CN107083166A - A kind of preparation method of waterproof material - Google Patents
A kind of preparation method of waterproof material Download PDFInfo
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- CN107083166A CN107083166A CN201710429313.2A CN201710429313A CN107083166A CN 107083166 A CN107083166 A CN 107083166A CN 201710429313 A CN201710429313 A CN 201710429313A CN 107083166 A CN107083166 A CN 107083166A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A kind of preparation method of waterproof material, comprises the following steps:First, PPG is dehydrated under conditions of 150 200 DEG C, the PPG after dehydration is added in agitator, stirred, obtain mixture one;2nd, composite modifier is added into mixture one, is warming up to 60 80 DEG C, heated and stir 40 60min, obtain mixture two;3rd, inorganic filler, stabilizer, plasticizer and softening agent are added into mixture two successively, 2 3h are reacted at a temperature of 120 180 DEG C, mixture three is obtained;4th, it is cooled to after normal temperature.The present invention has excellent water resistance, and low, heat-resist, waterproof, anti-aging, the corrosion-resistant and anti-ultraviolet advantage of good endurance, cost, also there is excellent mechanical property, storage stability and higher thermal insulation, and its preparation method is simple, lower cost for material, is adapted to industrialization mass production.
Description
Technical field
The invention belongs to waterproof material technical field, and in particular to a kind of preparation method of waterproof material.
Background technology
China is a building big country, and the high speed development of building trade has also driven the development of anti-aquatic products industry, and existing
Waterproof material has certain use limitation, such as waterproof roll in waterproof construction when the shape according to waterproof matrix is cut out
Cut, need polylith to splice for complicated basic unit, the bonding of the mutual lap-joint of waterproof roll is loosely or service life short fatal lacks
Fall into and be just completely exposed, by the effect of colding and heat succeed each other, easily caused leakage hidden trouble.The protection and leak of waterproof roll after construction
Maintenance afterwards is also problem, and exposed waterproof layer seems very sensitive to external mechanical injuries, i.e., waterproof roll with
Either Man Pu, Dian Pu, bar are spread the bonding of basic unit, sky is spread, and all will be to walk water layer between coiled material and basic unit, no matter any position
Penetrability is damaged, degumming, leak adhesive, and the whole coupled water-proof function for passing through aspect is all by the mistake that all declines, if can not find breakage
And rejected region, then need all to reform waterproof layer, cause great fund and waste of time.
Waterproof material waterproof layer is after being brushed in basic unit, by being generated after the physical and chemical reaction consolidation of material in itself
Waterproof layer, traditional soluble polyurethane waterproof material is made up of polyurethane with coal tar as raw material, is volatilized in use
Tar gas, toxicity is big and not easy-clear, and hardening time is long, and 2000 disabled in China.The polyurethane water-proof of existing in the market
Material generally existing solid content is low, poor from thickening property, the characteristic such as water resistance and glued membrane intensity difference, and construction needs multipass brushing, often
There is certain interval time all over brushing, the engineering time is longer.The problem of waterproof material waterproof layer is maximum is an exposure under sunlight,
Easily the degradation and decomposition because of ultraviolet, loses the function of waterproof layer.In the urgent need to address these of current field of waterproof materials are asked
Topic.
In summary, it is therefore desirable to a kind of preparation method of more preferable waterproof material, to improve the deficiencies in the prior art, from
And promote the development of building trade.
The content of the invention
It is an object of the invention to provide a kind of preparation method of waterproof material, the present invention has excellent water proofing property
Can, and low, heat-resist, waterproof, anti-aging, the corrosion-resistant and anti-ultraviolet advantage of good endurance, cost, also with excellent
Different mechanical property, storage stability and higher thermal insulation, and its preparation method is simple, lower cost for material, is adapted to
Industrialize mass production.
The invention provides following technical scheme:
A kind of preparation method of waterproof material, comprises the following steps:
First, PPG is dehydrated under conditions of 150-200 DEG C, the PPG after dehydration is added to stirring
In device, stir, obtain mixture one;
2nd, composite modifier is added into mixture one, is warming up to 60-80 DEG C, heated and stir 40-60min, obtain mixture
Two;
3rd, inorganic filler, stabilizer, plasticizer and softening agent are added into mixture two successively, it is anti-at a temperature of 120-180 DEG C
2-3h is answered, mixture three is obtained;
4th, it is cooled to after normal temperature.
It is preferred that, the waterproof material includes the raw material of following parts by weight:10-15 parts of PPG, composite modifier
8-12 parts of 10-14 parts, 8-16 parts of inorganic filler, 10-15 parts of stabilizer, 7-12 parts of plasticizer and softening agent.
It is preferred that, the waterproof material includes the raw material of following parts by weight:15 parts of PPG, composite modifier 10
8 parts of part, 16 parts of inorganic filler, 10 parts of stabilizer, 12 parts of plasticizer and softening agent.
It is preferred that, the composite modifier of the step 2 is styrene-butadiene block copolymer, polystyrene-fourth two
Alkene copolymer, polyethylene and any of polypropylene and its derivative or a variety of combinations, the washability of the composition are numerous,
So that material source scope is wide, it is with low cost, it is easy to prepare.
