CN107099439B - White-spirit purifying equipment and wine liquid impurity-removing method - Google Patents
White-spirit purifying equipment and wine liquid impurity-removing method Download PDFInfo
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- CN107099439B CN107099439B CN201710319722.7A CN201710319722A CN107099439B CN 107099439 B CN107099439 B CN 107099439B CN 201710319722 A CN201710319722 A CN 201710319722A CN 107099439 B CN107099439 B CN 107099439B
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- wine
- white
- impurity
- white wine
- wine liquid
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/12—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages without precipitation
- C12H1/16—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages without precipitation by physical means, e.g. irradiation
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/06—Precipitation by physical means, e.g. by irradiation, vibrations
- C12H1/063—Separation by filtration
Abstract
The present invention provides white-spirit purifying equipment and wine liquid impurity-removing method, is related to the technical field of liquor production technology, including equipment body, stirring system, cleaning system and filtration system;The cleaning system includes variable-voltage power supply group and electrolysis electrode;The electrolysis electrode is located in the cavity volume of the equipment body;The stirring system includes stirring motor and agitating paddle, and the agitating paddle is located in the equipment body, and the stirring motor is connected with the variable-voltage power supply group.White-spirit purifying equipment provided by the invention and wine liquid impurity-removing method can clean to the impurity of the white wine in equipment body, and stirring system makes the high impurity volatilization device for transferring main body of the volatility in white wine, not volatile higher boiling grease type impurity in white wine, in alkaline environment, produce good fortune reaction, formed after non-solubility is fixed and produce flocculation and separate out, removed after filtration system, so reach the purpose of impurity in purified spirit.
Description
Technical field
The present invention relates to liquor production technical field, more particularly, to a kind of white-spirit purifying equipment and wine liquid impurity-removing method.
Background technology
The standard of white wine defines:Using Cereals as primary raw material, with Daqu, Chinese yeast or wheat bran and distiller's yeast etc. for diastatic fermentation
Agent, through boiling, saccharification, fermentation, distillation and manufactured Spirit.Also known as liquor, white spirit, aquavit etc..
Vinosity colourless (or micro- Huang) is transparent, and fragrant odour is pure, and entrance is sweet refreshing net, and alcohol content is higher, old through storing
After ripe, there is the compound fragrant based on esters.Using bent class, distiller's yeast as saccharifying ferment, using starchiness (saccharic) raw material,
Through boiling, saccharification, fermentation, distillation, ageing and all kinds of wine blent and brewed.
And said on stricti jurise, it is white wine that the assembled alcoholic drinks blent by edible alcohol and flavorant, which can not be then considered,
And it should be referred to as to contain spirituous beverage.
Traditional liquor is predominantly adsorbed, so for the physical filtering of impurity in wine by adding filter aid into wine
Diatomaceous earth filter, active carbon filter or millipore filter are utilized afterwards, are filtered.Its shortcoming is miscellaneous in white wine after filtering
Matter remnants are more, and degree control is more difficult, easily filter other fragrance matters, cause liquor flavor boring.Particularly to fusel oil
The higher tail wine processing of content is more difficult.
The cooling freezing and filtering impurity removal method cost used now is higher;It is larger to distill impurity elimination method operating procedure difficulty, effect
More difficult control;Natural storage cleans, cycle length, and cost is high.
The content of the invention
It is an object of the invention to provide white-spirit purifying equipment and wine liquid impurity-removing method, to alleviate the various removal of impurities of present white wine
Technology is undesirable, easily removes the fragrance matter either technical problem of cost height or cycle length.
