CN107036951A - A kind of micro-channel model for simulating porous media internal flow - Google Patents

A kind of micro-channel model for simulating porous media internal flow Download PDF

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Publication number
CN107036951A
CN107036951A CN201611170135.8A CN201611170135A CN107036951A CN 107036951 A CN107036951 A CN 107036951A CN 201611170135 A CN201611170135 A CN 201611170135A CN 107036951 A CN107036951 A CN 107036951A
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China
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micro
channel
entrance
silicon chip
microtrabeculae
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CN201611170135.8A
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郝鹏飞
李佳琦
谢斌
黄波
王荣
高叶
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Tsinghua University
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Tsinghua University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • G01N15/0826Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/088Investigating volume, surface area, size or distribution of pores; Porosimetry

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  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Fluid Mechanics (AREA)
  • Automatic Analysis And Handling Materials Therefor (AREA)

Abstract

A kind of micro-channel model for simulating porous media internal flow, and in particular to the micro-channel model of Complicated Pore Structures inside simulation core.The model includes silicon chip substrate, and entrance, entrance cavity, entrance, micro-channel, measuring section, outlet plenum and outlet of the etching in silicon chip substrate;Provided with multiple in staggered microtrabeculae in micro-channel, multiple microtrabeculaes formation micro-pillar arrays, the height of microtrabeculae is identical with the depth of micro-channel;Glass cover-plate is provided with the top of silicon chip substrate, the glass cover-plate is realized with micro-channel and silicon chip substrate and is tightly connected.By setting micro-pillar array inside micro-channel, and can be by changing the size, shape and arrangement mode of microtrabeculae, can real Complicated Pore Structures inside simulation core, while the visualization measurement of micro-channel internal flow details can also be realized by the glass cover-plate above micro-channel model.

Description

A kind of micro-channel model for simulating porous media internal flow
Technical field
The present invention relates to a kind of micro-channel model for simulating porous media internal flow, more particularly in a kind of simulation core The micro-channel model of portion's Complicated Pore Structures.
Background technology
In low-permeability oil deposit, blowhole very little and complicated, the Complex Flows how obtained inside rock core are thin Section is significant to understanding percolation law and raising oilfield exploitation efficiency inside rock core in depth.Oozed at present on measurement rock core The method of stream ability is mainly conventional core permeability survey method, i.e., rock core is put into high pressure pressure core flow tester clamper In, salt solution is squeezed into from rock core lower end in the presence of compression pump, upper end outflow, by measuring the pressure difference at rock core two ends and passing through The flow of rock core can calculate the size of permeability.But this method can only provide the overall negotiability of rock core, it is impossible to obtain Flowing details and micro flow mechanism inside rock core.
The content of the invention
It is an object of the invention to provide a kind of micro-channel model for simulating porous media internal flow, by being handed in micro-channel Complicated Pore Structures inside the micro-pillar array simulation core of mistake arrangement, injecting fluid into the micro-channel with micro-pillar array can With the flowing law inside simulation core porous media, and visualization measurement can be realized.
Technical scheme is as follows:
A kind of micro-channel model for simulating porous media internal flow, it is characterised in that:The model includes silicon chip substrate, with And entrance, entrance cavity, entrance, micro-channel, micro-pillar array, measuring section, outlet plenum and outlet of the etching in silicon chip substrate;It is micro- Post array is arranged on micro-channel;The upstream of described micro-channel is connected by entrance with entrance cavity, and the downstream of micro-channel passes through Measuring section is connected with outlet plenum;Described micro-pillar array is to be staggered to form by multiple microtrabeculaes, the height and micro-channel of microtrabeculae Depth it is identical;Glass cover-plate is provided with the top of silicon chip substrate, the glass cover-plate is realized with micro-channel and silicon chip substrate and sealed Connection.
Preferably, described channel depth is 20-80 microns.The section of each microtrabeculae is square, the length of side model of microtrabeculae Enclose for 10-50 microns, microtrabeculae spacing range is 2-10 microns.
Preferably, entrance is identical with the width of measuring section, is 2-3 times of micro-channel width, its depth and micro-channel Depth is identical.
Technique effect of the present invention with advantages below and high-lighting:1. by setting micro-pillar array inside micro-channel, And can be by changing Complicated Pore Structures inside the size, shape and arrangement mode of microtrabeculae, simulation core, while can also pass through Glass cover-plate above micro-channel model realizes that the visualization measurement of details is flowed in micro-channel internal flow.2. the model can pass through Etch and formed on silicon chip, by controlling etch period to process the micro-channel of different depth, preparation method is simple, sealing effect It is really good.
Brief description of the drawings
Fig. 1 is a kind of micro-channel model of simulation core porous media internal flow.
Fig. 2 is Fig. 1 A-A profiles.
Fig. 3 is the structural representation of micro-pillar array embodiment.
In figure:1- entrances;2- entrance cavities;3- entrances;4- micro-channels;5- micro-pillar arrays;6- measuring sections;7- Outlet plenum;8- is exported;9- substrates;10- glass cover-plates.
Embodiment
Concrete structure, principle and the course of work to the present invention elaborate below in conjunction with the accompanying drawings.
Fig. 1 be simulation core porous media internal flow micro-channel model, the model include silicon chip substrate 9, entrance 1, Entrance cavity 3, entrance 3, micro-channel 4, micro-pillar array 5, measuring section 6, outlet plenum 7, outlet 8 and glass cover-plate 10;Described is micro- Post array 5 is to be staggered to form by multiple microtrabeculaes;The upstream of described micro-channel 4 is connected by entrance 3 with entrance cavity 2, The downstream of micro-channel 4 is connected by measuring section 6 with outlet plenum 7;The height of microtrabeculae is identical with the depth of micro-channel;In silicon chip substrate Top be provided with glass cover-plate 10, glass cover-plate 10 and substrate 9 are realized using the method for anode linkage and seal and be connected.
In micro-channel model of the present invention, entrance 3 is identical with the width of measuring section 6, and its width is that micro-channel is wide 2-3 times of degree, its depth is identical with the depth of micro-channel 4.
As shown in figure 3, microtrabeculae of the micro-pillar array 5 by multiple sections for square is constituted, microtrabeculae is in staggered pattern, just The side size range of square microtrabeculae is generally 10-50 microns, and microtrabeculae spacing range is 2-10 microns, and the depth bounds of micro-channel is 20-80 microns, different types of rock core structure can be simulated by designing the micro-pillar array with the different length of sides and spacing.
The preparation method of micro-channel model is that entrance cavity is etched on silicon chip first with the method for photoetching and ion etching 2nd, entrance 3, micro-channel 4, micro-pillar array 5, measuring section 6 and outlet plenum 7, the method for then utilizing bulk silicon etching in silicon chip back side Two through holes are made respectively in entrance cavity 2 and outlet plenum 7 as entrance 1 and outlet 8, are finally realized with the method for anode linkage The sealing of glass cover-plate 10 and silicon chip substrate 9 and the encapsulation of micro-channel.(as shown in Figure 2).
The measurement process of the present invention is as follows:
Testing liquid is injected into micro-channel model by graduated cylinder or compression pump, fluid is by entrance 3 and with micro- Measuring section 6 is flowed into the micro-channel 4 of post array 5, can obtain a certain by recording not the liquid level position in measuring section in the same time The flow of micro-channel is flowed through under driving pressure.If adding trace particle in a fluid, spike is not recorded by record in the same time Position of the particle in the gap of micro-pillar array 5 obtains the VELOCITY DISTRIBUTION of fluid.

