CN107063927A - Optical fiber oil product kinematic viscosity determines device - Google Patents

Optical fiber oil product kinematic viscosity determines device Download PDF

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Publication number
CN107063927A
CN107063927A CN201710281229.0A CN201710281229A CN107063927A CN 107063927 A CN107063927 A CN 107063927A CN 201710281229 A CN201710281229 A CN 201710281229A CN 107063927 A CN107063927 A CN 107063927A
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CN
China
Prior art keywords
optical fiber
tube
shaped optical
shaped
tube group
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Pending
Application number
CN201710281229.0A
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Chinese (zh)
Inventor
徐士博
杨先辉
朱礼斌
黄亮
何宇
于波涛
张际兵
张士川
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CNPC Bohai Drilling Engineering Co Ltd
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CNPC Bohai Drilling Engineering Co Ltd
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Application filed by CNPC Bohai Drilling Engineering Co Ltd filed Critical CNPC Bohai Drilling Engineering Co Ltd
Priority to CN201710281229.0A priority Critical patent/CN107063927A/en
Publication of CN107063927A publication Critical patent/CN107063927A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/02Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material
    • G01N11/04Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture
    • G01N11/06Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture by timing the outflow of a known quantity

Abstract

Device, including capillary viscometer, the first optical fiber tube group, the second optical fiber tube group, light source and photodetection and processing unit are determined the invention discloses a kind of optical fiber oil product kinematic viscosity;Wherein, first optical fiber tube group and the second optical fiber tube group include two symmetrically arranged two L-shaped optical fiber tubes, by will form the transmission of optical signal at two test point graticules being against on capillary viscometer of transverse tube pipe end per symmetrically arranged two L-shaped optical fiber tubes respectively and receive medium, the rapid interval time for inerrably detecting fast-changing liquid level, the stability and the degree of accuracy for making measurement are not disturbed by temperature fluctuation, the measure device continues to use the capillary viscometer and corresponding measurement request and measuring method of national regulations simultaneously, meet the requirement that laboratory is accurately tested the full-automatic kinematic viscosity of oil sample.