A kind of white-spirit purifying equipment provided by the invention, including equipment body, stirring system, cleaning system and filtering system
System;
The cleaning system includes variable-voltage power supply group and electrolysis electrode;The electrolysis electrode is located at the appearance of the equipment body
Intracavitary;
The stirring system includes stirring motor and agitating paddle, and the agitating paddle is located in the equipment body, described to stir
Motor is mixed with the variable-voltage power supply group to be connected;
The equipment body upper end is provided with charging aperture, and lower end is provided with discharging opening;The discharging opening and the first drainage conduit
It is connected, and the discharge outlet is provided with valve;
The filtration system includes supercharging device and filter, and the supercharging device is arranged on the discharging opening and the mistake
Between filter;And the filtration system is arranged in first drainage conduit;
Sample tap is provided with the equipment body, and the sample tap is located at the equipment body bottom.
And the PH monitors and institute further, in addition to the PH monitors for white wine PH in monitoring device main body,
State the connection of variable-voltage power supply group.
Further, the PH monitors include monitor main body and combination electrode, and the combination electrode is set positioned at described
In standby main body.
Further, it is provided with the equipment body for the pressure gauge of pressure in monitoring device main body, for controlling
The relief valve of pressure and for ensureing safety valve of the equipment body air pressure in safe range in equipment body.
Further, in addition to device for monitoring temperature, the device for monitoring temperature and it is arranged in the equipment body
Sensor is connected, and the device for monitoring temperature is connected with the variable-voltage power supply group.
White-spirit purifying equipment provided by the invention can clean to the impurity of the white wine in equipment body, and stir system
System makes the high impurity volatilization device for transferring main body of the volatility in white wine, and the not volatile higher boiling grease type in white wine is miscellaneous
Matter, in alkaline environment, good fortune reaction is produced, is formed after non-solubility is fixed and produces flocculation and separate out, after filtration system
Remove, so reach the purpose of impurity in purified spirit.
The present invention also provides a kind of wine liquid impurity-removing method, comprises the following steps:
(a) wine liquid is added in equipment body to be well mixed with processing aid and be electrolysed, while open stirring system;
(b) white wine pH is detected, when pH it is stable more than 8 after, wine liquid is filtered, isolate processing aid and
Impurity, complete the removal of impurities of wine liquid.
Further, in step (a), the temperature for being electrolysed wine liquid is less than 40 DEG C.
Further, in step (a), the pressure for being electrolysed wine liquid is less than 0.2mPa.
Further, in step (a), the rotating speed of stirring system is in 36r/min-90r/min.
Further, in step (b), determine that pH is stable more than 8, comprise the following steps:
(s) in wine liquid electrolytic process, it is monitored by PH monitors, when pH is more than 8.5, stands wine liquid 10-24
Hour, detection wine liquid pH;
(m) when wine liquid pH is less than 8, repeat the above steps.
Wine liquid impurity-removing method provided by the invention, by increasing processing aid in wine liquid, is electrolysed, then to wine liquid
By filter by processing aid and contaminant filter, so as to complete the requirement to wine liquid removal of impurities, compared with conventional method, more
It is effectively quick, the quality of drinks can be lifted, mouthfeel is drunk in improvement, shortens the production cycle, reduces production cost.
Brief description of the drawings
, below will be to specific in order to illustrate more clearly of the specific embodiment of the invention or technical scheme of the prior art
The required accompanying drawing used is briefly described in embodiment or description of the prior art, it should be apparent that, in describing below
Accompanying drawing is some embodiments of the present invention, for those of ordinary skill in the art, before creative work is not paid
Put, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the structural representation of white-spirit purifying equipment provided in an embodiment of the present invention;
Fig. 2 is the partial schematic diagram of the A of white-spirit purifying equipment shown in Fig. 1;
Fig. 3 is the partial schematic diagram of the B of white-spirit purifying equipment shown in Fig. 1;
Fig. 4 is the structural representation of another white-spirit purifying equipment provided in an embodiment of the present invention.
Icon:100- equipment bodies;200- cavity volumes;300- charging apertures;400- discharging openings;The drainage conduits of 500- first;
600- supercharging devices;700- filters;800- monitor main bodys;900- combination electrodes;110- variable-voltage power supply groups;120-
Electrolysis electrode;130- stirring motors;140- agitating paddles;150- pressure gauges;160- relief valves;170- safety valves;180-
Sample tap;190- sensors;210- device for monitoring temperature.
