CN107056883B - The method and apparatus of albumen and phosphatide is recycled in a kind of euphausia superba powder production line waste water from boat-carrying - Google Patents

The method and apparatus of albumen and phosphatide is recycled in a kind of euphausia superba powder production line waste water from boat-carrying Download PDF

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CN107056883B
CN107056883B CN201710289688.3A CN201710289688A CN107056883B CN 107056883 B CN107056883 B CN 107056883B CN 201710289688 A CN201710289688 A CN 201710289688A CN 107056883 B CN107056883 B CN 107056883B
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krill
phosphatide
albumen
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liquid
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CN107056883A (en
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薛长湖
姜晓明
薛勇
尹利昂
田利利
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Ocean University of China
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    • C07ORGANIC CHEMISTRY
    • C07KPEPTIDES
    • C07K1/00General methods for the preparation of peptides, i.e. processes for the organic chemical preparation of peptides or proteins of any length
    • C07K1/14Extraction; Separation; Purification
    • C07K1/30Extraction; Separation; Purification by precipitation
    • C07K1/32Extraction; Separation; Purification by precipitation as complexes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07KPEPTIDES
    • C07K1/00General methods for the preparation of peptides, i.e. processes for the organic chemical preparation of peptides or proteins of any length
    • C07K1/02General methods for the preparation of peptides, i.e. processes for the organic chemical preparation of peptides or proteins of any length in solution

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Abstract

A kind of method that albumen and phosphatide are recycled the present invention relates to polar region development of resources and utilization, more particularly in euphausia superba powder production line waste water from boat-carrying, comprises the following steps:The first step, krill plus water are mixed and heated;Second step, carries out separation of solid and liquid by the mixed material A in the first step, obtains boiling rear krill and boil liquid A;3rd step, boil liquid A is further heated, and the protein encapsulation phosphatide in boil liquid A is formed protein, phospholipid compound;4th step, carries out separation of solid and liquid by the mixed material B obtained in the 3rd step, obtains protein, phospholipid compound and boil liquid B;5th step, the protein, phospholipid compound obtained in the 4th step is mixed with the rear krill of boiling obtained in second step, obtains mixing krill material;6th step, mixing krill material is dried, shrimp med is made;The advantage of the invention is that:Albumen and phosphatide have efficiently been recycled, has improved the output capacity of euphausia superba powder, has avoided the phenomenon of existing production line digesting apparatus " being burned ".

Description

A kind of method that albumen and phosphatide are recycled in the euphausia superba powder production line waste water from boat-carrying And equipment
Technical field
The present invention relates to polar region development of resources and field is utilized, more particularly to one kind is given up from boat-carrying euphausia superba powder production line The method and apparatus of albumen and phosphatide is recycled in water.
Background technology
Krill (Euphausia superba Dana) is a kind of small-sized shellfish for living in South Pole marine site, Marine stock biomass is about 1.25~7.5 hundred million tons, is not yet sufficiently developed at present.Krill is at present mainly by ship On be directly processed into euphausia superba powder or freezing krill.
Euphausia superba powder has higher protein, fat content, and amino acid composition is reasonable;Using euphausia superba powder as raw material The product research of exploitation also achieves positive progress.But the quality of current euphausia superba powder is generally poor, and research is found, influences The factor of euphausia superba powder nutrition and quality characteristic mainly includes:Time, place and the condition of capture, the quality of raw material and fresh Degree, processing technology and equipment, technology of storage and transport and condition etc..But at present on the processing of krill shrimp med and the report of storage technique It is less.
Euphausia superba powder is using krill as raw material, and the one kind obtained through processes such as boiling, dehydration, drying, crushing is produced Product, are mainly used in feed, krill oil extract etc. at present;Due to containing a large amount of enzymes in krill body, South Pole phosphorus can be caused Shrimp self-dissolving.Therefore, krill must be aboard ship processed as early as possible after capture.The euphausia superba powder of high-quality should adopt Aboard ship processed with the complete krill in 1~2h after capture.