Description

Optical fiber oil product kinematic viscosity determines device
Technical field
The present invention relates to oil field development experimental assembly technical field, more particularly to a kind of optical fiber oil product kinematic viscosity is surveyed Determine device.
Background technology
With successively decreasing year by year for Some Domestic field output, equipment wearing aggravation is changed by the cycle to oil product What is become is particularly important, and viscosity is to evaluate whether oil property can meet right in one of important indicator of need of work, national standard There are many introductions in the measuring method of viscosity.Wherein, capillary tube method is produced because its is simple to operate, the degree of accuracy is high by vast oil The favor of product reviewer, it is often more important that it is still that metrological service can demarcate unique instrument of normal viscosity at present.At present The viscosity measurement of national regulations is to use manual viscosity determinator, but its complex operation, and labor intensity is big, and system is missed It is poor big;There is " temperature drift " phenomenon, serious restriction and shadow in oil sample viscosity measurement of the measurement module of conditional electronic class in constant temperature bath Ring the accuracy of measurement result;And similar foreign products are expensive, maintenance cost is high.
The content of the invention
Meeting national standard it is an object of the invention to provide one kind being capable of limnograph oil sample viscosity and not by temperature change The optical fiber oil product kinematic viscosity of influence determines device.
Therefore, technical solution of the present invention is as follows:
A kind of optical fiber oil product kinematic viscosity determines device, including capillary viscometer, the first optical fiber tube group, the second light Fine pipe group, light source and photodetection and processing unit;Wherein,
First optical fiber tube group includes two L-shaped optical fiber tubes, and two L-shaped optical fiber tubes are symmetricly set on capillary viscometer two Side, and make that the transverse tube of two L-shaped optical fiber tubes is located in same horizontal line and transverse tube pipe end is against the capillary of capillary viscometer On the wall of offside side;
Second optical fiber tube group also includes two L-shaped optical fiber tubes, and two L-shaped optical fiber tubes are symmetricly set on capillary viscometer two Side, and make that the transverse tube of two L-shaped optical fiber tubes is located in same horizontal line and transverse tube pipe end is against the capillary of capillary viscometer On the wall of offside side, and the transverse tube of two L-shaped optical fiber tubes of the second optical fiber tube group is disposed on two L-shaped of the first optical fiber tube group Below the transverse tube of optical fiber tube;
Each L-shaped optical fiber tube of first optical fiber tube group and the second optical fiber tube group is neighbouring to be set, and is positioned adjacent to light source Above the vertical tube pipe end of the two L-shaped optical fiber tubes set, the flashlight that light source is sent is set to enter L-shaped optical fiber tube by Space Coupling Fibre bundle in carry out optical transport;
Photodetection and processing unit are arranged far from above the vertical tube pipe end of two L-shaped optical fiber tubes of light source, and it includes First photodetector, the second photodetector, signal processor, timer and the display screen being connected with timer;Described L-shaped optical fiber tube of one photodetector respectively with timer and the first optical fiber tube group of lower section is connected;Second photodetector point L-shaped optical fiber tube not with timer and the second optical fiber tube group of lower section is connected.
Further, light source is LED/light source;L-shaped optical fiber tube is by internal diameter 3mm L-shaped steel pipe and filling and full of in steel pipe The multi beam multimode fibre in side space is constituted.
Further, the transverse tube of two L-shaped optical fiber tubes of the second optical fiber tube group and the L-shaped optical fiber tube of the first optical fiber tube group Perpendicular separation distance between transverse tube is 35 ± 2mm.
Further, one L-shaped glass protection pipe is housed in every L-shaped optical fiber tube outer layer jacket.
Compared with prior art, the optical fiber oil product kinematic viscosity assay device structures are simple, and cost is low, and measurement is easy Fast, data are accurately and reliably;Specifically, the capillary viscometer and corresponding measurement request of the measure device national regulations and Measuring method;Medium is transmitted and received simultaneously as signal using multi beam optical fiber, can inerrably be detected rapidly quick The interval time of the liquid level of change, the stability and the degree of accuracy for making measurement is not disturbed by temperature fluctuation, meets laboratory to oil The requirement that the full-automatic kinematic viscosity of sample is accurately tested, has higher commercial value in terms of the measurement of oil kinematic viscosity at home.
Brief description of the drawings
Fig. 1 determines the positive structure schematic of device for the optical fiber oil product kinematic viscosity of the present invention;
Fig. 2 determines the side structure schematic diagram of device for the optical fiber oil product kinematic viscosity of the present invention;
Fig. 3 determines the structural representation of the capillary viscometer of device for the optical fiber oil product kinematic viscosity of the present invention;
Fig. 4 determines the capillary viscometer of device, the second optical fiber tube group for the optical fiber oil product kinematic viscosity of the present invention And second set-up mode between optical fiber tube group structural representation.
Embodiment