Embodiment
Technical scheme is clearly and completely described below in conjunction with accompanying drawing, it is clear that described implementation
Example is part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, ordinary skill
The every other embodiment that personnel are obtained under the premise of creative work is not made, belongs to the scope of protection of the invention.
In the description of the invention, it is necessary to explanation, such as occur term " " center ", " on ", " under ", "left", "right",
" vertical ", " level ", " interior ", " outer " etc., its orientation indicated or position relationship are to be closed based on orientation shown in the drawings or position
System, it is for only for ease of and describes the present invention and simplify description, rather than indicates or imply that signified device or element must have
Specific orientation, with specific azimuth configuration and operation, therefore be not considered as limiting the invention.In addition, such as there is art
Language " first ", " second ", " the 3rd " are only used for describing purpose, and it is not intended that instruction or hint relative importance.
In the description of the invention, it is necessary to illustrate, unless otherwise clearly defined and limited, term " installation ", " phase
Even ", " connection " should be interpreted broadly, for example, it may be being fixedly connected or being detachably connected, or be integrally connected;Can
To be mechanical connection or electrical connection;Can be joined directly together, can also be indirectly connected by intermediary, Ke Yishi
The connection of two element internals.For the ordinary skill in the art, with concrete condition above-mentioned term can be understood at this
Concrete meaning in invention.
As shown in Figure 1, Figure 2 and Figure 3, a kind of white-spirit purifying equipment provided by the invention, including equipment body 100, stirring
System, cleaning system and filtration system;
The cleaning system includes variable-voltage power supply group 110 and electrolysis electrode 120;The electrolysis electrode 120 is set positioned at described
In the cavity volume 200 of standby main body 100;
The stirring system includes stirring motor 130 and agitating paddle 140, and the agitating paddle 140 is located at the equipment body
In 100, the stirring motor 130 is connected with the variable-voltage power supply group 110;
The upper end of equipment body 100 is provided with charging aperture 300, and lower end is provided with discharging opening 400;The discharging opening 400
It is connected with the first drainage conduit 500, and valve is provided with the discharging opening 400;
The filtration system includes supercharging device 600 and filter 700, and the supercharging device 600 is arranged on the discharging
Between mouth 400 and the filter 700;And the filtration system is arranged in first drainage conduit 500;
Sample tap 180 is provided with the equipment body 100, and the sample tap 180 is located under the equipment body 100
Portion.
In certain embodiments, there is stirring system on equipment body 100, during white wine cleans, white wine is carried out
Stirring, variable-voltage power supply group 110 are electrolysed by electrolysis electrode 120 to white wine, can be easy by some in white wine to white wine motor
Decompose impurity and gas is produced in electrolytic process, with the progress of electrolysis, white wine gradually forms alkaline environment, produces certain soap
Change reaction, produce flocculation after forming non-solubility solid and separate out.
Charging aperture 300 on equipment body 100, for white wine to be cleaned to be poured into equipment body 100;Discharging opening
400 after the lower end of equipment body 100, white wine electrolysis removal of impurities, and white wine flows into the first drainage conduit 500, filtered system filtering
After, impurity is isolated, just obtains satisfactory white wine.
In electrolytic process, by being sampled in sample tap 180, detected, whether the impurity seen in white wine is electrolysed removing,
Determine whether to complete impurity electrolysis in white wine with final, prevent that the white wine after filtering is undesirable.
On above-described embodiment basis, further, in addition to the pH prisons for white wine pH in monitoring device main body 100
Instrument is surveyed, and the PH monitors are connected with the variable-voltage power supply group 110.
PH monitors monitor the pH of white wine in real time, when the PH of white wine gradually rises, the rotating speed of the agitating paddle 140 of stirring system
Also constantly increase, so that the white spirit mixed in equipment body 100 is uniform, PH monitors can accurately read PH.
