will produce
Thing is heated to 40-50 DEG C, while adding 3-5 parts of Tea Polyphenols into product, obtains material four；
F. make its pH value be 7.1-7.2 with sodium hydroxide titration material four, material one is then added into material four, is connect
Makes its pH value be 6.85-6.95 with marine alga acidometric titration, then filters, and obtains filtrate, filtrate is coating.
Raw material in the traditional Chinese medicine fine powder is：15 parts of greater celandine, 13 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 8 parts of sweet wormwood, white 7 parts of tangerine, 4 parts of bitter dish,
4 parts of west safflower, 4 parts of rhizoma menispermi.
Freezing is divided into two stages in step a, freezed 3 days before this, and then heated to 30-35 DEG C, then freeze again four days.
Added in step d after standing one day after chitosan and add 0.5-1 parts of Rhizoma Gastrodiae powders, 0.5-1 parts of chlorinations to mixed liquor again
Sodium, 1-2 part tetrahydrofuran, 1-2 parts of andrographolides.
Added in step d after Rhizoma Gastrodiae powder, sodium chloride, tetrahydrofuran, andrographolide stand one day and mixed liquor is put into sun
Exposure 3-5 days under light.
The beneficial effects of the invention are as follows：This coating is directly applied on modeling rattan, nontoxic free from extraneous odour, and coating is scratch-resistant
Wound, and the peeling that do not ftracture under high temperature and low temperature, the absorbability to ultraviolet are weak, greatly protect modeling rattan.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
A kind of preparation method for moulding rattan article antioxidant coating, specifically includes following steps：
A. 15 parts of greater celandine, 13 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 8 parts of sweet wormwood, white 7 parts of tangerine, 4 parts of bitter dish, 4 parts of west safflower, rhizoma menispermi 4 are taken
Part, by each raw material grind into 50-100 mesh traditional Chinese medicine fine powders, traditional Chinese medicine fine powder is mixed thoroughly with glutinous paste and freezing in -5 DEG C of freezers is sent into
One week；
B. the material after above-mentioned freezing is boiled and melted, be then fed into vulcanizing tank and carry out vulcanizing treatment 1 hour, vulcanizing treatment
Terminate to obtain material one；
C. take 1.5 parts of 3,4- dimethoxys cinnamic acid, it is 1.5 parts of linalool, 7 parts of Pyrolin, 3 parts of oleanonic acid, different
1.2 parts of quercitin, 1.2 parts of dichloro coumarone, 1.2 parts of β-gurjunene, 120-160 parts of purified water, are placed in after each raw material is mixed
Stirred in agitator tank, mixing speed is 3000r/mim, whipping temp is 60-70 DEG C, obtains material two；
D. 3.3 parts of tannin acid, 3.3 parts of guar gum ether, 0.2 part of lauric monoglyceride, 55 parts of mixing of ethanol are taken, are heated to
50 DEG C, then 50 DEG C of holding temperature 20 minutes adds material two into solution and is warming up to 53-55 DEG C and keeps 10 points of the temperature
Clock, then adds 2 parts of chitosan into mixed liquor, is then irradiated 3 minutes with 240-260nm ultraviolet, obtains material three；
E. material three is added into activated yeast and is in fermentation process one week in anaerobic environment, then taken out product and will produce
Thing is heated to 40-50 DEG C, while adding 4 parts of Tea Polyphenols into product, obtains material four；
F. make its pH value be 7.1-7.2 with sodium hydroxide titration material four, material one is then added into material four, is connect
Makes its pH value be 6.85-6.95 with marine alga acidometric titration, then filters, and obtains filtrate, filtrate is coating.
Freezing is divided into two stages in step a, freezed 3 days before this, and then heated to 30-35 DEG C, then freeze again four days.
Added in step d after standing one day after chitosan again to mixed liquor add 0.8 part of Rhizoma Gastrodiae powder, 0.8 part of sodium chloride,
1.5 parts of tetrahydrofurans, 1.5 parts of andrographolides.
Added in step d after Rhizoma Gastrodiae powder, sodium chloride, tetrahydrofuran, andrographolide stand one day and mixed liquor is put into sun
Exposure 3-5 days under light.