Below in conjunction with the accompanying drawings and specific embodiment the present invention is described further, but following embodiments are absolutely not to this hair It is bright to have any limitation.
As shown in figure 1, the capillary that the optical fiber oil product kinematic viscosity, which determines device, to be included being arranged on main frame 6 glues The 1, first optical fiber tube group 2 of degree meter, the second optical fiber tube group 3, light source 4 and photodetection and processing unit 5;Specifically:
As shown in Fig. 1~2, main frame includes montant 601, the first level plate 602 for being fixed on the top of montant 601 and fixed The second level board 603 in the bottom of montant 601, two upper and lower spaced first light guides are further fixed at the middle part of montant 601 The optical fibre tube fixed plate 605 of fibre pipe fixed plate 604 and second;Specifically, the first optical fibre tube fixed plate 604 and second Perpendicular separation distance between optical fibre tube fixed plate 605 is 35mm;First optical fibre tube fixed plate 604 and the second light guide Two inserting grooves being located on same axis are offered in fibre pipe fixed plate 605, make the He of the first optical fibre tube fixed plate 604 Second optical fibre tube fixed plate 605 is arranged on the capillary side of capillary viscometer 1;
As shown in figure 3, capillary viscometer 1 is standard GB/T/T265-88《Oil product kinematic viscosity determination method and Dynamic viscosity calculating method》Specified in U-shaped capillary viscometer, its concrete structure include by the first pipe shaft 101, capillary 104 With the second pipe shaft 106, top-down processing has the first enlarged portion 102 and second to expand between the first pipe shaft 101 and capillary 104 Portion 103 is opened, the downside of the second pipe shaft 106 is machined with the 3rd enlarged portion 105;On the side wall close to the port of the second pipe shaft 106 A connecting branch is machined with, for connecting air extractor;Specifically, the internal diameter of the first pipe shaft 101 is 4mm;Second pipe shaft 106 Internal diameter is 10mm;And depending on species of the internal diameter of capillary 104 according to oil sample to be tested;For example, when oil sample to be tested is diesel oil, The internal diameter of capillary 104 is processed as 0.8mm, and 200s is no less than in the flowing time of timing section to meet oil sample to be tested;
Wherein, the first optical fibre tube fixed plate 604 is horizontally disposed and is fixed on the first enlarged portion 102 and the second enlarged portion 103 junction, the second optical fibre tube fixed plate 605 is horizontally disposed and is fixed on the second enlarged portion 103 and capillary 104 Junction;Second pipe shaft 106 is fixed on the second level board 603;
As shown in figs. 34, the first optical fiber tube group 2 includes two L-shaped optical fiber tubes 201,202, and two L-shaped optical fiber tubes are symmetrical Be arranged on the both sides of capillary viscometer 1, and make the transverse tube of two L-shaped optical fiber tubes be located in same horizontal line and transverse tube pipe end end Face is against on the capillary offside side wall of capillary viscometer 1;
Correspondingly, to make two L-shaped optical fiber tubes 201,202 of the first optical fiber tube group 2 and the capillary of capillary viscometer 1 104 set location is fixed, and radially offering two from the two sides of the first optical fibre tube fixed plate 604 is located at same water Jack on horizontal line, and two jacks with plate axially extending bore be interconnected, make the horizontal stroke of two L-shaped optical fiber tubes 201,202 Pipe is inserted into jack and end face is contacted with the capillary 104 of capillary viscometer 1;Two L-shaped optical fiber tubes 201,202 take the shape of the letter U, The light-path for first connection of formation of capillary 104 that clear glass between is made;
As shown in figs. 34, the second optical fiber tube group 3 also includes two L-shaped optical fiber tubes, and two L-shaped optical fiber tubes are symmetricly set on The both sides of capillary viscometer 1, and make that the transverse tube of two L-shaped optical fiber tubes is located in same horizontal line and the pipe end end face of transverse tube is against On the capillary offside side wall of capillary viscometer 1, and the transverse tube of two L-shaped optical fiber tubes of the second optical fiber tube group 3 is arranged at intervals Below the transverse tube of two L-shaped optical fiber tubes of the first optical fiber tube group 2;
Correspondingly, to make two L-shaped optical fiber tubes 301,302 of the second optical fiber tube group 3 and the capillary of capillary viscometer 1 104 set locations are fixed, and radially offering two from the two sides of the second optical fibre tube fixed plate 605 is located at same level Jack on line, two jacks are equally interconnected with the axially extending bore on plate, and the transverse tube of two L-shaped optical fiber tubes 301,302 is inserted In jack and end face is contacted with the capillary 104 of capillary viscometer 1, two L-shaped optical fiber tubes 301,302 is taken the shape of the letter U, lead to The light-path of the formation Article 2 connection of clear glass vertical tube 101 between crossing;
Wherein, the vertical tube length of two L-shaped optical fiber tubes 201,202 of the second optical fiber tube group 3 is more than the first optical fiber tube group 2 The vertical tube length of two L-shaped optical fiber tubes 301,302, flushes the vertical tube top port of four L-shaped optical fiber tubes, and by being opened in Four through holes on first level plate 602 stretch out first level plate 602;Wherein, L-shaped optical fiber tube 201 and L-shaped optical fiber tube 301 are adjacent Near to set, light source 4 is arranged on first level plate 602, and is particularly located at the top of L-shaped optical fiber tube 201 and L-shaped optical fiber tube 301, The flashlight that light source 4 is sent is entered by Space Coupling in the fibre bundle of optical fiber tube and carry out optical transport, i.e. L-shaped optical fiber tube 201 For input path, accordingly, L-shaped optical fiber tube 202 is emitting light path, similarly, and L-shaped optical fiber tube 301 is input path, accordingly, L Shape optical fiber tube 302 is emitting light path;