Controller, controller control stirring system and purifier are provided with variable-voltage power supply group 110, pH monitors will be examined
To controller, controller according to pre-seting stirring system and purifier is adjusted the PH data transfers measured.
On above-described embodiment basis, further, the pH monitors include monitor main body 800 and combination electrode
900, the combination electrode 900 is located in the equipment body 100.
The combination electrode 900 of pH monitors monitors the change of white wine, monitor main body 800 in real time in equipment body 100
Send the PH of white wine data to controller, controller carries out follow-up control.
On above-described embodiment basis, further, it is provided with the equipment body 100 for monitoring device main body
The pressure gauge 150 of pressure, the relief valve 160 for pressure in control device main body 100 and for ensureing equipment body in 100
Safety valve 170 of 100 air pressure in safe range.
In certain embodiments, there are pressure gauge 150, relief valve 160 and safety valve 170 on equipment body 100, pass through pressure
Table 150 is capable of the size of the intuitively pressure in facilities for observation main body 100, and relief valve 160 typically sets the maximum that white wine is electrolysed
Pressure, when the Inner electrolysis of equipment body 100 produces gas, pressure constantly increases in equipment body 100, when more than relief valve 160
Setting pressure when, relief valve 160 by equipment body 100 gas discharge, while also discharged electrolysis white wine production
Volatile impurity in raw gas and white wine.
The pressure of the setting of safety valve 170 is more than the pressure of relief valve 160, when relief valve 160 breaks down, it is impossible to pressure release
In the case of, safety valve 170 sheds pressure;So ensure that pressure will not be too high in equipment body 100, and ensure equipment body
Pressure in 100 can be shed, and ensure the safety of equipment body 100, accident will not occur.
As shown in figure 4, in order to preferably control the temperature of white wine, on above-described embodiment basis, further, also wrap
Include device for monitoring temperature 210, the device for monitoring temperature 210 and the phase of sensor 190 being arranged in the equipment body 100
Even, and the device for monitoring temperature 210 is connected with the variable-voltage power supply group 110.
In certain embodiments, sensor 190 is arranged in equipment body 100, and device for monitoring temperature 210 is by sensor
190 data transfer to variable-voltage power supply group 110, variable-voltage power supply group 110 controller according to preset value, control variable-voltage power supply group
110 power being electrolysed, temperature rise, the power of electrolysis electrode 120 reduces, when temperature is more than 40 DEG C, stopping pair
The electrolysis of white wine;The monitoring to white wine in real time of device for monitoring temperature 210, makes white wine be electrolysed below 40 DEG C.
White-spirit purifying equipment provided by the invention can clean to the impurity of the white wine in equipment body 100, and stir
The system of mixing makes the high impurity volatilization device for transferring main body 100 of the volatility in white wine, the not volatile higher boiling oil in white wine
Lipid impurities, in alkaline environment, good fortune reaction is produced, is formed after non-solubility is fixed and produces flocculation and separate out, by filtering
Removed after system, so reach the purpose of impurity in purified spirit.
The present invention also provides a kind of wine liquid impurity-removing method, comprises the following steps:
(a) wine liquid is added in equipment body to be well mixed with processing aid and be electrolysed, while open stirring system;
(b) white wine pH is detected, when pH it is stable more than 8 after, wine liquid is filtered, isolate processing aid and
Impurity, complete the removal of impurities of wine liquid.
In certain embodiments, wine liquid can be white wine, wine liquid and processing aid are blended in equipment body, Ran Houjin
Row electrolysis, the voltage general control of electrolysis is between 0-36V, and in electrolytic process, stirring system is stirred to white wine, so
The pH of white wine can be measured accurate, when the pH of white wine is stable more than 8, is then separated by filtration impurity and processing aid, is produced
To qualified white wine.
The amount of white wine is the 1/2-2/3 of equipment body capacity, and processing aid is no less than the 0.5% of white wine volume, due to adding
The work auxiliary agent later stage can be filtered to remove, and on the premise of meeting the needs of electrolysis, can arbitrarily add.Processing aid can select
Activated carbon, calcium chloride, potassium carbonate, sodium acid carbonate, magnesia, the one or several kinds in diatomite and magnesium silicate.