Existing krill processing technology is mainly to have used for reference the Processing Technology Development of fish meal.But fish meal and shrimp Powder is having larger difference in terms of property of raw material and product performance.As fish meal raw material fish protein composition with krill have compared with Big difference;Fat requires as far as possible low in fish meal process, and as far as possible more reservation fat is required in shrimp med process;Fish meal It is not present pigment problem in process, there are the pigments such as degradable astaxanthin in shrimp med process.On the whole, shrimp med The technical issues that need to address are far more than fish meal in process.
At present, krill shrimp med boat-carrying processing mainly using krill as raw material, continental rise processing mainly with Freezing krill is raw material, is transported to by conveyer belt in digester, and digester heats for steam jacket, generally will be warm in pot Degree control completes boiling at 90 DEG C or so.But the digesting apparatus that the equipment of majority boat-carrying uses at present is spiral precooker, the South Pole The digestion time through going through is about 15~30min after krill enters digester, and the time is longer.Since digesting apparatus is continuous, steam The temperature of equipment is boiled due to the fluctuation of krill amount of fishing, in actual production process, according to produce reality on the ship of certain company Measurement, the temperature of digesting apparatus end is generally at 75 DEG C or so, and 75 DEG C for the part aqueous albumen of krill It heated denaturalization and then can not solidify completely, usually entered and boiled by the separation of solid and liquid of separation equipment with boil liquid Among liquid, although there is also the muscle protein of fish forms, fish larger with krill difference to this process in fish meal processing The content of myosinogen is relatively low in class muscle, and loss in this process is smaller, yield is impacted smaller.But the South Pole In krill shrimp med process, the phosphatide that the loss of this Partial Protein is usually associated with emulsification is entered in boil liquid at the same time.
And existing digesting apparatus is when temperature control is more than 90 DEG C, krill begins to warm to temperature from into digester Reach 90 DEG C take the dish out of the pot during, have substantial amounts of water-solubility protein dissolution into boil liquid.And substantial amounts of water-solubility protein is in pot Inside continue to heat up, start to condense, can gather the inner wall of digester, form one layer of albumen adhesion layer, and jacket steam pressure one As in 0.5MPa or so, " being burned ", which can occur, for albumen adhesion layer at this time causes the reduction of boiling vessel heat exchange efficiency, meanwhile, cause boiling Occur albumen in liquid and be charred taste, influence the quality of krill meal.
So how to ensure the output capacity of shrimp med, while " being burned " of conventional boil device is avoided again, while from boat-carrying The method of albumen and phosphatide is recycled in euphausia superba powder production line waste water up for exploitation.
The content of the invention
Present invention solves the technical problem that be, substantial amounts of sarcoplasm egg in shrimp med production line in euphausia superba in the prior art White and loss of lipid, causes shrimp med output capacity low.
To solve the above problems, we have proposed one kind to recycle albumen and phosphorus from boat-carrying euphausia superba powder production line waste water The method of fat, this method recycle albumen and phosphatide in boil liquid by the way that the separated liquid of feed liquid after boiling is carried out secondary temperature elevation, Avoid and apparatus for production line is significantly replaced, while also improve the output capacity of shrimp med, while avoid in production line " being burned " phenomenon of digesting apparatus.
To realize the demand, the present invention is achieved through the following technical solutions above-mentioned purpose:It is a kind of from boat-carrying South Pole phosphorus The method that albumen and phosphatide are recycled in shrimp med production line waste water, comprises the following steps:
The first step, krill plus water are mixed and heated, obtains mixed material A;
Second step, separation of solid and liquid is carried out by the mixed material A in the first step, obtains boiling rear krill slurry and boil liquid A;
3rd step, boil liquid A is further heated, and the protein encapsulation phosphatide in boil liquid A is formed protein, phospholipid compound;
4th step, carries out separation of solid and liquid by the mixed material B obtained in the 3rd step, obtains protein, phospholipid compound and boil liquid B;
5th step, the protein, phospholipid compound obtained in the 4th step is mixed with the rear krill slurry that boils obtained in second step, Obtain mixing krill material;
6th step, mixing krill material is dried, shrimp med is made;
In the first step, the ratio of krill and water is not less than 1:1,60-75 DEG C of boiling temperature;
The moisture that rear krill slurry is boiled in the second step, after separation is 55-70%, and the solid content of the boil liquid A is 8-12%;
In 3rd step, temperature >=80 DEG C after boil liquid A heatings;
In 4th step, the moisture content range of protein, phospholipid compound is 75-85%.