Wherein, light source 4 selects LED/light source;L-shaped optical fiber tube is by internal diameter 3mm L-shaped steel pipe and filling and full of on the inside of steel pipe The multi beam multimode fibre in space is constituted, to meet the transmission requirement of light.Meanwhile, to prevent L-shaped optical fiber tube from damaging, in every L-shaped Optical fiber outer tube layer is set with the adaptable L-shaped glass protection pipe of one ruler cun structure;
Photodetection and processing unit 5 are arranged on first level plate 602, and it includes the first photodetector, the second light Electric explorer, signal processor, timer and the display screen being connected with timer;Wherein, the first photodetector difference It is connected with the vertical tube pipe end of the L-shaped optical fiber tube 202 in timer and the first optical fiber tube group 2;Second photodetector respectively with meter When device and the L-shaped optical fiber tube 302 in the second optical fiber tube group 3 of homonymy vertical tube pipe end connection;First photodetector and Second photodetector is respectively used to receive the first optical fiber tube group 2 and the optical transport come that transmits of the second optical fiber tube group 3 blocks letter Number or optical transport communications signals, and the startup and stopping of timer for controlling to be attached thereto by signal processor, final timing The display screen of the actual timing time connection of device shows the interval time t of centre.Wherein, the first photodetector, the second light Electric explorer, signal processor, timer and LED/light source are connected by power line with plug, and direct plug-in can be opened when using Beginning work.
In use, preparing a depth in laboratory first is more than the height that the optical fiber oil product kinematic viscosity determines device The glass jar of degree, is added water as water-bath, and bath temperature is set in into a certain temperature that national regulations are measured by internal heater Lower holding temperature constant state 15 minutes;Then determined to the optical fiber oil product kinematic viscosity in device and inject oil sample to be tested, had Body method for implanting is:Capillary viscometer 1 is inverted and fills the port immersion of the first pipe shaft 101 in the container of oil sample, is blocked up On the firmly port of the second pipe shaft 106, the connecting branch that manual getter device is connected to the second pipe shaft 106 by gas pipeline, lead to The gas crossed in the second pipe shaft 106 of suction makes oil sample enter in the first enlarged portion 102 in the first pipe shaft 101;
After the completion of oil sample is extracted, the position of U-shaped capillary viscometer 1 is returned just, oil sample is left to capillary by Action of Gravity Field The bending section of the bottom of pipe viscosimeter 1;Capillary viscometer 1 is inserted in water bath with thermostatic control, specially by first level plate below 602 It is partially disposed in water bath with thermostatic control 15 minutes, after temperature is constant, you can proceed by determination step;
Unlatching LED/light source 4 and the first photodetector of photodetection and processing unit 5, the second photodetector, timing Device and display screen, make each device keep normal power-up working condition;Because the flashlight that LED/light source 4 is sent passes through Space Coupling Respectively enter in first light-path and Article 2 light-path that the first optical fiber tube group 2 and the second optical fiber tube group 3 are formed, i.e. signal Light is transmitted to the tube wall side of capillary 104 by incident optical beam, is received with another beam of incident optical on the same line Optical fiber is just relative in the tube wall opposite side of capillary 104, receives the signal for passing through capillary 104 from the outgoing of incident optical beam Light, then by reception optical fiber by the optical signal transmission received to photodetector;Therefore when oil sample is horizontal by optical fibre tube During the end face of pipe, because oil sample is acted on reflection, absorption of space optical signal etc., the light signal strength received is caused significantly to drop Low, light-path is blocked, and the first photodetector and the second photodetector can be received accordingly, that is, whether judge oil sample Or pass through the detection end face;
Vavuum pump is connected on the port of the first pipe shaft 101 of capillary viscometer 1 by gas pipeline;Opening vavuum pump makes Oil sample is slow along along the enlarged portion 103 of capillary 104 and second, when oil sample upper end liquid level reaches the first optical fibre tube fixed plate When 604, first optical transmission pathway of the first optical fibre tube formation is blocked, and the first photodetector detects the disconnected letter of photoresistance Number, and be transferred to signal processor and start timer and start timing, while vavuum pump stops suction, and make the first pipe shaft 101 with Air communication;Oil sample declines by self gravitation, is formed when oil sample upper end liquid level persistently falls and just leaves the second optical fiber tube group 3 Article 2 optical transmission pathway when, Article 2 optical transmission pathway is connected again, and the second photodetector detects light communications signals, And when being transferred to signal processor stopping timer, timing terminates, and the timing time t of timer is shown on screen;Repeat Even if measuring three time t, average and obtain tIt is average, and bring the oil sample kinematic viscosity calculating formula provided in standard into, you can Calculate oil sample to be tested kinematic viscosity vt

