CN107056331A - A kind of ceramic tile of resin glue filling porous ceramics formation and preparation method thereof - Google Patents

A kind of ceramic tile of resin glue filling porous ceramics formation and preparation method thereof Download PDF

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Publication number
CN107056331A
CN107056331A CN201710412757.5A CN201710412757A CN107056331A CN 107056331 A CN107056331 A CN 107056331A CN 201710412757 A CN201710412757 A CN 201710412757A CN 107056331 A CN107056331 A CN 107056331A
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CN
China
Prior art keywords
resin glue
porous ceramics
brick
ceramic
ceramic tile
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Pending
Application number
CN201710412757.5A
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Chinese (zh)
Inventor
郑辉
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ANHUI YA'OU CERAMIC Co Ltd
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ANHUI YA'OU CERAMIC Co Ltd
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Priority to CN201710412757.5A priority Critical patent/CN107056331A/en
Publication of CN107056331A publication Critical patent/CN107056331A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/46Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
    • C04B41/48Macromolecular compounds
    • C04B41/4853Epoxides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/46Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/46Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
    • C04B41/48Macromolecular compounds
    • C04B41/4811Condensation polymers of aldehydes or ketones
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/46Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
    • C04B41/48Macromolecular compounds
    • C04B41/488Other macromolecular compounds obtained otherwise than by reactions only involving unsaturated carbon-to-carbon bonds
    • C04B41/4884Polyurethanes; Polyisocyanates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/82Coating or impregnation with organic materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/82Coating or impregnation with organic materials
    • C04B41/83Macromolecular compounds

Abstract

The invention discloses a kind of ceramic tile of resin glue filling porous ceramics formation, by brick body and be overlying on the coating on brick body surface and constitute, described brick body by porous ceramics brick skeleton, the middle film layer being attached on ceramic hole and be filled into outside middle film layer, the resin glue of fill ceramics hole is constituted.

Description

A kind of ceramic tile of resin glue filling porous ceramics formation and preparation method thereof
Technical field
The present invention relates to the ceramic tile and its system in ceramic technology field, more particularly to a kind of filling porous ceramics formation of resin glue Preparation Method.
Background technology
Ceramic Tiles are seen everywhere in daily life, are a kind of important construction materials, and traditional Ceramic Tiles are by clay With other inorganic non-metallic raw materials, tabular or Bulk ceramic product through technique productions such as shaping, sintering, for decorating and protecting Building, the metope of structures and ground.Generally it is molded at room temperature by dry-pressing, extruding or other forming methods, Ran Hougan It is dry, burn till at a certain temperature.It is right because the preparation of traditional ceramic tile needs to consume the native natural resources of substantial amounts of ore deposit and fossil fuel Environment has irreversible harm;In addition, traditional Ceramic Tiles are held from great when being pasted onto on metope after keel stress Yielding, displacement, the length of time one being the problems such as may result in hollowing, drop, and not only influences attractive in appearance also there is potential safety hazard.
Given birth to improve the defect of traditional ceramics brick, the ceramic-like light brick application of non-sintered, this kind of material is relied primarily on Organic or inorganic sizing material replaces high temperature sintering, the imitative ceramic tile that is prepared with some inorganic fillers under normal temperature or relatively low temperature Product, this product reduces the consumption of fossil fuel, and the range of choice to inorganic filler is wider, not only reduces production cost Also so that color and the kind more horn of plenty of ceramic tile, the market competitiveness are stronger.《Total utilization of PCA》Printed on 01 phases in 2013 " preparation of flyash polyurethane ceramic tile imitation and performance study " one text gone out is using flyash as filler, and polyurethane is used as adhesive A kind of non-sintered imitative ceramic tile is prepared for, although needed for this imitative ceramic tile can meet production and living in mechanical property, Corrosion resistance, wear-resistant scratch resistant etc. are poor, and contain some poisonous and harmful substances inside flyash, using being limited in scope.
The content of the invention
The present invention in order to make up the defect of prior art there is provided a kind of ceramic tile of resin glue filling porous ceramics formation and its Preparation method.
The present invention is achieved by the following technical solutions:
A kind of ceramic tile of resin glue filling porous ceramics formation, is made up of brick body and the coating for being overlying on brick body surface, described Brick body is by porous ceramics brick skeleton, the middle film layer being attached on ceramic hole and is filled into outside middle film layer, fills ceramics The resin glue composition of hole.
A kind of preparation method of the ceramic tile of described resin glue filling porous ceramics formation comprises the following steps:
(1)The porous pottery of different porosities and pore shape is made through being molded base, sintering in ceramic slurry according to needed for production Ceramic tile skeleton;
(2)By immersion treatment 12-18h in the porous ceramics brick skeleton input film forming treatment fluid of gained, processing is taken out after terminating, used Deionized water is dried after cleaning 2-3 times;
(3)Ceramic Tiles skeleton after processing is placed on the table, using glue-injection machine pressurization resin by injection glue, gone out after filling Curing process in material, feeding solidification equipment, completes the solidification of resin glue;
(4)Brick body after being fully cured is polished, cleaning, after coating treatment, produce described Ceramic Tiles.
The porosity of described porous ceramics brick skeleton is 10-90%, aperture 1-10mm.
Described film forming treatment fluid is that the concentration being formulated by Dopamine hydrochloride, buffer reagent, water is many of 1-10g/L Bar amine aqueous solution, pH value is 8-8.5.
Described resin glue is one kind in epoxylite glue, phenolic resinoid glue, polyurethane based resin glue.
The present invention is prepared for a kind of ceramics/resin being made up of porous ceramic skeleton, middle poly-dopamine film layer, resin glue Composite ceramics is as the Ceramic Tiles of brick body, and this Ceramic Tiles had both had the advantages that full Ceramic Tiles, again anti-with light-weight refractory, cracking resistance Shake, waterproof corrosion resistant, it is environment-protecting and non-poisonous the advantages of, using poly-dopamine film layer as intermediate layer in preparation process, effectively raise Adhesion strength of the resin in hole, improves the stability of product, and the preparation method high-efficiency environment friendly of ceramic tile of the present invention is adapted to work Industry metaplasia is produced.
Embodiment
A kind of ceramic tile of resin glue filling porous ceramics formation, is made up of, institute brick body and the coating for being overlying on brick body surface The brick body stated is by porous ceramics brick skeleton, the middle film layer being attached on ceramic hole and is filled into outside middle film layer, fills The resin glue composition of ceramic hole.
The preparation method of the embodiment ceramic tile comprises the following steps:
(1)The circular hole porous ceramics that porosity is 45% is made through being molded base, sintering in ceramic slurry according to needed for production Brick skeleton, aperture is 2mm;
(2)By immersion treatment 12h in the porous ceramics brick skeleton input film forming treatment fluid of gained, processing is taken out after terminating, spent Ionized water is dried after cleaning 2 times;
(3)Ceramic Tiles skeleton after processing is placed on the table, using glue-injection machine pressurization injection epoxide-resin glue, after filling Curing process in discharging, feeding solidification equipment, completes the solidification of resin glue;
(4)Brick body after being fully cured is polished, cleaning, after coating treatment, produce described Ceramic Tiles.
Wherein film forming treatment fluid is the dopamine that the concentration being formulated by Dopamine hydrochloride, buffer reagent, water is 1g/L Solution, pH value is 8.