After isolating boil liquid B in the 4th step, boil liquid B can add the water that water mixes to make as krill in the first step again With formation circulation, this process reduces technique water consumption;But needed in cyclic process ensure boil liquid B with krill raw material Temperature should be less than 50 DEG C during mixing;If the boil liquid B temperature isolated from separator is higher than 50 DEG C, it is necessary to by cooling It can enter in the first step and recycle;More specifically, albumen and phosphatide are recycled from boat-carrying euphausia superba powder production line waste water Method, krill is needed by shelling, defibrination in the first step, stirring, emulsification after mix with water;Shelling uses aperture 2-3mm Roller flesh separator, granularity≤2mm after defibrination.
More specifically, the method for albumen and phosphatide is recycled from boat-carrying euphausia superba powder production line waste water, it is characterised in that: Separation uses two-phase horizontal spiral centrifuge, centrifuge speed >=3500rpm in the second step;Separate and adopt in 4th step With triphase horizontal screw centrifuge, centrifuge speed >=4500rpm.
More specifically, the method for albumen and phosphatide is recycled from boat-carrying euphausia superba powder production line waste water, by such as the 4th step In obtained protein, phospholipid compound be directly dried in vacuo, obtained protein, phospholipid powder, protein content >=50%;Lipid Content >=35%;Content of phospholipid >=40%;Moisture≤10%;The μ g/g of Oil repellent≤30.
Present invention also offers a kind of realize to recycle the auxiliary of albumen and phosphatide from boat-carrying euphausia superba powder production line waste water Device is helped, including is provided with the heating pipe and equipment for separating liquid from solid of automatically cleaning stirring scraper, the connection of heating pipe feed end is general The liquid outlet of horizontal spiral centrifuge on logical production line, discharge end connection equipment for separating liquid from solid;The pipeline center is provided with Shaft, the scraper for being close to duct wall setting is provided with shaft;Shaft both ends are connected by transmission device with motor, described turn Axis, which rotates, drives scraper to carry out continuing cleaning to inner-walls of duct, and the heating pipe is provided with heating unit.
More specifically, a kind of realize the auxiliary dress that albumen and phosphatide are recycled from boat-carrying euphausia superba powder production line waste water Put, the heating unit of the heating pipe is steam jacket, and the equipment for separating liquid from solid is three-phase type horizontal spiral centrifuge.
More specifically, a kind of realize the auxiliary dress that albumen and phosphatide are recycled from boat-carrying euphausia superba powder production line waste water Put, the scraper in the shaft is provided with some groups, is arranged alternately in shaft both sides, and scraper shape is rectangle, the scraper The sum of length is more than the length of heating pipe.
More specifically, a kind of realize the auxiliary dress that albumen and phosphatide are recycled from boat-carrying euphausia superba powder production line waste water Put, the heating unit of the heating pipe is electrical heating, and pipeline is provided with interlayer, is conduction oil in interlayer;The separation of solid and liquid Device is spiral pressing dehydrator.
It is according to mesh that albumen and the method for phosphatide are recycled in the euphausia superba powder production line waste water provided by the invention from boat-carrying The inventive improvements that the krill shrimp med production line common problem of preceding boat-carrying carries out, containing a large amount of water-soluble in krill Albumen, the temperature of its thermal denaturation solidification is higher, and substantial amounts of albuminous degeneration solidification is had in the range of 70-90 DEG C.Therefore, in krill There are contradiction point in the actual mechanical process of shrimp med production line:
When temperature is low (75 DEG C of t <), substantial amounts of water-solubility protein can be lost in boil liquid, and the number of dropouts of this Partial Protein is big About the 30% of total protein, if from total nitrogen angle calculation, the water-solubility protein and nonprotein nitrogen of loss account for total nitrogen More than the 40% of content, or even close to 50%, this is the significant wastage to living marine resources;During this, phosphatide conduct A kind of macromolecular of parents, stable lotion is easily created with water-solubility protein, after lotion is formed, water-solubility protein stream Can be with the loss of phosphatide while mistake, according to experimental data, the amount that phosphatide is lost in accounts for being lost in 20% left side of total solid The right side, the amount of protein loss account for being lost in the 40% of total solid;
When temperature is high (95 DEG C of t >), since the boat-carrying digesting apparatus heating of current krill is carried out using steam Heating, when temperature is excessive, the temperature of digesting apparatus inner wall may be up to 120-150 DEG C, and water-solubility protein can rapidly hold in boiling The adhesion solidification of device inner wall, forms one layer of hot non-conductor, causes the reduction of the digesting apparatus thermal efficiency, can be sent out with time lengthening Raw local " being charred ", finally seriously affects the quality of shrimp med;
Even if by temperature control at medium temperature (75 DEG C of 95 DEG C of < t <), the different journeys of above-mentioned two situations also occur Degree superposition, explains to a certain extent, and since the control of boat-carrying boiling set temperature is unstable, the output capacity that result in shrimp med exists Fluctuation, output capacity are differed from 10 to 14.3% (in terms of shrimp med/fresh krill) in one larger scope.