There are some not volatile, high boiling grease type impurity in white wine, in order to remove these impurity, it is necessary to make white wine
In alkaline environment, so in alkaline environment, grease type impurity can produce certain saponification, form non-solubility and consolidate
Flocculation is produced after fixed and is separated out, in follow-up filtration step, removes impurity and the processing aid added in white wine.
In a preferred embodiment of the invention, in step (a), the temperature for being electrolysed wine liquid is less than 40 DEG C.
It is electrolysed for white wine, white wine temperature is unsuitable too high, due to 78 DEG C or so of the temperature of ethanol, when white wine is electrolysed temperature
Height is spent, white wine volatilizees serious, while escaping gas in removing white wine, can also discharge substantial amounts of ethanol, cause white
The loss of wine.
When the temperature for being electrolysed wine liquid is higher than 40 DEG C, temperature is set not increase by reducing the voltage of electrolysis, even
By the voltage Tiao Jiedao 0V of electrolysis, stop the electrolysis to wine liquid, when less than 40 DEG C of temperature decline, then re-start electrolysis;We
The voltage between 0-36V that method uses is electrolysed, and 36V is the safe voltage of alternating current, and electricity is carried out below this safe voltage
Solution, can avoid that unexpected accident occurs, and ensure being smoothed out for production, and ensure the safety of operating personnel.
In the preferred embodiment for the present invention, in step (a), the pressure for being electrolysed wine liquid is less than 0.2mPa.
In order to reduce the loss of white wine, when electrolysis, control pressure is in 0.2mPa;When pressure is more than this numerical value
When, the gas in equipment body is discharged, when less than 0.2mPa, gas caused by electrolysis white wine is unable to arrange in slave unit main body
Go out, the ethanol volatilized in white wine can not discharge, with the raising of pressure in equipment body, white wine under higher pressure,
The volatilization of ethanol is also reduced, can be in time by equipment body Inner electrolysis when pressure is exhausted more than 0.2mPa in equipment body
Gas caused by white wine is discharged, and and can reduces the volatilization of ethanol in white wine.
In the preferred embodiment for the present invention, in step (a), the rotating speed of stirring system is in 36r/min-90r/min.
In white wine electrolytic process, the pH rises of white wine, the rotating speed of stirring system constantly increases, as pH is raised, pH
Rise is also rapider, in order that the rise that pH will not be local, causes the inaccurate of monitoring, stirring system quick rotation, make white wine
PH stirs.
In a preferred embodiment of the invention, in step (b), determine that pH is stable more than 8, comprise the following steps:
(s) in wine liquid electrolytic process, it is monitored by pH monitors, when pH is more than 8.5, stands wine liquid 10-24
Hour, detection wine liquid pH;
(m) when wine liquid pH is less than 8, repeat the above steps.
During white wine is electrolysed, the pH of white wine is constantly elevated, when white wine pH rises to more than 8.5, stop into
Row electrolysis, static wine liquid 10-24 hours, the hydrogen ion during this in white wine is uniformly distributed, treat white wine pH it is stable with
Afterwards, whether pH is more than 8 after testing, and when less than 8, the alkaline environment of white wine can not meet grease type impurity soap occurs
Change reaction and remove, it is necessary to continue to be electrolysed, so that the impurity of grease type can remove under alkaline environment.
With reference to specific embodiment, the present invention is described further.