Embodiment 2
A kind of preparation method for moulding rattan article antioxidant coating, specifically includes following steps：
A. 10 parts of greater celandine, 10 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 6 parts of sweet wormwood, white 6 parts of tangerine, 3.5 parts of bitter dish, 2 parts of west safflower, rhizoma menispermi 2 are taken
Part, by each raw material grind into 50-100 mesh traditional Chinese medicine fine powders, traditional Chinese medicine fine powder is mixed thoroughly with glutinous paste and freezing in -5 DEG C of freezers is sent into
One week；
B. the material after above-mentioned freezing is boiled and melted, be then fed into vulcanizing tank and carry out vulcanizing treatment 1 hour, vulcanizing treatment
Terminate to obtain material one；
C. 1 part of 3,4- dimethoxys cinnamic acid, 1 part of linalool, 6 parts of Pyrolin, 2 parts of oleanonic acid, isoquercitrin are taken
1 part of glycosides, 1 part of dichloro coumarone, 1 part of β-gurjunene, 120 parts of purified water, are placed in agitator tank after each raw material is mixed and stir, stir
Speed is mixed for 3000r/mim, whipping temp is 60-70 DEG C, obtains material two；
D. 3.2 parts of tannin acid, 3.2 parts of guar gum ether, 0.1 part of lauric monoglyceride, 50 parts of mixing of ethanol are taken, are heated to
50 DEG C, then 50 DEG C of holding temperature 20 minutes adds material two into solution and is warming up to 53-55 DEG C and keeps 10 points of the temperature
Clock, then adds 1 part of chitosan into mixed liquor, is then irradiated 3 minutes with 240-260nm ultraviolet, obtains material three；
E. material three is added into activated yeast and is in fermentation process one week in anaerobic environment, then taken out product and will produce
Thing is heated to 40-50 DEG C, while adding 3 parts of Tea Polyphenols into product, obtains material four；
F. make its pH value be 7.1-7.2 with sodium hydroxide titration material four, material one is then added into material four, is connect
Makes its pH value be 6.85-6.95 with marine alga acidometric titration, then filters, and obtains filtrate, filtrate is coating.
Freezing is divided into two stages in step a, freezed 3 days before this, and then heated to 30-35 DEG C, then freeze again four days.
Added in step d after standing one day after chitosan and add 0.5 part of Rhizoma Gastrodiae powder, 0.5 part of sodium chloride, 1 to mixed liquor again
Part tetrahydrofuran, 1 part of andrographolide.
Added in step d after Rhizoma Gastrodiae powder, sodium chloride, tetrahydrofuran, andrographolide stand one day and mixed liquor is put into sun
Exposure 3-5 days under light.
Embodiment 3
A kind of preparation method for moulding rattan article antioxidant coating, specifically includes following steps：
A. 20 parts of greater celandine, 16 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 10 parts of sweet wormwood, white 8 parts of tangerine, 4.5 parts of bitter dish, 6 parts of west safflower, rhizoma menispermi are taken
6 parts, by each raw material grind into 100 mesh traditional Chinese medicine fine powders, traditional Chinese medicine fine powder is mixed thoroughly with glutinous paste and sent into -5 DEG C of freezers freeze one
Week；
B. the material after above-mentioned freezing is boiled and melted, be then fed into vulcanizing tank and carry out vulcanizing treatment 1 hour, vulcanizing treatment
Terminate to obtain material one；
C. 2 parts of 3,4- dimethoxys cinnamic acid, 2 parts of linalool, 8 parts of Pyrolin, 4 parts of oleanonic acid, isoquercitrin are taken
1.5 parts of glycosides, 1.5 parts of dichloro coumarone, 1.5 parts of β-gurjunene, 160 parts of purified water, are placed in agitator tank after each raw material is mixed
Stirring, mixing speed is 3000r/mim, and whipping temp is 60-70 DEG C, obtains material two；
D. 3.4 parts of tannin acid, 3.4 parts of guar gum ether, 0.3 part of lauric monoglyceride, 60 parts of mixing of ethanol are taken, are heated to
50 DEG C, then 50 DEG C of holding temperature 20 minutes adds material two into solution and is warming up to 53-55 DEG C and keeps 10 points of the temperature
Clock, then adds 3 parts of chitosan into mixed liquor, is then irradiated 3 minutes with 240-260nm ultraviolet, obtains material three；
E. material three is added into activated yeast and is in fermentation process one week in anaerobic environment, then taken out product and will produce
Thing is heated to 40-50 DEG C, while adding 5 parts of Tea Polyphenols into product, obtains material four；
F. make its pH value be 7.1-7.2 with sodium hydroxide titration material four, material one is then added into material four, is connect
Makes its pH value be 6.85-6.95 with marine alga acidometric titration, then filters, and obtains filtrate, filtrate is coating.
Freezing is divided into two stages in step a, freezed 3 days before this, and then heated to 30-35 DEG C, then freeze again four days.
Added in step d after standing one day after chitosan again to mixed liquor add 1 part of Rhizoma Gastrodiae powder, 1 part of sodium chloride, 2 part four
Hydrogen furans, 2 parts of andrographolides.
Added in step d after Rhizoma Gastrodiae powder, sodium chloride, tetrahydrofuran, andrographolide stand one day and mixed liquor is put into sun
Exposure 3-5 days under light.