And the method for the invention, heated by using two-part:
First segment uses the temperature less than 70 DEG C that krill is heated up, and its water miscible albumen is retained in consistency in boil liquid Solidification, at this time, phosphatide are also emulsified in the case where the stirring of boiling vessel is promoted with albumen in boil liquid, form the lotion of muddiness;
Centrifuge, boil liquid and the krill after boiling are separated, boil liquid is then entered into second segment heating schedule;
Second segment is used higher than 85 DEG C of temperature, and the albumen in boil liquid starts denaturation solidification, by phosphatide point while solidification Attached bag is rolled in wherein, forms protein, phospholipid compound, at this time, may be had attachment on the inner wall of steaming plant, at this time, be adopted With device provided by the invention, scraper is stirred by automatically cleaning inner-walls of duct is cleared up, so as to solve current krill meal Contradiction in production line.
The beneficial effects of the present invention are:This method is returned by the way that the separated liquid of feed liquid after boiling is carried out secondary temperature elevation The albumen and phosphatide in boil liquid are received, that is, avoids and apparatus for production line is significantly replaced, while also improve the output of shrimp med Rate, while avoid " being burned " phenomenon of digesting apparatus in production line;Meanwhile additionally provide one kind and realize party's subtraction unit, can Simply to be added on the basis of primary producing line, you can realize above-mentioned function.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing There is attached drawing needed in technology description to be briefly described.It is clear that drawings in the following description are of the invention Some embodiments, for those of ordinary skill in the art, without creative efforts, can also be according to this A little attached drawings obtain other attached drawings.
Fig. 1 is the process flow diagram of the present invention;
Fig. 2 is that the auxiliary of albumen and phosphatide is recycled in the realization of the offer of the present invention from boat-carrying euphausia superba powder production line waste water Help schematic device;
Fig. 3 is setting schematic diagram and mass transfer schematic diagram of the method for the present invention in conventional production lines.
In Fig. 2, heating pipe 1, feed end 11, discharge end 12, shaft 13, scraper 14, transmission device 15, motor 16, Heating unit 17.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention In attached drawing, the technical solution in the embodiment of the present invention is clearly and completely described.Obviously, described embodiment is Part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art All other embodiments obtained without making creative work, belong to the scope of protection of the invention.
Embodiment 1:
A kind of method that albumen and phosphatide are recycled in the euphausia superba powder production line waste water from boat-carrying:
The first step, the krill of fishing is shelled with the roller flesh separator of 2mm, the krill meat slurry particle after defibrination 2mm is remained less than, krill plus water are mixed and heated, the ratio of krill and water is 1:1,70 DEG C of boiling temperature, is mixed Material A;
Second step, separation of solid and liquid is carried out by the mixed material A in the first step, and separation is centrifuged using horizontal spiral centrifuge, The rotating speed of centrifugation is 3500rpm, obtains boiling rear krill slurry and boil liquid A, the moisture that rear krill slurry is boiled after separation is left for 65% The right side, the solid content of the boil liquid A is 8-12%;
3rd step, boil liquid A is further heated, and the protein encapsulation phosphatide in boil liquid A is formed protein, phospholipid compound, is boiled Temperature after liquid A heatings is to 90 DEG C;
4th step, carries out separation of solid and liquid, separation uses triphase horizontal spiral centrifugal by the mixed material B obtained in the 3rd step Machine, rotating speed 4500rpm, obtains protein, phospholipid compound and boil liquid B, the moisture content range of protein, phospholipid compound is 75- 85%;
5th step, the protein, phospholipid compound obtained in the 4th step is mixed with the rear krill slurry that boils obtained in second step, Obtain mixing krill material;
6th step, mixing krill material is dried, shrimp med is made;
Or the protein, phospholipid compound obtained in the 4th step in above-mentioned steps is dried in vacuo, drying temperature 50 DEG C, obtain krill phospholipoprotein powder, protein content 51.32%;Lipid content 37.96%;Content of phospholipid 40.15%;Moisture Content 9.43%;12 μ g/g of Oil repellent.