Claims (5)

1. a kind of ceramic tile of resin glue filling porous ceramics formation, is made up of, it is special brick body and the coating for being overlying on brick body surface Levy and be, described brick body is by porous ceramics brick skeleton, the middle film layer being attached on ceramic hole and is filled into intermediate coat Layer is outer, the resin glue composition of the ceramic hole of filling.
2. a kind of preparation method of the ceramic tile of resin glue filling porous ceramics formation as claimed in claim 1, it is characterised in that Comprise the following steps:
(1)The porous pottery of different porosities and pore shape is made through being molded base, sintering in ceramic slurry according to needed for production Ceramic tile skeleton;
(2)By immersion treatment 12-18h in the porous ceramics brick skeleton input film forming treatment fluid of gained, processing is taken out after terminating, used Deionized water is dried after cleaning 2-3 times;
(3)Ceramic Tiles skeleton after processing is placed on the table, using glue-injection machine pressurization resin by injection glue, gone out after filling Curing process in material, feeding solidification equipment, completes the solidification of resin glue;
(4)Brick body after being fully cured is polished, cleaning, after coating treatment, produce described Ceramic Tiles.
3. a kind of preparation method of the ceramic tile of resin glue filling porous ceramics formation as claimed in claim 2, it is characterised in that The porosity of described porous ceramics brick skeleton is 10-90%, aperture 1-10mm.
4. a kind of preparation method of the ceramic tile of resin glue filling porous ceramics formation as claimed in claim 2, it is characterised in that Described film forming treatment fluid is that the concentration being formulated by Dopamine hydrochloride, buffer reagent, water is molten for 1-10g/L dopamine Liquid, pH value is 8-8.5.
5. a kind of preparation method of the ceramic tile of resin glue filling porous ceramics formation as claimed in claim 2, it is characterised in that Described resin glue is one kind in epoxylite glue, phenolic resinoid glue, polyurethane based resin glue.
CN201710412757.5A 2017-06-05 2017-06-05 A kind of ceramic tile of resin glue filling porous ceramics formation and preparation method thereof Pending CN107056331A (en)

Priority Applications (1)

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CN201710412757.5A CN107056331A (en) 2017-06-05 2017-06-05 A kind of ceramic tile of resin glue filling porous ceramics formation and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201710412757.5A CN107056331A (en) 2017-06-05 2017-06-05 A kind of ceramic tile of resin glue filling porous ceramics formation and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107056331A true CN107056331A (en) 2017-08-18

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108571131A (en) * 2018-04-16 2018-09-25 广东金意陶陶瓷集团有限公司 A kind of porous ceramics dalle and preparation method thereof with air-cleaning function
CN113563116A (en) * 2021-07-21 2021-10-29 佛山欧神诺陶瓷有限公司 Composite ceramic tile and preparation method and application thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102234187A (en) * 2010-04-29 2011-11-09 比亚迪股份有限公司 Ceramic composite material and preparation method thereof
CN105920668A (en) * 2016-06-08 2016-09-07 西南交通大学 Preparation method of antibacterial biological activity ceramic coating with magnetic responsiveness

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102234187A (en) * 2010-04-29 2011-11-09 比亚迪股份有限公司 Ceramic composite material and preparation method thereof
CN105920668A (en) * 2016-06-08 2016-09-07 西南交通大学 Preparation method of antibacterial biological activity ceramic coating with magnetic responsiveness

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108571131A (en) * 2018-04-16 2018-09-25 广东金意陶陶瓷集团有限公司 A kind of porous ceramics dalle and preparation method thereof with air-cleaning function
CN113563116A (en) * 2021-07-21 2021-10-29 佛山欧神诺陶瓷有限公司 Composite ceramic tile and preparation method and application thereof

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Application publication date: 20170818