Experiment
Coating made from embodiment 1,2,3 is tested, result of the test is as follows：
Experiment is proved：This antioxidant coating volatility is extremely low, and is resistant to ultraviolet radiation, is fitted under high temperature and low temperature
Answering property is good, do not ftracture, and substantially increases service life.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (5)
1. a kind of preparation method for moulding rattan article antioxidant coating, it is characterised in that specifically include following steps：
A. white 6-8 parts 10-20 parts of greater celandine, 10-16 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 6-10 parts of sweet wormwood, tangerine, 3.5-4.5 parts of bitter dish, west safflower are taken
2-6 parts, 2-6 parts of rhizoma menispermi, traditional Chinese medicine fine powder by each raw material grind into 50-100 mesh traditional Chinese medicine fine powders, mixed thoroughly and sent with glutinous paste
Enter freezing one week in -5 DEG C of freezers；
B. the material after above-mentioned freezing is boiled and melted, be then fed into vulcanizing tank and carry out vulcanizing treatment 1 hour, vulcanizing treatment terminates
Obtain material one；
C. 1-2 parts of 3,4- dimethoxy cinnamic acids are taken, it is 1-2 parts of linalool, 6-8 parts of Pyrolin, 2-4 parts of oleanonic acid, different
1-1.5 parts of quercitin, 1-1.5 parts of dichloro coumarone, β -1-1.5 parts of gurjunene, 120-160 parts of purified water, each raw material is mixed
After be placed in agitator tank and stir, mixing speed is 3000r/mim, and whipping temp is 60-70 DEG C, obtains material two；
D. 3.2-3.4 parts of tannin acid, 3.2-3.4 parts of guar gum ether, 0.1-0.3 parts of lauric monoglyceride, 50-60 parts of ethanol are taken
Mixing, is heated to 50 DEG C, then 50 DEG C of holding temperature 20 minutes adds material two into solution and be warming up to 53-55 DEG C and protect
Hold the temperature 10 minutes, 1-3 parts of chitosan is then added into mixed liquor, then irradiate 3 points with 240-260nm ultraviolet
Clock, obtains material three；
E. material three is added into activated yeast and is in fermentation process one week in anaerobic environment, then taken out product and add product
Heat, while adding 3-5 parts of Tea Polyphenols into product, obtains material four to 40-50 DEG C；
F. make its pH value be 7.1-7.2 with sodium hydroxide titration material four, material one is then added into material four, is then used
Marine alga acidometric titration makes its pH value be 6.85-6.95, then filters, and obtains filtrate, filtrate is coating.
2. the preparation method of modeling rattan article antioxidant coating according to claim 1, it is characterised in that the traditional Chinese medicine fine powder
In raw material be：15 parts of greater celandine, 13 parts of CAULIS SCHEFFLERAE KWANGSIENSIS, 8 parts of sweet wormwood, white 7 parts of tangerine, 4 parts of bitter dish, 4 parts of west safflower, 4 parts of rhizoma menispermi.
3. the preparation method of modeling rattan article antioxidant coating according to claim 1, it is characterised in that freezed in step a
It is divided into two stages, freezed 3 days before this, and then heated to 30-35 DEG C, then freeze again four days.
4. the preparation method of modeling rattan article antioxidant coating according to claim 1, it is characterised in that added in step d
0.5-1 parts of Rhizoma Gastrodiae powders, 0.5-1 parts of sodium chloride, 1-2 parts of tetrahydrofurans, 1-2 are added after standing one day after chitosan to mixed liquor again
Part andrographolide.
5. the preparation method of modeling rattan article antioxidant coating according to claim 4, it is characterised in that added in step d
Mixed liquor is put into exposure 3-5 days under sunlight by Rhizoma Gastrodiae powder, sodium chloride, tetrahydrofuran, andrographolide after standing one day.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710325547.2A CN107118625A (en) | 2017-05-10 | 2017-05-10 | Mould the preparation method of rattan article antioxidant coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710325547.2A CN107118625A (en) | 2017-05-10 | 2017-05-10 | Mould the preparation method of rattan article antioxidant coating |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102824533A (en) * | 2012-09-29 | 2012-12-19 | 刘永平 | Antioxidant traditional Chinese medicine composition and preparation method thereof |
| CN106217556A (en) * | 2016-07-21 | 2016-12-14 | 阜南县宏泰工艺品有限公司 | Low temperature resistant, the damp-proof treatment agent of a kind of wicker plaiting article rattan |
| CN106366925A (en) * | 2016-08-29 | 2017-02-01 | 安徽阜南县向发工艺品有限公司 | Water-tolerant paint preparation method for surfaces of flower baskets woven by plastic rattans |
| CN106366924A (en) * | 2016-08-29 | 2017-02-01 | 安徽阜南县向发工艺品有限公司 | Water-tolerant coating preparation method for surfaces of plastic rattans used on plastic rattan chairs |
-
2017
- 2017-05-10 CN CN201710325547.2A patent/CN107118625A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102824533A (en) * | 2012-09-29 | 2012-12-19 | 刘永平 | Antioxidant traditional Chinese medicine composition and preparation method thereof |
| CN106217556A (en) * | 2016-07-21 | 2016-12-14 | 阜南县宏泰工艺品有限公司 | Low temperature resistant, the damp-proof treatment agent of a kind of wicker plaiting article rattan |
| CN106366925A (en) * | 2016-08-29 | 2017-02-01 | 安徽阜南县向发工艺品有限公司 | Water-tolerant paint preparation method for surfaces of flower baskets woven by plastic rattans |
| CN106366924A (en) * | 2016-08-29 | 2017-02-01 | 安徽阜南县向发工艺品有限公司 | Water-tolerant coating preparation method for surfaces of plastic rattans used on plastic rattan chairs |
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Application publication date: 20170901 |