It is a kind of to realize the auxiliary device that albumen and phosphatide are recycled from boat-carrying euphausia superba powder production line waste water, including set There are the heating pipe 1 and equipment for separating liquid from solid of automatically cleaning stirring scraper, 1 feed end 11 of heating pipe is connected and crouched on common production line The liquid outlet of formula screw centrifuge, discharge end 12 connect equipment for separating liquid from solid;The pipeline center is provided with shaft 13, shaft The scraper 14 for being close to duct wall setting is provided with 13;13 both ends of shaft are connected by transmission device 15 with motor 16, described Shaft 13, which rotates, drives scraper 14 to carry out continuing cleaning to 1 inner wall of pipeline, and the heating pipe 1 is provided with heating unit 17.
The heating unit 17 of the heating pipe 1 is steam jacket, and the equipment for separating liquid from solid is three-phase type horizontal spiral Centrifuge.Or the heating unit 17 of the heating pipe is electrical heating, pipeline is provided with interlayer, is conduction oil in interlayer;Institute It is spiral pressing dehydrator to state equipment for separating liquid from solid.
Scraper 14 in the shaft 13 is provided with some groups, is arranged alternately in 13 both sides of shaft, and 14 shape of scraper is length Square, the sum of described 14 length of scraper is more than the length of heating pipe 1.
The method that albumen and phosphatide are recycled using the device, is concretely comprised the following steps:
The first step, the krill of fishing is shelled with the roller flesh separator of 2mm, the krill meat slurry particle after defibrination 2mm is remained less than, krill plus water are mixed and heated by spiral precooker, the ratio of krill and water is 1:1, boiling temperature 70 DEG C, obtain mixed material A;
Second step, separation of solid and liquid is carried out by the mixed material A in the first step, and separation is centrifuged using horizontal spiral centrifuge, The rotating speed of centrifugation is 3500rpm, obtains boiling rear krill slurry and boil liquid A, the moisture that rear krill slurry is boiled after separation is left for 65% The right side, the solid content of the boil liquid A is 8-12%;
3rd step, boil liquid A is further heated by the heating pipe 1 of auxiliary device, makes the protein encapsulation phosphorus in boil liquid A Fat forms protein, phospholipid compound, and the temperature after boil liquid A heatings is to 90 DEG C;Albumen in boil liquid during heating starts to become Property solidification, while solidification by phospholipid molecule parcel wherein, form protein, phospholipid compound, at this time, may be in boiling There is attachment on the inner wall of device, open motor 16 at this time, drive automatically cleaning to stir scraper 14 by shaft 13 and rotate to pipeline Inner wall is cleared up;
The mixed material B obtained in 3rd step is transferred to equipment for separating liquid from solid and carries out solid-liquid point by the 4th step, discharge end 13 From separation uses triphase horizontal screw centrifuge, and rotating speed 4500rpm, obtains protein, phospholipid compound and boil liquid B, albumen phosphorus The moisture content range of fat complexes is 75-85%;
5th step, the protein, phospholipid compound obtained in the 4th step is mixed with the rear krill slurry that boils obtained in second step, Obtain mixing krill material;
6th step, mixing krill material is dried, shrimp med is made.