Embodiment 1
A kind of wine liquid impurity-removing method is present embodiments provided, is carried out in accordance with the following steps:
2/3 white wine of equipment body capacity and 0.5% magnesium carbonate, the silica no less than white wine volume are added to
Relaxed uniformly in equipment body, while open stirring system, the speed setting of agitating paddle is 36r/min;White wine is controlled at 40 DEG C
It is electrolysed below, the relief valve on equipment body is set as 0.2mPa;Such continued electrolysis, with pH rise, improve
The rotating speed of the agitating paddle of stirring system, the electrolysis power of electrolysis motor is reduced, so reduce pH ramp-up rate, when pH is 7
When, the rotating speed of agitator of stirring system brings up to 90r/min;PH monitors monitor the PH of white wine in real time;When the PH of white wine is big
When 8.5, stop electrolysis and stirring, static white wine 24 hours, then detect the PH of white wine;When white wine PH be less than 8, continue
White wine is electrolysed, white wine PH is reached more than 8.5, then stands 24 hours, detects white wine PH, after white wine stands 24 hours,
PH carries out filtering to isolate processing aid and impurity, the white wine after this spline filter just completes removal of impurities more than 8.
Wine liquid impurity-removing method provided by the invention, by increasing processing aid in wine liquid, is electrolysed, then to wine liquid
By filter by processing aid and contaminant filter, so as to complete the requirement to wine liquid removal of impurities, compared with conventional method, more
It is effectively quick, the quality of drinks can be lifted, mouthfeel is drunk in improvement, shortens the production cycle, reduces production cost.
Finally it should be noted that:Various embodiments above is merely illustrative of the technical solution of the present invention, rather than its limitations;To the greatest extent
The present invention is described in detail with reference to foregoing embodiments for pipe, it will be understood by those within the art that:Its according to
The technical scheme described in foregoing embodiments can so be modified, either which part or all technical characteristic are entered
Row equivalent substitution;And these modifications or replacement, the essence of appropriate technical solution is departed from various embodiments of the present invention technology
The scope of scheme.
Claims (1)
1. a kind of wine liquid impurity-removing method, it is characterised in that comprise the following steps:
(a) wine liquid is added in equipment body to be well mixed with processing aid and be electrolysed, while open stirring system;
(b) white wine pH is detected, when pH it is stable more than 8 after, wine liquid is filtered, isolates processing aid and miscellaneous
Matter, complete the removal of impurities of wine liquid;
In step (a), the temperature for being electrolysed wine liquid is less than 40 DEG C;In step (a), the pressure for being electrolysed wine liquid is less than 0.2mPa;
In step (a), the rotating speed of stirring system is in 36r/min-90r/min;In step (b), determine pH it is stable 8 with
On, comprise the following steps:
(s) in wine liquid electrolytic process, it is monitored by PH monitors, when pH is more than 8.5, stands wine liquid 10-24 hours,
Detect wine liquid pH;
(m) when wine liquid pH is less than 8, repeat to be electrolysed.
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CN201710319722.7A CN107099439B (en) | 2017-05-09 | 2017-05-09 | White-spirit purifying equipment and wine liquid impurity-removing method |
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CN107099439A CN107099439A (en) | 2017-08-29 |
CN107099439B true CN107099439B (en) | 2018-03-16 |
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CN112387004A (en) * | 2020-11-03 | 2021-02-23 | 江苏金昉首乌酒业有限公司 | Filtering process and filtering equipment for white spirit production |
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CN1099413A (en) * | 1993-08-26 | 1995-03-01 | 王彦 | Method and apparatus for clarifying white spirt |
US20080035548A1 (en) * | 2006-08-01 | 2008-02-14 | Quos, Inc. | Multi-functional filtration and ultra-pure water generator |
US20080029395A1 (en) * | 2006-08-01 | 2008-02-07 | Gas Technology Institute | Multi-functional filtration and ultra-pure water generator |
CN201506786U (en) * | 2009-05-12 | 2010-06-16 | 新疆汇德源果酒有限公司 | High-voltage electric field wine processing device |
CN106148147A (en) * | 2015-04-18 | 2016-11-23 | 天津市凯源天诚过滤设备有限公司 | A kind of micro computer Chinese liquor processing equipment |
CN205132171U (en) * | 2015-11-24 | 2016-04-06 | 四川省宜宾市天坛酒业有限责任公司 | Gravity tank of white spirit filling |
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