It is preferred that, the inorganic filler of the step 3 is calcium carbonate, barium sulfate or talcum powder.
It is preferred that, the species of the plasticizer of the step 3 is aliphatic dibasic acid ester, Phthalates, benzene polyacid
Any of esters, benzoates, epoxies, citric acid ester type and polyesters or a variety of combinations.
It is preferred that, the softening agent softening agent of the step 3 is times in naphthenic oil, hydrocarbon oil and industrial vaseline
One or more combinations, the composition is conducive to the hydrophobicity of raising mode material so that water resistance is improved.
It is preferred that, the step 4 is cooled to after normal temperature and stands 2-3 days again.
The beneficial effects of the invention are as follows:
The present invention has excellent water resistance, and good endurance, cost are low, heat-resist, waterproof, anti-aging, corrosion resistant
Erosion and anti-ultraviolet advantage, also with excellent mechanical property, storage stability and higher thermal insulation, and it is prepared
Method is simple, lower cost for material, is adapted to industrialization mass production.
The composite modifier of the step two of the present invention is styrene-butadiene block copolymer, styrene-butadiene is common
Polymers, polyethylene and any of polypropylene and its derivative or a variety of combinations, the washability of the composition are numerous so that
Material source scope is wide, with low cost, it is easy to prepare.
The softening agent softening agent of the step three of the present invention is any of naphthenic oil, hydrocarbon oil and industrial vaseline
Or a variety of combinations, the composition is conducive to the hydrophobicity of raising mode material so that water resistance is improved.
Embodiment
Embodiment 1
A kind of preparation method of waterproof material, comprises the following steps:
First, PPG is dehydrated under conditions of 150 DEG C, the PPG after dehydration is added to agitator
In, stir, obtain mixture one;
2nd, composite modifier is added into mixture one, is warming up to 80 DEG C, heated and stir 60min, obtain mixture two;
3rd, inorganic filler, stabilizer, plasticizer and softening agent are added into mixture two successively, is reacted at a temperature of 180 DEG C
3h, obtains mixture three;
4th, it is cooled to after normal temperature.
Waterproof material includes the raw material of following parts by weight:15 parts of PPG, 10 parts of composite modifier, inorganic filler 16
Part, 10 parts of stabilizer, 12 parts of plasticizer and 8 parts of softening agent.
The composite modifier of step 2 is styrene-butadiene block copolymer, PSB, gathered
The combination of ethene and polypropylene and its derivative, the washability of the composition is numerous so that material source scope is wide, with low cost,
It is easily prepared.
The inorganic filler of step 3 is calcium carbonate.
The species of the plasticizer of step 3 is aliphatic dibasic acid ester, Phthalates, benzoates, epoxy
The combination of class, citric acid ester type and polyesters.
The softening agent softening agent of step 3 is the combination of naphthenic oil and industrial vaseline, and the composition is conducive to raising mode
The hydrophobicity of material so that water resistance is improved.
Step 4 is cooled to after normal temperature stands 2 days again.
Embodiment 2
A kind of preparation method of waterproof material, comprises the following steps:
First, PPG is dehydrated under conditions of 200 DEG C, the PPG after dehydration is added to agitator
In, stir, obtain mixture one;
2nd, composite modifier is added into mixture one, is warming up to 60 DEG C, heated and stir 40min, obtain mixture two;
3rd, inorganic filler, stabilizer, plasticizer and softening agent are added into mixture two successively, is reacted at a temperature of 180 DEG C
2h, obtains mixture three;
4th, it is cooled to after normal temperature.
Waterproof material includes the raw material of following parts by weight:15 parts of PPG, 14 parts of composite modifier, inorganic filler 8
Part, 15 parts of stabilizer, 7 parts of plasticizer and 8 parts of softening agent.
The composite modifier of step 2 is styrene-butadiene block copolymer, polyethylene and polypropylene and its derivative
Combination, the washability of the composition is numerous so that material source scope is wide, with low cost, it is easy to prepare.
The inorganic filler of step 3 is talcum powder.
The species of the plasticizer of step 3 is Phthalates, many esters of gallic acid of benzene, benzoates, epoxies, lemon
The combination of esters of gallic acid and polyesters.
The softening agent softening agent of step 3 is the combination of hydrocarbon oil and industrial vaseline, and the composition is conducive to raising side
The hydrophobicity of formula material so that water resistance is improved.
Step 4 is cooled to after normal temperature stands 3 days again.
Embodiment 3
A kind of preparation method of waterproof material, comprises the following steps:
First, PPG is dehydrated under conditions of 200 DEG C, the PPG after dehydration is added to agitator
In, stir, obtain mixture one;
2nd, composite modifier is added into mixture one, is warming up to 60 DEG C, heated and stir 60min, obtain mixture two;
3rd, inorganic filler, stabilizer, plasticizer and softening agent are added into mixture two successively, is reacted at a temperature of 180 DEG C
2h, obtains mixture three;
4th, it is cooled to after normal temperature.