It is basis that albumen and the method for phosphatide are recycled in the euphausia superba powder production line waste water provided in this embodiment from boat-carrying The inventive improvements that the krill shrimp med production line common problem of boat-carrying carries out at present, containing a large amount of water-soluble in krill Property albumen, the temperature of its thermal denaturation solidification is higher, and the solidification of substantial amounts of albuminous degeneration is had in the range of 70-90 DEG C.Therefore, in phosphorus There are contradiction point in the actual mechanical process of shrimp shrimp med production line:
When temperature is low (75 DEG C of t <), substantial amounts of water-solubility protein can be lost in boil liquid, and the number of dropouts of this Partial Protein is big About the 30% of total protein, if from total nitrogen angle calculation, the water-solubility protein and nonprotein nitrogen of loss account for total nitrogen More than the 40% of content, or even close to 50%, this is the significant wastage to living marine resources;During this, phosphatide conduct A kind of macromolecular of parents, stable lotion is easily created with water-solubility protein, after lotion is formed, water-solubility protein stream Can be with the loss of phosphatide while mistake, according to experimental data, the amount that phosphatide is lost in accounts for being lost in 20% left side of total solid The right side, the amount of protein loss account for being lost in the 40% of total solid;
When temperature is high (95 DEG C of t >), since the boat-carrying digesting apparatus heating of current krill is carried out using steam Heating, when temperature is excessive, the temperature of digesting apparatus inner wall may be up to 120-150 DEG C, and water-solubility protein can rapidly hold in boiling The adhesion solidification of device inner wall, forms one layer of hot non-conductor, causes the reduction of the digesting apparatus thermal efficiency, can be sent out with time lengthening Raw local " being charred ", finally seriously affects the quality of shrimp med;
Even if by temperature control at medium temperature (75 DEG C of 95 DEG C of < t <), the different journeys of above-mentioned two situations also occur Degree superposition, explains to a certain extent, and since the control of boat-carrying boiling set temperature is unstable, the output capacity that result in shrimp med exists Fluctuation, output capacity are differed from 10 to 14.3% (in terms of shrimp med/fresh krill) in one larger scope.
And the method for the invention, heated by using two-part:
First segment uses the temperature less than 70 DEG C that krill is heated up, and its water miscible albumen is retained in consistency in boil liquid Solidification, at this time, phosphatide are also emulsified in the case where the stirring of boiling vessel is promoted with albumen in boil liquid, form the lotion of muddiness;
Centrifuge, boil liquid and the krill after boiling are separated, boil liquid is then entered into second segment heating schedule;
Second segment is used higher than 85 DEG C of temperature, and the albumen in boil liquid starts denaturation solidification, by phosphatide point while solidification Attached bag is rolled in wherein, forms protein, phospholipid compound, at this time, may be had attachment on the inner wall of steaming plant, at this time, be adopted With device provided by the invention, scraper is stirred by automatically cleaning inner-walls of duct is cleared up, so as to solve current krill meal Contradiction in production line.
By taking the above method, 198kg krill raw materials are processed, the protein, phospholipid recycled in process is compound Thing is 41.94kg, and the moisture of protein, phospholipid compound is 78.04%, and krill raw material moisture is 81%, therefore, should Process recycles dry matter 9.23kg by the 37.62kg dry matters in krill raw material, by the recovery method, accounts for total dry The 24.5% of material.And the method for traditional processing shrimp med can only obtain after boiling when being processed to the krill raw material of same 198kg Shrimp slurry part, weight 105kg, it is 78.28% to boil rear shrimp slurry moisture, dry matter content 22.81kg;Therefore, utilize After the recovery method, the yield of shrimp med can improve 40.46% on the basis of traditional handicraft, this industrialized production in shrimp med On be very big progress.Dry matter ratio forms explanation in krill process:
Remarks:Data are experiment actual measurement, due to inevitable error, cause each several part dry matter summation slightly larger than total Dry matter, there is ± 2.5% deviation.
Euphausia superba powder, krill phospholipoprotein powder and the traditional shrimp med product that new processing technology is obtained (boil rear krill Slurry dried object) it is compared, leading indicator is as follows:
Contrasted in the material of this method recovery section it can be seen from the above results its nutritional ingredient common shrimp med have it is larger Difference, its main cause, which is that fat content is opposite, to be improved, and causes protein content relative reduction, but from Oil repellent, hence it is evident that it is low In traditional shrimp med product.