Claims (4)

1. a kind of optical fiber oil product kinematic viscosity determines device, it is characterised in that including capillary viscometer (1), the first light Fine pipe group (2), the second optical fiber tube group (3), light source (4) and photodetection and processing unit (5);Wherein,
First optical fiber tube group (2) includes two L-shaped optical fiber tubes, and two L-shaped optical fiber tubes are symmetricly set on capillary viscometer (1) two Side, and make that the transverse tube of two L-shaped optical fiber tubes is located in same horizontal line and transverse tube pipe end is against the capillary of capillary viscometer (1) On the wall of pipe offside side;
Second optical fiber tube group (3) also includes two L-shaped optical fiber tubes, and two L-shaped optical fiber tubes are symmetricly set on capillary viscometer (1) Both sides, and make that the transverse tube of two L-shaped optical fiber tubes is located in same horizontal line and transverse tube pipe end is against the hair of capillary viscometer (1) On the wall of tubule offside side, and the transverse tube of two L-shaped optical fiber tubes of the second optical fiber tube group (3) is disposed on the first optical fiber tube group (2) below the transverse tube of two L-shaped optical fiber tubes;
Each L-shaped optical fiber tube of first optical fiber tube group (2) and the second optical fiber tube group (3) is neighbouring to be set, and is arranged on light source (4) Above the vertical tube pipe end of the neighbouring two L-shaped optical fiber tubes set, the flashlight that light source (4) is sent is set to enter L by Space Coupling Optical transport is carried out in the fibre bundle of shape optical fiber tube;
Photodetection and processing unit (5) are arranged far from above the vertical tube pipe end of two L-shaped optical fiber tubes of light source (4), and it is wrapped Include the first photodetector, the second photodetector, signal processor, timer and the display screen being connected with timer;It is described L-shaped optical fiber tube of first photodetector respectively with timer and the first optical fiber tube group (2) of lower section is connected;Second photodetection L-shaped optical fiber tube of the device respectively with timer and the second optical fiber tube group (3) of lower section is connected.
2. optical fiber oil product kinematic viscosity according to claim 1 determines device, it is characterised in that light source (4) is LED light Source;L-shaped optical fiber tube is made up of internal diameter 3mm L-shaped steel pipe and filling and the multi beam multimode fibre full of steel pipe inner space.
3. optical fiber oil product kinematic viscosity according to claim 2 determines device, it is characterised in that the second optical fiber tube group (3) Two L-shaped optical fiber tubes transverse tube and the first optical fiber tube group (2) L-shaped optical fiber tube transverse tube between perpendicular separation distance be 35 ±2mm。
4. optical fiber oil product kinematic viscosity according to claim 2 determines device, it is characterised in that in every L-shaped optical fiber tube Outer layer jacket is equipped with a L-shaped glass protection pipe.
CN201710281229.0A 2017-04-26 2017-04-26 Optical fiber oil product kinematic viscosity determines device Pending CN107063927A (en)

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Application Number Priority Date Filing Date Title
CN201710281229.0A CN107063927A (en) 2017-04-26 2017-04-26 Optical fiber oil product kinematic viscosity determines device

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109653835A (en) * 2018-12-24 2019-04-19 重庆金康新能源汽车设计院有限公司 Detection method, detection system and the automobile of engine motor oil viscosity
CN113634027A (en) * 2021-07-04 2021-11-12 林哲鑫 Suction filtration experimental device and method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD216319A1 (en) * 1983-05-26 1984-12-05 Cottbus Energiekombinat ARRANGEMENT AND METHOD FOR DETECTING PROPERTIES OF A FLUID, IN PARTICULAR A GLASS MELT
CN2468038Y (en) * 2001-03-18 2001-12-26 唐祥元 Automatic detecting means of ping's caplastometer
CN201096700Y (en) * 2007-08-30 2008-08-06 中国人民解放军海军后勤技术装备研究所 Motion viscidity testing system
CN102539286A (en) * 2011-11-16 2012-07-04 山东轻工业学院 Automatic timing device and timing method of capillary viscometer

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD216319A1 (en) * 1983-05-26 1984-12-05 Cottbus Energiekombinat ARRANGEMENT AND METHOD FOR DETECTING PROPERTIES OF A FLUID, IN PARTICULAR A GLASS MELT
CN2468038Y (en) * 2001-03-18 2001-12-26 唐祥元 Automatic detecting means of ping's caplastometer
CN201096700Y (en) * 2007-08-30 2008-08-06 中国人民解放军海军后勤技术装备研究所 Motion viscidity testing system
CN102539286A (en) * 2011-11-16 2012-07-04 山东轻工业学院 Automatic timing device and timing method of capillary viscometer

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109653835A (en) * 2018-12-24 2019-04-19 重庆金康新能源汽车设计院有限公司 Detection method, detection system and the automobile of engine motor oil viscosity
CN113634027A (en) * 2021-07-04 2021-11-12 林哲鑫 Suction filtration experimental device and method
CN113634027B (en) * 2021-07-04 2022-12-23 林哲鑫 Suction filtration experimental device and method
CN113634027B8 (en) * 2021-07-04 2023-03-14 林哲鑫 Suction filtration experimental device and method

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Application publication date: 20170818