Claims (4)

1. a kind of micro-channel model for simulating porous media internal flow, it is characterised in that:The model includes silicon chip substrate (9), And entrance (1) of the etching in silicon chip substrate, entrance cavity (2), entrance (3), micro-channel (4), micro-pillar array (5), measurement Section (6), outlet plenum (7) and outlet (8);Micro-pillar array (5) is arranged on micro-channel (4);The upstream of described micro-channel (4) passes through Entrance (3) is connected with entrance cavity (2), and the downstream of micro-channel (4) is connected by measuring section (6) with outlet plenum (7);Described is micro- Post array (5) is to be staggered to form by multiple microtrabeculaes, and the height of microtrabeculae is identical with the depth of micro-channel;On the top of silicon chip substrate Portion is provided with glass cover-plate (10), and the glass cover-plate is realized with micro-channel and silicon chip substrate and is tightly connected.
2. a kind of micro-channel model for simulating porous media internal flow according to claim 1, it is characterised in that:Each The section of microtrabeculae is square, and the side size range of microtrabeculae is 10-50 microns, and microtrabeculae spacing range is 2-10 microns.
3. a kind of micro-channel model for simulating porous media internal flow according to claim 1 or 2, it is characterised in that: Described channel depth is 20-80 microns.
4. a kind of micro-channel model for simulating porous media internal flow according to claim 3, it is characterised in that:It is described Entrance (3) is identical with the width of measuring section (3), is 2-3 times of micro-channel width, and its depth is identical with the depth of micro-channel.
CN201611170135.8A 2016-12-16 2016-12-16 A kind of micro-channel model for simulating porous media internal flow Pending CN107036951A (en)

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CN109827822A (en) * 2019-03-15 2019-05-31 西北大学 A kind of true rock flow model in porous media of high-temperature and high-pressure visual and preparation method thereof
CN113092339A (en) * 2021-04-10 2021-07-09 河南工业大学 Visual micro-channel model for simulating migration process of pollutants in porous medium containing preferential flow
CN115254213A (en) * 2022-06-24 2022-11-01 中国计量大学 Micro-fluidic chip device based on real soil pore network

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CN109827822A (en) * 2019-03-15 2019-05-31 西北大学 A kind of true rock flow model in porous media of high-temperature and high-pressure visual and preparation method thereof
CN113092339A (en) * 2021-04-10 2021-07-09 河南工业大学 Visual micro-channel model for simulating migration process of pollutants in porous medium containing preferential flow
CN115254213A (en) * 2022-06-24 2022-11-01 中国计量大学 Micro-fluidic chip device based on real soil pore network
CN115254213B (en) * 2022-06-24 2024-05-03 中国计量大学 Microfluidic chip device based on true soil pore network

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