The beneficial effect of the present embodiment is:This method by the way that the separated liquid of feed liquid after boiling is carried out secondary temperature elevation, The albumen and phosphatide in boil liquid are recycled, that is, avoids and apparatus for production line is significantly replaced, while also improve the production of shrimp med Extracting rate, while avoid " being burned " phenomenon of digesting apparatus in production line;Meanwhile additionally provide one kind and realize party's subtraction unit, Can simply it be added on the basis of primary producing line, you can realize above-mentioned function.

Claims (8)

1. the method for albumen and phosphatide is recycled in a kind of euphausia superba powder production line waste water from boat-carrying, it is characterised in that:Including with Lower step:
The first step, by krill by shelling, defibrination, stirs after being mixed with water, emulsifies, add water mixing and heated, mixed Close material A;
Second step, separation of solid and liquid is carried out by the mixed material A in the first step, obtains boiling rear krill slurry and boil liquid A;
3rd step, boil liquid A is further heated, and the protein encapsulation phosphatide in boil liquid A is formed protein, phospholipid compound;
4th step, carries out separation of solid and liquid by the mixed material B obtained in the 3rd step, obtains protein, phospholipid compound and boil liquid B;
5th step, the protein, phospholipid compound obtained in the 4th step is mixed with the rear krill slurry that boils obtained in second step, is obtained Mix krill material;
6th step, mixing krill material is dried, shrimp med is made;
In the first step, during heating, the ratio of krill slurry and water is not less than 1:1,60-75 DEG C of boiling temperature;
The moisture that rear krill slurry is boiled in the second step, after separation is 55-70%, and the solid content of the boil liquid A is 8- 12%;
In 3rd step, temperature >=80 DEG C after boil liquid A heatings;
In 4th step, the moisture content range of protein, phospholipid compound is 75-85%.
2. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 1, it is special Sign is:Shell and use the roller flesh separator of aperture 2-3mm, granularity≤2mm after defibrination.
3. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 1, it is special Sign is:Separation uses two-phase horizontal spiral centrifuge, centrifuge speed >=3500rpm in the second step;4th step Middle separation uses triphase horizontal screw centrifuge, centrifuge speed >=4500rpm.
4. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 1, it is special Sign is:Directly it is dried in vacuo, is obtained by the protein, phospholipid compound obtained in the 4th step as claimed in claim 1 Protein, phospholipid powder, protein content >=50%;Lipid content >=35%;Content of phospholipid >=40%;Moisture≤10%;Fluorine contains Measure≤30 μ g/g.
5. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 1, it is special Sign is:The auxiliary device of albumen and phosphatide is recycled from boat-carrying euphausia superba powder production line waste water using a kind of realize, including The heating pipe and equipment for separating liquid from solid of automatically cleaning stirring scraper are provided with, heating pipe feed end is connected and crouched on common production line The liquid outlet of formula screw centrifuge, discharge end connection equipment for separating liquid from solid;The pipeline center is provided with shaft, is set in shaft It is equipped with the scraper for being close to duct wall setting;Shaft both ends are connected by transmission device with motor, and the shaft rotates drive and scrapes Knife carries out inner-walls of duct to continue cleaning, and the heating pipe is provided with heating unit.
6. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 5, it is special Sign is:The heating unit of the heating pipe is steam jacket, and the equipment for separating liquid from solid is three-phase type horizontal screw centrifugal Machine.
7. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 5, it is special Sign is:Scraper in the shaft is provided with some groups, is arranged alternately in shaft both sides, and scraper shape is rectangle, described The sum of scraper length is more than the length of heating pipe.
8. recycling the method for albumen and phosphatide from boat-carrying euphausia superba powder production line waste water as claimed in claim 5, it is special Sign is:The heating unit of the heating pipe is electrical heating, and pipeline is provided with interlayer, is conduction oil in interlayer;The solid-liquid Separator is spiral pressing dehydrator.
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CN113980110A (en) * 2021-11-02 2022-01-28 青岛海洋科学与技术国家实验室发展中心 Method for preparing protein peptide by using euphausia superba shelling wastewater
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