Waterproof material includes the raw material of following parts by weight:10 parts of PPG, 14 parts of composite modifier, inorganic filler 8
Part, 10 parts of stabilizer, 12 parts of plasticizer and 12 parts of softening agent.
The composite modifier of step 2 is styrene-butadiene block copolymer, PSB, gathered
The combination of ethene and polypropylene and its derivative, the washability of the composition is numerous so that material source scope is wide, with low cost,
It is easily prepared.
The inorganic filler of step 3 is talcum powder.
The species of the plasticizer of step 3 be aliphatic dibasic acid ester, many esters of gallic acid of benzene, benzoates, epoxies,
The combination of citric acid ester type and polyesters.
The softening agent softening agent of step 3 is the combination of naphthenic oil, hydrocarbon oil and industrial vaseline, and the composition is favourable
In the hydrophobicity for improving mode material so that water resistance is improved.
Step 4 is cooled to after normal temperature stands 3 days again.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality
Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention
God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (8)
1. a kind of preparation method of waterproof material, it is characterised in that comprise the following steps:
First, PPG is dehydrated under conditions of 150-200 DEG C, the PPG after dehydration is added to stirring
In device, stir, obtain mixture one;
2nd, composite modifier is added into mixture one, is warming up to 60-80 DEG C, heated and stir 40-60min, obtain mixture
Two;
3rd, inorganic filler, stabilizer, plasticizer and softening agent are added into mixture two successively, it is anti-at a temperature of 120-180 DEG C
2-3h is answered, mixture three is obtained;
4th, it is cooled to after normal temperature.
2. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the waterproof material bag
Include the raw material of following parts by weight:10-15 parts of PPG, 10-14 parts of composite modifier, 8-16 parts of inorganic filler, stabilizer
8-12 parts of 10-15 parts, 7-12 parts of plasticizer and softening agent.
3. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the waterproof material bag
Include the raw material of following parts by weight:15 parts of PPG, 10 parts of composite modifier, 16 parts of inorganic filler, 10 parts of stabilizer, plasticising
8 parts of 12 parts of agent and softening agent.
4. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the step 2 is answered
Conjunction modifying agent is styrene-butadiene block copolymer, PSB, polyethylene and polypropylene and its spread out
Any of biology or a variety of combinations.
5. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the nothing of the step 3
Machine filler is calcium carbonate, barium sulfate or talcum powder.
6. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the increasing of the step 3
The species for moulding agent is aliphatic dibasic acid ester, Phthalates, many esters of gallic acid of benzene, benzoates, epoxies, citric acid
Any of esters and polyesters or a variety of combinations.
7. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the step 3 it is soft
Agent softening agent is any of naphthenic oil, hydrocarbon oil and industrial vaseline or a variety of combinations.
8. a kind of preparation method of waterproof material according to claim 1, it is characterised in that the step 4 cooling
2-3 days are stood again after to normal temperature.
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CN201710429313.2A CN107083166A (en) | 2017-06-08 | 2017-06-08 | A kind of preparation method of waterproof material |
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CN201710429313.2A CN107083166A (en) | 2017-06-08 | 2017-06-08 | A kind of preparation method of waterproof material |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108342939A (en) * | 2018-01-08 | 2018-07-31 | 深圳市东进技术服务有限公司 | A kind of anti-ponding type asphalt pavement construction method |
CN109712750A (en) * | 2019-02-26 | 2019-05-03 | 广州粤道智能科技发展有限公司 | A kind of comprehensive wiring cable of resistance to limiting temperature |
CN113085429A (en) * | 2021-03-26 | 2021-07-09 | 广东虎彩影像有限公司 | Digital stained paper ceramic thermal transfer printing process |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104031545A (en) * | 2014-06-11 | 2014-09-10 | 江苏通铨防水材料科技有限公司 | W-OH-WP permeable reactive waterproof material and preparation method and using method thereof |
CN106221250A (en) * | 2016-08-15 | 2016-12-14 | 安庆越球建筑防水材料有限公司 | A kind of rubber modified asphalt waterproof material |
-
2017
- 2017-06-08 CN CN201710429313.2A patent/CN107083166A/en not_active Withdrawn
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104031545A (en) * | 2014-06-11 | 2014-09-10 | 江苏通铨防水材料科技有限公司 | W-OH-WP permeable reactive waterproof material and preparation method and using method thereof |
CN106221250A (en) * | 2016-08-15 | 2016-12-14 | 安庆越球建筑防水材料有限公司 | A kind of rubber modified asphalt waterproof material |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108342939A (en) * | 2018-01-08 | 2018-07-31 | 深圳市东进技术服务有限公司 | A kind of anti-ponding type asphalt pavement construction method |
CN109712750A (en) * | 2019-02-26 | 2019-05-03 | 广州粤道智能科技发展有限公司 | A kind of comprehensive wiring cable of resistance to limiting temperature |
CN113085429A (en) * | 2021-03-26 | 2021-07-09 | 广东虎彩影像有限公司 | Digital stained paper ceramic thermal transfer printing process |
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Application publication date: 20170822 |